# SK1806 # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 759' _shelx_refln_list_code 4 _shelx_F_calc_maximum 205.60 _exptl_crystal_F_000 280.00 _reflns_d_resolution_high 0.7694 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.0671 _cell_length_b 8.0739 _cell_length_c 8.6212 _cell_angle_alpha 112.616 _cell_angle_beta 115.060 _cell_angle_gamma 93.810 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13282.62 12558.99 145.52 o 3 0 0 2285.59 2262.60 31.73 o 4 0 0 3772.17 3709.18 46.15 o 5 0 0 1856.39 1875.16 28.41 o 6 0 0 169.83 167.93 6.03 o 7 0 0 1294.71 1341.35 52.96 o 8 0 0 88.13 92.88 18.84 o 9 0 0 342.41 263.72 32.45 o -9 1 0 786.72 824.90 52.97 o -8 1 0 348.57 338.58 30.78 o -7 1 0 1145.21 1216.70 43.62 o -6 1 0 765.11 750.92 26.03 o -5 1 0 1534.74 1577.48 24.67 o -4 1 0 1336.31 1271.26 19.96 o -3 1 0 609.68 574.31 10.33 o -2 1 0 5592.10 5195.82 69.80 o 1 1 0 4940.50 4642.79 58.87 o 2 1 0 3391.21 3225.19 40.86 o 3 1 0 5778.62 5489.79 66.27 o 4 1 0 125.68 127.71 5.37 o 5 1 0 3474.89 3573.34 57.98 o 6 1 0 39.18 47.56 5.34 o 7 1 0 512.39 508.16 16.11 o 8 1 0 332.75 296.99 38.22 o -9 2 0 294.45 226.74 28.37 o -8 2 0 755.48 791.02 37.41 o -7 2 0 315.05 297.21 28.93 o -6 2 0 2503.13 2534.31 58.40 o -5 2 0 163.41 161.39 5.64 o -4 2 0 4875.00 4902.64 68.87 o -3 2 0 1776.11 1687.12 28.60 o -2 2 0 3419.84 3263.39 49.87 o -1 2 0 3179.93 2972.87 49.87 o 0 2 0 2805.48 2652.73 46.66 o 1 2 0 6691.58 6286.61 100.45 o 2 2 0 49.83 49.43 3.58 o 3 2 0 4019.89 3976.76 54.79 o 4 2 0 432.58 423.84 12.33 o 5 2 0 1720.62 1765.10 44.01 o 6 2 0 1152.42 1227.72 31.20 o 7 2 0 1384.17 1279.48 43.67 o 8 2 0 379.52 346.60 43.52 o -9 3 0 66.18 54.68 21.37 o -8 3 0 1089.24 1154.18 53.12 o -7 3 0 487.74 462.73 16.20 o -6 3 0 3421.71 3519.70 54.55 o -5 3 0 1163.42 1185.84 21.20 o -4 3 0 3379.96 3273.68 46.44 o -3 3 0 5289.88 5267.97 78.63 o -2 3 0 2291.86 2422.29 46.80 o -1 3 0 9951.49 9640.38 161.78 o 0 3 0 7.38 13.85 4.97 o 1 3 0 2869.76 2779.86 49.74 o 2 3 0 363.95 343.52 8.56 o 3 3 0 595.23 578.80 13.07 o 4 3 0 1030.10 1018.40 22.35 o 5 3 0 57.73 46.35 8.33 o 6 3 0 329.90 358.01 18.75 o 7 3 0 310.55 263.41 25.00 o -9 4 0 55.06 90.54 52.01 o -8 4 0 562.19 525.50 49.12 o -7 4 0 8.70 13.76 5.12 o -6 4 0 43.65 44.57 5.22 o -5 4 0 1614.62 1683.03 30.94 o -4 4 0 0.13 10.74 5.14 o -3 4 0 2896.40 2753.15 53.21 o -2 4 0 816.56 804.29 16.39 o -1 4 0 3365.84 3319.79 61.60 o 0 4 0 1724.87 1655.29 36.24 o 1 4 0 2200.89 2261.89 46.27 o 2 4 0 3811.61 3842.83 60.04 