# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' imw212m in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 231.96 _exptl_crystal_F_000 1048.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.6308 _cell_length_b 11.9248 _cell_length_c 18.5690 _cell_angle_alpha 96.558 _cell_angle_beta 106.782 _cell_angle_gamma 105.669 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 39740.04 39064.48 272.64 o 2 0 0 3252.41 3465.85 36.63 o 3 0 0 1221.68 1171.30 39.42 o 4 0 0 3412.12 3223.19 49.80 o 5 0 0 6022.94 5670.05 69.37 o 6 0 0 4318.30 4102.22 61.37 o 7 0 0 5366.44 5499.18 78.32 o 8 0 0 3202.91 3102.33 60.81 o 9 0 0 4405.50 4453.69 78.69 o 10 0 0 1392.07 1389.77 252.60 o 11 0 0 2082.14 2183.75 96.32 o 12 0 0 2805.94 2835.83 116.55 o -12 1 0 259.26 336.06 97.99 o -11 1 0 168.86 246.87 45.98 o -10 1 0 726.18 686.67 53.90 o -9 1 0 468.82 434.03 37.53 o -8 1 0 1632.31 1668.64 44.82 o -7 1 0 1655.96 1820.35 42.95 o -6 1 0 3676.51 3731.45 57.59 o -5 1 0 6109.83 6061.25 71.00 o -4 1 0 1952.28 1851.20 32.36 o -3 1 0 5194.49 5280.47 54.45 o -2 1 0 4479.69 4991.04 46.77 o -1 1 0 10188.56 10896.32 93.76 o 0 1 0 22546.00 23289.46 190.49 o 1 1 0 2741.89 2877.03 35.34 o 2 1 0 1215.55 1240.90 20.84 o 3 1 0 5796.79 5776.03 60.17 o 4 1 0 2003.59 1995.10 35.18 o 5 1 0 2110.95 2025.92 39.46 o 6 1 0 3416.24 3224.11 73.48 o 7 1 0 1501.58 1464.24 42.26 o 8 1 0 1294.62 1211.68 40.93 o 9 1 0 4578.81 4581.22 102.89 o 10 1 0 577.03 551.14 96.50 o 11 1 0 3062.37 3129.42 118.09 o 12 1 0 1917.76 1944.15 105.20 o -13 2 0 455.95 354.25 80.43 o -12 2 0 991.95 1053.12 105.58 o -11 2 0 440.29 338.05 40.82 o -10 2 0 174.35 115.12 30.63 o -9 2 0 126.64 96.14 20.79 o -8 2 0 29.81 3.30 14.51 o -7 2 0 63.85 49.23 15.50 o -6 2 0 50.85 23.54 12.94 o -5 2 0 7.11 -13.64 8.03 o -4 2 0 2590.28 2551.03 38.51 o -3 2 0 1096.20 1046.19 32.04 o -2 2 0 6785.58 6994.35 61.51 o -1 2 0 25.81 33.39 10.40 o 0 2 0 1799.58 1893.01 23.01 o 1 2 0 2937.35 2783.55 39.78 o 2 2 0 66.10 58.85 10.93 o 3 2 0 107.80 82.14 16.00 o 4 2 0 30.89 14.68 9.15 o 5 2 0 30.26 28.24 11.39 o 6 2 0 39.33 50.15 13.81 o 7 2 0 352.71 323.01 28.86 o 8 2 0 11.20 0.72 19.92 o 9 2 0 391.85 348.20 50.36 o 10 2 0 105.66 64.67 48.89 o 11 2 0 103.12 92.01 44.60 o -13 3 0 636.06 811.21 102.83 o -12 3 0 1838.97 1813.25 90.10 o -11 3 0 1793.04 1782.99 