Acta Crystallographica Section C

Crystal Structure Communications

Volume 61, Part 6 (June 2005)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The hydrogen-bonding pattern in 6-methyl-2-pyridone, forming infinite chains. See Nichol & Clegg [Acta Cryst. (2005), C61, o383-o385].

inorganic compounds


 

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Acta Cryst. (2005). C61, i59-i60  [ doi:10.1107/S010827010501111X ]

Barium divanadium(V) tellurite(IV)

J.-Y. Hou, C.-C. Huang, H.-H. Zhang, Q.-Y. Yang, Y.-P. Chen and J.-F. Xu

Synopsis: A new three-dimensional bimetallic tellurite, BaV2TeO8, was synthesized by the hydrothermal reaction of Ba(OH)2, TeO2 and V2O5, and characterized by single-crystal X-ray diffraction. The three-dimensional framework is built up from anionic [V2TeO8]n2n- layers parallel to (101) and connected via Ba-O bonds. The anionic layers are formed by three types of polyhedra, namely VO5 tetragonal pyramids, VO4 tetrahedra and TeO4+2 `folded square' polyhedra.

Formula: BaV2TeO8

Online 13 May 2005


 

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Acta Cryst. (2005). C61, i61-i62  [ doi:10.1107/S0108270105010759 ]

Cerium triiodate, Ce(IO3)3

X.-A. Chen, L. Zhang, X.-A. Chang, H.-G. Zang and W.-Q. Xiao

Synopsis: The structure of Ce(IO3)3 consists of chains of edge-sharing CeO9 polyhedra, which are linked into layers by IO3- groups. The layers are held together via long I...O contacts, resulting in a three-dimensional network.

Formula: Ce(IO3)3

Online 13 May 2005


 

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Acta Cryst. (2005). C61, i63-i64  [ doi:10.1107/S0108270105012552 ]

Dilead(II) trimercury(II) tetraoxide chromate(VI), Pb2(Hg3O4)(CrO4)

W. Klein, J. Curda and M. Jansen

Synopsis: Pb2(Hg3O4)(CrO4) consists of isolated CrO42- tetrahedra and Hg3O42- zigzag chains connected by interstitial Pb atoms. The Hg atoms are linearly coordinated by O atoms; the divalent lead ions are coordinated by three close and five more distant neighbours.

Formula: Pb2(Hg3O4)(CrO4)

Online 13 May 2005


 

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Acta Cryst. (2005). C61, i65-i66  [ doi:10.1107/S0108270105010504 ]

Rubidium gadolinium bis(tungstate)

K.-P. Wang, W.-T. Yu, J.-X. Zhang, J.-Y. Wang, H.-J. Zhang and X.-P. Wang

Synopsis: The structure of rubidium gadolinium bis(tungstate), RbGd(WO4)2, has been determined. The crystal is built up from corner- and edge-sharing WO6 octahedral and GdO8 polyhedral groups, giving rise to a Gd-WO4 polyhedral backbone surrounding structural cavities filled with Rb+ cations. The Gd and Rb atoms lie on twofold axes.

Formula: RbGd(WO4)2

Online 13 May 2005


 

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Acta Cryst. (2005). C61, i67-i68  [ doi:10.1107/S0108270105013181 ]

Hexalithium hexadecahydrate decavanadate, [Li6(H2O)16V10O28]n

A.-L. Xie and C.-A. Ma

Synopsis: The novel title compound, poly[octa-[mu]-aqua-octaaqua-[mu]-decavanadato-hexalithium], contains [V10O28]6- polyanions with 2/m symmetry linked by centrosymmetric [Li6(H2O)16]6+ cation chains to form a two-dimensional network structure.

Formula: Li6(H2O)16V10O28

Online 31 May 2005


metal-organic compounds


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Acta Cryst. (2005). C61, m253-m255  [ doi:10.1107/S0108270105012291 ]

A 1:1 adduct of DL-threonine and arsenic acid

H. S. Wilkinson and W. T. A. Harrison

Formula: C4H9NO3·H3AsO4

Online 13 May 2005


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Acta Cryst. (2005). C61, m256-m258  [ doi:10.1107/S0108270105011078 ]

catena-Poly[[(1,10-phenanthroline-[kappa]2N,N')manganese(II)]-di-[mu]-salicylato-[kappa]4O:O']

J.-R. Su and D.-J. Xu

Formula: [Mn(C7H5O3)2(C12H8N2)]

Online 13 May 2005


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Acta Cryst. (2005). C61, m259-m262  [ doi:10.1107/S0108270105011820 ]

Strontium D-glutamate hexahydrate and strontium di(hydrogen L-glutamate) pentahydrate

S. Christgau, J. Odderhede, K. Stahl and J. E. T. Andersen

Formula: [Sr(C5H7NO4)]·6H2O and [Sr(C5H8NO4)2]·5H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, m263-m265  [ doi:10.1107/S0108270105010498 ]