o 3 4 0 291.07 286.34 12.91 o 4 4 0 1911.58 1953.26 42.07 o 5 4 0 63.26 48.95 11.65 o 6 4 0 781.31 778.61 44.13 o 7 4 0 52.93 43.92 18.64 o -9 5 0 703.25 612.56 75.13 o -8 5 0 161.03 166.09 30.82 o -7 5 0 2725.79 2790.61 68.90 o -6 5 0 15.06 7.07 6.46 o -5 5 0 1841.37 1945.73 53.88 o -4 5 0 471.39 437.45 16.08 o -3 5 0 1460.89 1525.67 37.33 o -2 5 0 1285.26 1235.13 26.09 o -1 5 0 384.05 393.06 12.86 o 0 5 0 4267.53 4298.61 80.61 o 1 5 0 89.17 98.17 8.32 o 2 5 0 1808.59 1885.46 39.84 o 3 5 0 77.05 66.68 8.09 o 4 5 0 991.67 949.52 32.03 o 5 5 0 201.21 207.08 24.31 o 6 5 0 227.25 237.94 25.19 o -8 6 0 156.03 127.38 25.04 o -7 6 0 1115.75 1080.97 66.21 o -6 6 0 740.17 734.56 54.50 o -5 6 0 1322.62 1270.26 38.29 o -4 6 0 1622.17 1801.84 47.00 o -3 6 0 172.29 172.50 12.63 o -2 6 0 2273.92 2337.19 45.55 o -1 6 0 63.21 58.42 6.87 o 0 6 0 157.53 146.09 12.51 o 1 6 0 1451.82 1485.18 34.25 o 2 6 0 319.67 324.92 15.92 o 3 6 0 1076.16 1073.17 39.63 o 4 6 0 4.38 39.89 16.07 o 5 6 0 663.14 581.63 55.93 o -8 7 0 226.66 166.67 47.19 o -7 7 0 228.10 222.82 53.94 o -6 7 0 1623.66 1571.90 80.37 o -5 7 0 1.64 7.62 12.21 o -4 7 0 3390.26 3292.08 98.53 o -3 7 0 137.89 156.90 14.47 o -2 7 0 2685.25 2684.75 62.91 o -1 7 0 1071.74 1100.84 31.91 o 0 7 0 2662.74 2691.92 63.88 o 1 7 0 875.46 923.16 28.91 o 2 7 0 96.62 98.23 16.13 o 3 7 0 789.70 767.41 48.38 o 4 7 0 15.40 12.93 22.43 o -7 8 0 2.42 17.34 40.45 o -6 8 0 855.10 871.74 61.11 o -5 8 0 122.80 77.05 46.23 o -4 8 0 442.92 387.20 69.93 o -3 8 0 818.34 785.85 53.48 o -2 8 0 244.15 266.83 20.19 o -1 8 0 1370.85 1407.90 62.77 o 0 8 0 12.68 13.17 15.00 o 1 8 0 1095.46 1118.16 63.94 o 2 8 0 41.34 36.00 23.39 o 3 8 0 444.63 452.68 69.35 o -5 9 0 895.46 813.71 69.43 o -4 9 0 123.75 119.94 41.39 o -3 9 0 1112.62 1077.47 77.64 o -2 9 0 29.23 38.53 36.78 o -1 9 0 595.44 516.73 59.52 o 0 9 0 246.45 238.38 40.25 o -2 -9 1 578.44 512.49 50.96 o -1 -9 1 23.65 29.38 22.07 o 0 -9 1 1185.20 1310.16 84.93 o 1 -9 1 14.01 21.40 24.07 o 2 -9 1 1028.78 1020.22 112.69 o 3 -9 1 515.49 474.42 48.22 o 4 -9 1 397.54 358.86 43.33 o 5 -9 1 512.21 373.63 42.38 o -3 -8 1 22.20 19.06 19.19 o -2 -8 1 798.00 792.41 49.20 o -1 -8 1 76.01 63.72 14.74 o 0 -8 1 700.30 686.78 30.62 o 1 -8 1 869.03 922.01 34.46 o 2 -8 1 195.93 178.79 23.07 o 3 -8 1 1773.22 1700.03 77.63 o 4 -8 1 39.81 18.08 17.30 o 5 -8 1 1621.51 1497.57 83.92 o 6 -8 1 291.71 249.13 38.53 o 7 -8 1 584.05 591.37 61.64 o -5 -7 1 103.29 44.64 29.17 o -4 -7 1 638.73 638.29 70.21 