84.32 o -10 3 0 1268.88 1312.32 56.81 o -9 3 0 2295.99 2286.37 54.79 o -8 3 0 877.97 900.92 34.56 o -7 3 0 3644.89 3645.09 60.24 o -6 3 0 3856.45 3989.46 59.35 o -5 3 0 5409.72 5667.70 68.17 o -4 3 0 5092.80 5004.92 91.98 o -3 3 0 21841.94 22812.28 173.20 o -2 3 0 1129.86 1097.87 20.81 o -1 3 0 1042.75 970.94 20.62 o 0 3 0 2614.97 2834.00 31.36 o 1 3 0 10460.40 10626.26 109.03 o 2 3 0 2824.17 2724.86 48.04 o 3 3 0 900.24 717.33 23.98 o 4 3 0 3946.52 4000.44 53.28 o 5 3 0 4199.29 4360.22 61.70 o 6 3 0 2398.14 2237.79 77.47 o 7 3 0 2114.08 2012.38 59.39 o 8 3 0 900.27 1007.18 48.17 o 9 3 0 2609.86 2620.98 76.83 o 10 3 0 314.76 318.16 53.15 o 11 3 0 602.03 761.97 71.60 o -13 4 0 909.84 893.50 79.20 o -12 4 0 513.64 659.75 142.21 o -11 4 0 1661.90 1736.32 83.95 o -10 4 0 3650.61 3480.51 111.03 o -9 4 0 3980.66 3963.33 71.82 o -8 4 0 336.89 285.41 23.75 o -7 4 0 4281.27 4406.28 67.65 o -6 4 0 3944.02 3970.93 88.59 o -5 4 0 4494.67 4242.15 55.83 o -4 4 0 8395.05 8573.67 83.48 o -3 4 0 10718.39 10842.76 101.82 o -2 4 0 3528.51 3427.21 45.21 o -1 4 0 11469.40 11778.15 104.10 o 0 4 0 7845.07 8164.61 103.06 o 1 4 0 2453.57 2412.03 45.23 o 2 4 0 7869.64 8175.44 144.57 o 3 4 0 6287.77 5781.53 121.84 o 4 4 0 5119.99 4804.15 81.22 o 5 4 0 3939.11 4190.08 87.14 o 6 4 0 4349.76 4207.73 85.25 o 7 4 0 5878.96 5902.51 108.75 o 8 4 0 3531.46 3630.60 114.62 o 9 4 0 2197.15 2218.02 73.32 o 10 4 0 2079.64 2071.61 97.54 o -13 5 0 428.39 446.41 64.45 o -12 5 0 12.15 37.26 43.04 o -11 5 0 288.38 337.79 51.22 o -10 5 0 446.07 548.71 91.11 o -9 5 0 356.61 342.25 31.45 o -8 5 0 22.31 -2.90 18.07 o -7 5 0 736.18 666.37 36.35 o -6 5 0 1785.90 1912.49 38.68 o -5 5 0 198.35 128.76 12.66 o -4 5 0 2159.69 2110.06 47.83 o -3 5 0 1349.84 1316.78 50.07 o -2 5 0 10423.01 10978.21 104.54 o -1 5 0 833.17 722.51 28.52 o 0 5 0 284.30 227.08 19.05 o 1 5 0 84.11 31.67 11.76 o 2 5 0 1391.24 1371.94 38.88 o 3 5 0 1239.54 1163.26 38.81 o 4 5 0 2999.97 2838.55 78.52 o 5 5 0 5223.40 5193.75 94.32 o 6 5 0 7165.73 7418.29 121.74 o 7 5 0 1222.18 1139.03 68.82 o 8 5 0 882.94 865.31 51.54 o 9 5 0 503.02 586.06 64.23 o 10 5 0 635.69 520.05 61.64 o -13 6 0 63.17 71.17 46.44 o -12 6 0 330.01 491.56 64.69 o -11 6 0 84.80 95.22 40.31 o -10 6 0 463.56 477.46 40.82 o -9 6 0 4.82 -6.90 20.43 o -8 6 0 58.09 43.51 20.95 o -7 6 0 219.29 196.90 22.65 o -6 6 0 491.43 498.83 34.70 o -5 6 0 2726.78 2584.94 58.47 o -4 6 0 224.48 180.29 27.55 o -3 6 0 3234.47 3580.78 53.53 o -2 6 0 3.14 6.18 12.87 o -1 6 0 4.71 -9.32 10.45 o 0 6 0 561.09 588.94 27.17 o 1 6 0 21.55 14.64 12.17 o 2 6 0 98.83 88.47 17.08 o 3 6 0 36.91 53.76 16.99 o 4 6 0 500.27 463.86 33.57 o 5 6 0 1639.92 1685.08 74.85 o 6 6 0 5.24 -6.15 20.07 o 7 6 0 45.22 41.03 24.76 o 8 6 0 8.23 -31.22 26.61 o 9 6 0 4.43 -21.48 31.42 o -12 7 0 810.68 1013.52 81.93 o -11 7 0 1017.68 1053.12 82.07 o -10 7 0 837.04 1003.75 71.46 o -9 7 0 2148.38 2236.74 89.55 o -8 7 0 3155.63 2955.51 75.36 o -7 7 0 2432.06 2452.12 63.60 o -6 7 0 4834.64 4608.97 135.23 o -5 7 0 2441.77 2330.83 88.50 o -4 7 0 4040.90 4058.40 77.19 o -3 7 0 843.44 774.78 37.51 o -2 7 0 527.85 349.00 27.68 o -1 7 0 930.60 935.12 31.21 o 0 7 0 3399.50 3173.33 54.00 o 1 7 0 2789.05 2655.43 69.06 o 2 7 0 1094.08 1217.81 44.07 o 3 7 0 1359.86 1218.19 44.89 o 4 7 0 2605.95 2585.67 67.64 o 5 7 0 5036.53 4973.96 100.03 o 6 7 0 3274.93 3070.35 151.16 o 7 7 0 387.86 365.84 39.20 o 8 7 0 677.20 776.01 67.10 o -12 8 0 723.54 767.79 78.34 o -11 8 0 858.46 881.03 75.46 o -10 8 0 307.85 320.04 66.54 o -9 8 0 2057.07 1826.87 64.66 o -8 8 0 5354.98 5204.38 120.29 o -7 8 0 1779.39 1611.75 55.26 o -6 8 0 2110.92 2160.47 79.30 o -5 8 0 2589.64 2448.88 63.64 o -4 8 0 2612.69 2627.76 64.32 o -3 8 0 3840.62 4073.16 127.53 o -2 8 0 1714.06 1632.36 43.23 o -1 8 0 2923.13 3154.12 59.00 o 0 8 0 3347.91 3398.59 93.05 o 1 8 0 3181.62 3171.39 78.89 o 2 8 0 1796.09 1816.16 71.42 o 3 8 0 2104.88 1926.88 59.00 o 4 8 0 1077.56 1079.29 49.32 o 5 8 0 1784.77 1800.95 75.88 o 6 8 0 1052.35 959.11 95.24 o 7 8 0 1449.44 1436.72 65.70 o -12 9 0 22.01 -60.80 48.07 o -11 9 0 700.39 767.88 142.78 o -10 9 0 0.68 -12.24 30.03 o -9 9 0 160.93 260.25 34.91 o -8 9 0 9.53 -4.18 21.66 o -7 9 0 194.24 202.52 28.68 o -6 9 0 651.09 780.22 44.56 o -5 9 0 604.69 606.58 42.99 o -4 9 0 169.38 161.75 30.15 o -3 9 0 250.16 163.20 25.87 o -2 9 0 318.82 281.86 28.68 o -1 9 0 45.75 72.88 25.46 o 0 9 0 3226.82 3068.97 79.60 o 1 9 0 1193.11 1217.00 72.06 o 2 9 0 288.19 256.75 35.13 o 3 9 0 181.90 162.25 26.27 o 4 9 0 4.29 -6.02 22.62 o 5 9 0 421.58 470.55 42.80 o 6 9 0 460.29 525.82 80.12 o -11 10 0 2.81 65.09 49.41 o -10 10 0 125.24 123.75 