o -3 -7 1 468.21 417.52 44.74 o -2 -7 1 238.46 231.76 17.60 o -1 -7 1 1388.25 1434.56 42.88 o 0 -7 1 138.62 145.64 16.94 o 1 -7 1 1783.79 1846.99 49.14 o 2 -7 1 20.77 14.36 8.61 o 3 -7 1 1435.59 1550.59 49.17 o 4 -7 1 678.82 604.36 24.13 o 5 -7 1 979.84 984.33 34.56 o 6 -7 1 715.18 666.95 36.29 o 7 -7 1 406.58 378.48 35.41 o -6 -6 1 782.08 710.77 59.69 o -5 -6 1 260.08 242.11 28.49 o -4 -6 1 327.54 317.33 22.47 o -3 -6 1 1428.49 1461.00 36.35 o -2 -6 1 175.22 173.90 14.77 o -1 -6 1 2632.66 2837.95 59.40 o 0 -6 1 270.68 272.15 12.73 o 1 -6 1 3003.33 3134.29 57.10 o 2 -6 1 1788.68 1812.03 33.13 o 3 -6 1 1161.90 1176.78 36.73 o 4 -6 1 1361.10 1396.29 33.82 o 5 -6 1 164.85 183.53 13.47 o 6 -6 1 1331.42 1394.75 56.78 o 7 -6 1 102.31 132.12 22.20 o 8 -6 1 807.77 759.42 50.18 o -7 -5 1 257.66 223.84 36.98 o -6 -5 1 63.97 60.47 16.36 o -5 -5 1 1033.51 1003.60 37.47 o -4 -5 1 26.77 21.26 6.69 o -3 -5 1 2774.55 2949.23 53.61 o -2 -5 1 404.47 407.91 13.44 o -1 -5 1 3009.57 2998.74 55.61 o 0 -5 1 2420.30 2444.95 49.47 o 1 -5 1 851.97 807.79 19.14 o 2 -5 1 5809.09 5901.30 77.04 o 3 -5 1 138.45 136.46 10.63 o 4 -5 1 5231.02 5377.01 93.31 o 5 -5 1 732.87 757.04 20.44 o 6 -5 1 2255.57 2330.46 50.65 o 7 -5 1 721.32 698.16 21.54 o 8 -5 1 414.17 381.80 28.89 o -7 -4 1 476.16 547.08 48.53 o -6 -4 1 1.88 3.00 9.03 o -5 -4 1 1356.19 1364.51 35.86 o -4 -4 1 266.14 251.90 10.93 o -3 -4 1 680.43 631.44 15.40 o -2 -4 1 1632.99 1605.39 29.37 o -1 -4 1 1197.30 1225.58 25.61 o 0 -4 1 3899.91 3866.03 67.07 o 1 -4 1 1298.38 1441.25 28.38 o 2 -4 1 3315.04 3214.95 43.26 o 3 -4 1 489.15 496.84 12.25 o 4 -4 1 2449.27 2494.11 39.18 o 5 -4 1 671.33 680.72 15.45 o 6 -4 1 559.07 575.82 16.75 o 7 -4 1 1541.77 1589.09 39.82 o 8 -4 1 19.36 22.34 19.23 o -8 -3 1 21.98 17.78 25.30 o -7 -3 1 1193.29 1269.49 56.80 o -6 -3 1 621.28 593.93 19.54 o -5 -3 1 706.09 720.47 18.39 o -4 -3 1 3398.93 3439.87 53.36 o -3 -3 1 946.41 986.89 18.43 o -2 -3 1 5741.01 5585.05 78.77 o -1 -3 1 331.13 324.96 9.01 o 0 -3 1 5283.62 5126.73 103.90 o 1 -3 1 4711.14 4677.12 75.87 o 2 -3 1 3150.34 3079.62 40.79 o 3 -3 1 2780.17 2781.90 38.22 o 4 -3 1 763.38 753.28 14.18 o 5 -3 1 3634.24 3821.62 57.79 o 6 -3 1 1.18 -4.87 4.87 o 7 -3 1 1292.22 1339.87 29.18 o 8 -3 1 214.69 208.08 56.83 o 9 -3 1 459.27 471.71 55.90 o -8 -2 1 184.24 190.67 35.92 o -7 -2 1 240.31 226.86 12.35 o -6 -2 1 867.99 882.64 29.46 o -5 -2 1 207.52 205.55 8.37 o -4 -2 1 3211.50 3236.31 43.07 o -3 -2 1 729.75 699.83 12.59 o -2 -2 1 5461.19 