36.32 o -9 10 0 49.24 11.23 25.11 o -8 10 0 28.20 59.00 26.07 o -7 10 0 823.62 723.74 47.24 o -6 10 0 452.91 334.61 41.33 o -5 10 0 2.27 -15.24 20.48 o -4 10 0 57.23 23.93 22.50 o -3 10 0 340.59 343.27 33.87 o -2 10 0 28.21 47.39 26.23 o -1 10 0 1638.39 1798.18 80.08 o 0 10 0 344.90 354.56 41.30 o 1 10 0 38.55 -20.41 23.81 o 2 10 0 14.53 -21.28 27.84 o 3 10 0 7.82 4.87 30.27 o 4 10 0 2.66 -6.85 23.09 o 5 10 0 74.24 70.46 26.91 o -11 11 0 990.12 1309.05 116.86 o -10 11 0 700.18 674.55 69.58 o -9 11 0 539.24 549.10 46.71 o -8 11 0 560.61 563.01 46.03 o -7 11 0 779.72 838.50 52.06 o -6 11 0 1597.93 1552.46 61.57 o -5 11 0 946.68 1125.16 57.19 o -4 11 0 2891.74 2780.17 132.61 o -3 11 0 2570.63 2468.58 95.51 o -2 11 0 2112.96 2424.00 94.57 o -1 11 0 1644.36 1611.46 79.94 o 0 11 0 742.10 774.34 63.76 o 1 11 0 886.37 1137.68 77.57 o 2 11 0 788.87 825.30 57.90 o 3 11 0 1419.91 1466.18 155.22 o 4 11 0 881.30 991.60 69.27 o -10 12 0 978.85 1052.91 90.73 o -9 12 0 795.88 874.71 72.41 o -8 12 0 251.79 227.89 66.82 o -7 12 0 256.89 320.54 41.65 o -6 12 0 1236.21 1343.15 64.24 o -5 12 0 817.14 969.12 70.55 o -4 12 0 443.58 398.69 50.61 o -3 12 0 408.17 443.59 54.28 o -2 12 0 1800.92 1561.24 146.53 o -1 12 0 1320.09 1225.55 111.62 o 0 12 0 1134.94 1202.78 105.26 o 1 12 0 771.16 820.72 71.61 o 2 12 0 1004.34 978.21 79.56 o -8 13 0 35.93 41.66 35.03 o -7 13 0 30.97 64.43 34.02 o -6 13 0 41.21 25.84 38.97 o -5 13 0 23.29 -23.24 35.76 o -4 13 0 150.81 132.97 45.64 o -3 13 0 116.16 94.62 68.54 o -2 13 0 293.25 290.67 61.87 o -1 13 0 47.03 22.00 41.93 o 0 13 0 31.42 9.62 66.68 o -5 14 0 94.26 73.61 51.81 o -4 14 0 114.72 200.17 54.34 o -3 14 0 53.07 82.77 47.72 o 3 -14 1 547.14 606.71 69.51 o 4 -14 1 238.49 264.74 73.70 o 5 -14 1 434.29 470.73 65.49 o -1 -13 1 386.04 278.13 73.15 o 0 -13 1 476.82 532.77 76.53 o 1 -13 1 770.54 876.39 77.24 o 2 -13 1 1076.66 1067.10 81.94 o 3 -13 1 883.45 1001.63 75.58 o 4 -13 1 767.42 882.48 86.18 o 5 -13 1 637.77 677.04 67.23 o 6 -13 1 567.64 508.59 60.22 o 7 -13 1 1286.77 1235.33 92.10 o 8 -13 1 625.34 650.75 108.69 o -3 -12 1 95.29 42.99 41.13 o -2 -12 1 299.84 211.99 48.61 o -1 -12 1 42.77 72.82 38.88 o 0 -12 1 15.87 0.22 38.05 o 1 -12 1 116.39 68.21 79.22 o 2 -12 1 567.38 529.03 55.81 o 3 -12 1 457.49 441.13 56.32 o 4 -12 1 702.66 606.86 58.59 o 5 -12 1 732.14 704.94 62.37 o 6 -12 1 1650.44 1592.05 67.09 o 7 -12 1 1113.42 1198.56 63.97 o 8 -12 1 187.80 241.97 38.06 o 9 -12 1 19.35 50.64 42.65 o 10 -12 1 54.33 41.88 61.47 o -4 -11 1 567.16 653.15 86.84 o -3 -11 1 464.55 436.13 49.54 o -2 -11 1 596.97 571.82 53.05 o -1 -11 1 285.43 234.19 43.69 o 0 -11 1 25.90 64.16 37.10 o 1 -11 1 223.50 175.97 41.22 o 2 -11 1 113.87 127.96 37.69 o 3 -11 1 399.48 442.72 110.50 o 4 -11 1 37.73 67.95 28.09 o 5 -11 1 108.83 85.70 28.31 o 6 -11 1 6.73 -12.92 24.03 o 7 -11 1 2.31 16.08 24.66 o 8 -11 1 11.95 -18.05 25.37 o 9 -11 1 68.00 72.74 45.22 o 10 -11 1 297.31 226.75 51.52 o -6 -10 1 1721.37 1559.79 66.82 o -5 -10 1 1406.17 1537.57 66.20 o -4 -10 1 1438.95 1516.09 73.24 o -3 -10 1 1051.47 1054.00 62.80 o -2 -10 1 672.20 639.30 50.87 o -1 -10 1 2857.44 2925.15 84.97 o 0 -10 1 3623.12 3580.02 92.55 o 1 -10 1 1420.88 1358.88 69.78 o 2 -10 1 2807.24 2615.57 91.29 o 3 -10 1 1368.56 1244.94 85.89 o 4 -10 1 3174.21 3101.93 78.30 o 5 -10 1 2289.43 2177.57 119.58 o 6 -10 1 1392.08 1353.78 59.04 o 7 -10 1 664.92 647.59 75.02 o 8 -10 1 756.38 821.10 64.78 o 9 -10 1 227.64 217.86 47.51 o 10 -10 1 570.02 643.23 102.51 o 11 -10 1 803.42 871.80 149.83 o -7 -9 1 1135.10 1061.28 60.93 o -6 -9 1 795.42 819.50 51.42 o -5 -9 1 1139.86 1099.19 80.88 o -4 -9 1 1071.22 1127.54 60.87 o -3 -9 1 1667.07 1826.92 68.80 o -2 -9 1 1048.66 1073.06 98.11 o -1 -9 1 751.70 730.75 48.17 o 0 -9 1 8100.77 7938.62 134.29 o 1 -9 1 1099.04 1066.43 50.42 o 2 -9 1 1562.63 1490.61 50.68 o 3 -9 1 1539.64 1624.98 54.08 o 4 -9 1 3685.01 3607.85 80.69 o 5 -9 1 4212.58 4389.74 90.53 o 6 -9 1 1906.14 1842.28 60.23 o 7 -9 1 3648.20 3340.84 81.39 o 8 -9 1 1069.51 1313.93 54.18 o 9 -9 1 1112.07 1165.96 80.65 o 10 -9 1 622.17 725.93 70.27 o 11 -9 1 1997.85 2073.39 105.77 o 12 -9 1 1428.59 1384.75 115.80 o -8 -8 1 24.62 56.47 31.96 o -7 -8 1 37.49 11.71 26.15 o -6 -8 1 70.20 94.63 25.71 o -5 -8 1 287.25 221.80 33.53 o -4 -8 1 221.20 226.52 29.64 o -3 -8 1 630.64 645.32 37.59 o -2 -8 1 821.75 791.24 46.58 o -1 -8 1 264.55 210.85 27.74 o 0 -8 1 300.58 330.66 39.86 o 1 -8 1 532.03 490.49 59.28 o 2 -8 1 73.71 55.08 19.33 o 3 -8 1 26.01 19.80 16.76 o 4 -8 1 40.62 14.10 16.20 o 5 -8 1 245.00 227.99 37.48 o 6 -8 1 511.50 452.99 32.79 o 7 -8 1 51.65 34.13 21.63 o 8 -8 1 277.24 260.76 