5176.32 63.48 o -1 -2 1 2809.44 2664.19 41.11 o 0 -2 1 4947.96 4763.56 70.95 o 1 -2 1 4491.75 4381.52 56.41 o 2 -2 1 1166.07 1179.10 18.81 o 3 -2 1 4552.87 4454.06 57.52 o 4 -2 1 601.42 613.96 11.63 o 5 -2 1 1736.40 1831.43 33.21 o 6 -2 1 523.25 537.54 14.37 o 7 -2 1 580.62 558.86 17.54 o 8 -2 1 273.48 317.08 31.03 o 9 -2 1 22.14 57.79 36.60 o -9 -1 1 25.36 43.25 26.84 o -8 -1 1 655.41 668.17 39.49 o -7 -1 1 0.73 4.37 12.23 o -6 -1 1 2103.30 2254.07 43.05 o -5 -1 1 188.69 181.70 6.31 o -4 -1 1 1091.20 1090.44 18.18 o -3 -1 1 1015.85 990.01 16.37 o -2 -1 1 2647.52 2567.92 34.75 o -1 -1 1 4449.78 4209.00 89.51 o 1 -1 1 8406.67 7748.26 98.67 o 2 -1 1 1776.91 1713.76 24.76 o 3 -1 1 6612.22 6448.30 78.55 o 4 -1 1 840.54 777.37 13.91 o 5 -1 1 1282.34 1292.69 26.04 o 6 -1 1 2073.31 2155.95 40.95 o 7 -1 1 5.68 9.56 3.75 o 8 -1 1 1303.83 1342.12 64.69 o -9 0 1 6.92 8.01 24.93 o -8 0 1 926.56 922.71 47.83 o -7 0 1 651.36 666.76 29.83 o -6 0 1 333.58 296.27 15.39 o -5 0 1 3995.00 4004.96 74.19 o -4 0 1 779.98 757.46 20.15 o -3 0 1 6649.10 6106.44 107.77 o -2 0 1 745.56 715.09 13.68 o 1 0 1 1167.93 1157.30 21.59 o 2 0 1 1130.86 1045.40 18.02 o 3 0 1 240.74 239.92 6.44 o 4 0 1 3434.32 3534.82 49.88 o 5 0 1 2.79 -0.98 3.92 o 6 0 1 1244.55 1274.87 31.39 o 7 0 1 56.49 45.95 7.74 o 8 0 1 291.70 260.98 32.47 o -9 1 1 318.20 263.33 31.10 o -8 1 1 322.04 309.59 26.96 o -7 1 1 1190.63 1222.77 42.93 o -6 1 1 281.64 285.64 15.04 o -5 1 1 3159.40 3156.32 70.90 o -4 1 1 1017.12 993.99 34.02 o -3 1 1 3096.51 3000.88 56.90 o -2 1 1 4866.02 4726.46 90.39 o -1 1 1 2531.20 2420.75 40.67 o 0 1 1 9349.78 8902.99 137.19 o 1 1 1 748.34 714.21 14.60 o 2 1 1 5026.38 4828.52 63.50 o 3 1 1 481.01 495.56 10.93 o 4 1 1 1313.18 1306.59 23.09 o 5 1 1 382.83 381.07 11.71 o 6 1 1 307.49 288.05 12.47 o 7 1 1 543.65 496.53 22.61 o 8 1 1 27.54 6.78 21.47 o -9 2 1 767.81 743.29 44.86 o -8 2 1 2.00 -9.25 15.86 o -7 2 1 2199.78 2394.61 95.32 o -6 2 1 476.85 473.01 23.66 o -5 2 1 2178.35 2285.96 35.67 o -4 2 1 2491.48 2474.17 39.24 o -3 2 1 4285.89 4266.09 75.30 o -2 2 1 6013.29 5797.38 97.88 o -1 2 1 114.99 125.79 5.48 o 0 2 1 7735.79 7603.31 119.36 o 1 2 1 2396.00 2438.79 41.03 o 2 2 1 5880.50 5829.28 73.76 o 3 2 1 1462.60 1510.39 30.12 o 4 2 1 1133.99 1110.66 23.78 o 5 2 1 2387.44 2513.71 66.46 o 6 2 1 26.11 15.61 10.09 o 7 2 1 813.27 796.02 43.62 o -9 3 1 695.47 749.40 47.50 o -8 3 1 402.57 347.12 30.44 o -7 3 1 401.37 401.78 19.54 o -6 3 1 1839.36 1977.92 41.37 o -5 3 1 366.93 