50.07 o 9 -8 1 1077.68 1095.25 55.93 o 10 -8 1 164.52 135.64 40.42 o 11 -8 1 892.68 825.51 78.31 o 12 -8 1 462.47 496.57 90.45 o -9 -7 1 216.01 228.97 39.37 o -8 -7 1 345.79 436.18 50.60 o -7 -7 1 444.83 420.64 40.23 o -6 -7 1 1714.80 1562.81 57.95 o -5 -7 1 2175.70 2115.51 62.98 o -4 -7 1 1232.44 1236.62 47.34 o -3 -7 1 211.68 236.36 38.21 o -2 -7 1 403.55 364.25 27.57 o -1 -7 1 1915.07 2056.32 99.33 o 0 -7 1 2130.09 1870.73 41.85 o 1 -7 1 959.73 1004.40 33.01 o 2 -7 1 1970.19 1906.18 43.31 o 3 -7 1 3810.57 3871.88 61.43 o 4 -7 1 186.19 154.85 19.54 o 5 -7 1 1041.47 1048.71 40.22 o 6 -7 1 51.00 47.41 17.63 o 7 -7 1 989.40 964.25 42.98 o 8 -7 1 1537.98 1582.81 61.47 o 9 -7 1 15.78 28.32 24.15 o 10 -7 1 1.01 -14.01 34.46 o 11 -7 1 39.46 43.89 39.28 o 12 -7 1 1.07 19.52 45.61 o -9 -6 1 868.84 866.11 65.44 o -8 -6 1 521.79 606.18 46.43 o -7 -6 1 1538.23 1579.30 59.53 o -6 -6 1 2692.06 2859.51 74.63 o -5 -6 1 3679.94 3453.97 78.00 o -4 -6 1 2019.15 2102.58 57.26 o -3 -6 1 3028.03 3006.00 64.36 o -2 -6 1 3009.32 2887.02 60.53 o -1 -6 1 2856.64 2765.79 44.89 o 0 -6 1 3905.55 3621.21 55.04 o 1 -6 1 11565.29 11629.17 116.23 o 2 -6 1 9005.41 9150.81 98.56 o 3 -6 1 1910.56 1737.88 53.99 o 4 -6 1 2979.63 2844.27 45.93 o 5 -6 1 4986.10 4797.02 81.52 o 6 -6 1 4561.27 4389.46 116.46 o 7 -6 1 2942.53 2904.27 66.51 o 8 -6 1 1966.87 1933.36 59.52 o 9 -6 1 832.38 869.99 51.62 o 10 -6 1 229.72 211.62 41.83 o 11 -6 1 1126.51 1172.37 82.34 o 12 -6 1 635.79 615.88 71.19 o -10 -5 1 981.53 1101.53 72.60 o -9 -5 1 908.01 1002.57 82.94 o -8 -5 1 665.84 721.67 48.36 o -7 -5 1 2101.90 2093.12 64.67 o -6 -5 1 450.49 479.57 57.95 o -5 -5 1 2046.84 1858.32 54.10 o -4 -5 1 2372.53 2319.59 61.66 o -3 -5 1 5088.04 5137.00 108.87 o -2 -5 1 4545.49 4518.45 72.92 o -1 -5 1 4015.72 3866.47 48.43 o 0 -5 1 8378.33 8659.80 89.17 o 1 -5 1 7712.68 7805.43 83.61 o 2 -5 1 14207.05 14864.82 194.76 o 3 -5 1 9588.13 9195.15 139.42 o 4 -5 1 579.78 510.14 18.99 o 5 -5 1 781.34 683.97 23.26 o 6 -5 1 3245.70 3276.07 52.88 o 7 -5 1 4311.08 4231.93 66.95 o 8 -5 1 4806.21 4708.15 89.03 o 9 -5 1 1534.66 1570.89 54.07 o 10 -5 1 1314.36 1448.58 78.35 o 11 -5 1 1456.69 1532.46 90.95 o 12 -5 1 1570.46 1720.51 94.57 o 13 -5 1 1066.35 1284.48 92.87 o -11 -4 1 1.18 47.32 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