357.71 11.35 o -4 3 1 2739.19 2678.10 44.27 o -3 3 1 1078.59 1207.70 25.70 o -2 3 1 3582.64 3522.98 54.83 o -1 3 1 1306.97 1333.58 26.75 o 0 3 1 2185.89 2124.62 38.98 o 1 3 1 1035.67 932.57 21.67 o 2 3 1 362.19 338.36 10.03 o 3 3 1 2605.83 2660.17 42.88 o 4 3 1 1.63 4.10 6.13 o 5 3 1 1012.59 994.23 28.78 o 6 3 1 117.87 93.33 19.31 o 7 3 1 446.00 452.81 34.49 o -9 4 1 443.64 367.92 63.57 o -8 4 1 1494.97 1486.26 50.05 o -7 4 1 317.25 307.41 12.91 o -6 4 1 3834.46 4005.86 75.60 o -5 4 1 227.56 242.69 8.15 o -4 4 1 4965.56 5085.50 91.19 o -3 4 1 1163.97 1120.01 30.13 o -2 4 1 2797.61 2824.34 58.87 o -1 4 1 4262.09 4124.95 63.68 o 0 4 1 456.34 432.19 14.28 o 1 4 1 4171.88 4248.64 74.01 o 2 4 1 60.15 48.37 5.89 o 3 4 1 1679.20 1711.94 33.86 o 4 4 1 125.43 127.07 12.75 o 5 4 1 515.25 502.72 41.98 o 6 4 1 363.86 390.64 48.49 o -9 5 1 53.99 63.57 50.08 o -8 5 1 938.84 811.95 45.49 o -7 5 1 98.01 90.08 10.82 o -6 5 1 1066.68 1073.07 37.75 o -5 5 1 1116.76 1135.41 33.96 o -4 5 1 1523.08 1531.85 43.00 o -3 5 1 3581.34 3679.66 75.24 o -2 5 1 145.12 138.38 8.42 o -1 5 1 3758.01 3931.63 68.39 o 0 5 1 294.11 311.78 13.70 o 1 5 1 2188.70 2199.54 51.13 o 2 5 1 619.67 606.91 18.99 o 3 5 1 398.21 394.33 21.25 o 4 5 1 1467.33 1488.21 55.68 o 5 5 1 33.51 41.54 18.59 o -8 6 1 526.91 549.11 85.72 o -7 6 1 821.99 803.15 41.66 o -6 6 1 605.55 553.22 29.88 o -5 6 1 1272.65 1303.62 46.48 o -4 6 1 17.38 44.65 11.26 o -3 6 1 1905.47 1974.79 51.28 o -2 6 1 165.90 179.77 12.60 o -1 6 1 1918.27 1911.77 50.73 o 0 6 1 582.27 563.86 24.52 o 1 6 1 811.30 825.34 36.61 o 2 6 1 1332.42 1341.48 53.27 o 3 6 1 168.48 145.18 29.98 o 4 6 1 453.33 505.13 41.88 o -8 7 1 143.67 98.34 24.07 o -7 7 1 1312.65 1332.21 138.69 o -6 7 1 68.88 11.23 55.86 o -5 7 1 1702.37 1638.93 67.94 o -4 7 1 229.68 211.70 18.95 o -3 7 1 1040.11 1083.59 32.34 o -2 7 1 861.48 887.13 33.92 o -1 7 1 95.54 110.98 16.10 o 0 7 1 943.25 1074.06 50.19 o 1 7 1 43.12 65.47 25.89 o 2 7 1 531.03 536.53 40.17 o 3 7 1 92.73 61.78 26.62 o -7 8 1 434.00 350.58 52.01 o -6 8 1 422.98 382.45 44.39 o -5 8 1 459.69 419.51 122.32 o -4 8 1 1258.85 1265.82 76.95 o -3 8 1 2.96 21.19 31.33 o -2 8 1 1559.11 1642.35 90.51 o -1 8 1 44.09 21.72 19.24 o 0 8 1 919.03 918.18 53.18 o 1 8 1 93.04 87.51 22.37 o -4 9 1 784.00 843.71 78.01 o -3 9 1 0.62 4.92 25.45 o -2 9 1 472.28 440.22 48.22 o -1 9 1 251.58 222.69 50.40 o 0 -10 2 14.17 4.77 31.24 o 1 -10 2 914.93 901.24 76.09 o 2 -10 2 140.74 90.54 32.35 o 3 -10 2 749.46 674.20 94.39 o -3 -9 2 646.94 566.36 54.48 o -2 -9 2 2.66 -0.39 23.82 o -1 -9 2 926.17 942.73 93.26 o 0 -9 2 216.94 173.97 22.15 o 1 -9 2 669.61 598.31 61.64 o 2 -9 2 378.71 308.09 42.89 o 3 -9 2 140.75 97.25 25.17 o 4 -9 2 921.63 850.03 70.48 o 5 -9 2 0.10 -3.61 21.29 o -4 -8 2 72.03 88.75 26.12 o -3 -8 2 398.31 382.46 36.12 o -2 -8 2 1744.02 1711.81 68.77 o -1 -8 2 557.40 540.71 28.26 o 0 -8 2 1977.80 2049.27 60.79 o 1 -8 2 50.29 37.22 10.87 o 2 -8 2 3196.64 3078.57 95.77 o 3 -8 2 15.98 3.74 22.27 o 4 -8 2 1718.00 1715.74 108.20 o 5 -8 2 265.49 207.14 28.60 o 6 -8 2 295.00 271.61 50.08 o -5 -7 2 567.69 523.67 41.77 o -4 -7 2 220.72 220.57 25.93 o -3 -7 2 952.04 957.63 38.71 o -2 -7 2 170.30 185.18 13.92 o -1 -7 2 44.27 30.24 9.79 o 0 -7 2 1900.68 1943.06 44.86 o 1 -7 2 195.10 216.66 16.28 o 2 -7 2 1297.49 1342.07 30.86 o 3 -7 2 1497.45 1612.35 59.87 o 4 -7 2 731.61 777.90 39.25 o 5 -7 2 1524.47 1563.59 66.33 o 6 -7 2 158.55 163.87 24.40 o 7 -7 2 1120.94 1119.17 88.61 o -6 -6 2 444.38 402.94 42.50 o -5 -6 2 44.11 39.81 14.80 o -4 -6 2 1004.85 1014.87 36.62 o -3 -6 2 72.65 76.33 12.06 o -2 -6 2 2823.24 3019.44 63.02 o -1 -6 2 334.32 315.73 12.80 o 0 -6 2 1192.72 1180.14 25.19 o 1 -6 2 1252.46 1266.52 36.70 o 2 -6 2 542.23 541.63 14.92 o 3 -6 2 2110.15 2121.39 47.29 o 4 -6 2 58.42 53.48 9.12 o 5 -6 2 3529.42 3713.24 86.10 o 6 -6 2 346.61 356.38 25.15 o 7 -6 2 1016.92 1028.32 59.49 o 8 -6 2 609.79 616.41 57.79 o -7 -5 2 19.38 12.07 19.89 o -6 -5 2 859.61 885.13 44.59 o -5 -5 2 221.01 194.53 19.67 o -4 -5 2 1745.45 1778.86 45.11 o -3 -5 2 1329.36 1296.94 31.00 o -2 -5 2 1011.15 953.46 23.47 o -1 -5 2 2362.80 2408.28 44.29 o 0 -5 2 579.52 589.09 21.96 o 1 -5 2 2948.04 3016.79 64.90 o 2 -5 2 0.23 4.57 5.13 o 3 -5 2 1847.27 1869.57 33.37 o 4 -5 2 13.93 16.13 3.85 o 5 -5 2 23.20 22.09 6.02 o 6 -5 2 675.08 681.55 21.96 o 7 -5 2 91.84 87.34 14.44 o -8 -4 2 170.17 183.00 67.42 o -7 -4 2 36.61 32.31 14.70 o -6 -4 2 597.39 531.13 22.49 o -5 -4 2 337.59 313.33 13.77 o -4 -4 2 311.30 293.64 12.60 o -3 -4 2 1989.20 1954.58 44.50 o -2 -4 2 4.73 7.95 5.41 o -1 -4 2 6816.46 6880.04 128.95 o 0 -4 2 2239.16 2377.64 46.14 o 1 -4 2 4050.51 4210.14 69.33 o 2 -4 2 4290.08 4204.45 69.82 o 3 -4 2 1193.88 1212.00 22.37 o 4 -4 2 5042.62 5205.38 78.49 o 5 -4 2 514.53 533.41 15.89 o 6 -4 2 1764.26 1871.14 42.12 o 7 -4 2 126.06 97.71 16.61 o 8 -4 2 546.79 506.08 44.05 o -8 -3 2 445.41 444.97 75.13 o -7 -3 2 768.24 731.81 27.54 o 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