Tetrakis([mu]2-1,8-naphthyridine)-1:2[kappa]4N:N';3:4[kappa]4N:N'-bis([mu]2-salicylato)-1:4[kappa]2O:O';2:3[kappa]2O:O'-tetrakis(salicylic acid)-1[kappa]O,2[kappa]O,3[kappa]O,4[kappa]O-tetrasilver(I)(4 Ag-Ag)

Y. Wang and N. Okabe

Formula: [Ag4(C7H5O3)2(C8H6N2)4(C7H6O3)4]

Online 13 May 2005


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Acta Cryst. (2005). C61, m266-m268  [ doi:10.1107/S010827010501053X ]

Bis(2,9-dimethyl-1,10-phenanthroline-[kappa]2N,N')copper(I) hydrogen squarate hemihydrate

I. Uçar, A. Bulut and O. Büyükgüngör

Formula: [Cu(C14H12N2)2](C4HO4)·0.5H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, m269-m271  [ doi:10.1107/S0108270105010206 ]

Poly[diaquahexakis(dimethyl sulfoxide-[kappa]O)cerium [([mu]2-hexacosaoxooctamolybdate)sodium]]

L.-J. Chen, C.-Z. Lu, Q.-Z. Zhang and S.-M. Chen

Formula: [Ce(C2H6OS)6(H2O)2][NaMo8O26]

Online 13 May 2005


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Acta Cryst. (2005). C61, m272-m274  [ doi:10.1107/S0108270105011960 ]

Second-sphere coordination in anion binding: cis-diazidobis(ethylenediamine-[kappa]2N,N')cobalt(III) picrate

R. P. Sharma, R. Sharma, R. Bala and A. D. Bond

Formula: [Co(N3)2(C2H8N2)2](C6H2N3O7)

Online 13 May 2005


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Acta Cryst. (2005). C61, m275-m277  [ doi:10.1107/S0108270105009820 ]

A new tricarbonylrhenium(I) compound incorporating the tridentate ligand N,N-bispicolyl-2-ethanolamine

S. R. Banerjee and J. Zubieta

Formula: [Re(C14H17N3O)(CO)3]Br·CH4O

Online 13 May 2005


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Acta Cryst. (2005). C61, m278-m280  [ doi:10.1107/S0108270105010814 ]

Poly[bis(N-methylformamide)tetra-[mu]-thiocyanato-manganese(II)mercury(II)]

X.-Q. Wang, W.-T. Yu, D. Xu, G.-H. Zhang and Y.-L. Geng

Formula: [MnHg(NCS)4(C2H5NO)2]

Online 13 May 2005


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Acta Cryst. (2005). C61, m281-m283  [ doi:10.1107/S0108270105012448 ]

Silver(I) complexes of 2-(2-aminoethyl)pyridine: nitrate and perchlorate salts of bis[[mu]-2-(2-aminoethyl)pyridine-[kappa]2N:N']disilver(I)

M. A. H. Khan, T. K. Prasad and M. V. Rajasekharan

Formula: [Ag2(C7H10N2)2](NO3)2 and [Ag2(C7H10N2)2](ClO4)2

Online 13 May 2005


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Acta Cryst. (2005). C61, m284-m286  [ doi:10.1107/S010827010501142X ]

Bis([mu]-phenyl 2-pyridyl ketone N4,N4-butane-1,4-diylthiosemicarbazonato)bis[chlorocopper(II)]

A. Sreekanth, V. Suni, R. P. John, M. Nethaji and M. R. P. Kurup

Formula: [Cu2(C17H17N4S)2Cl2]

Online 13 May 2005


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Acta Cryst. (2005). C61, m287-m288  [ doi:10.1107/S0108270105013594 ]

Chloro[N,N'-ethylenediiminobis(acetylacetonato)]gallium(III)

J. K. Vohs, D. O. Miller, D. R. Denomme, J. W. Ziller and B. D. Fahlman

Formula: [Ga(C12H18N2O2)Cl]

Online 13 May 2005


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Acta Cryst. (2005). C61, m289-m291  [ doi:10.1107/S0108270105012515 ]

Bis[(acetato-[kappa]2O,O')bis(4,4'-dimethyl-2,2'-bipyridyl-[kappa]2N,N')zinc(II)] trithionate pentahydrate

M. E. Díaz de Vivar, S. Baggio, M. T. Garland and R. Baggio

Formula: [Zn(C2H3O2)(C12H12N2)2]2(S3O6)·5H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, m292-m294  [ doi:10.1107/S0108270105007274 ]

A new chain-like cadmium(II) coordination polymer containing chains of water molecules

X. Lin, Y.-Q. Wang, R. Cao, F. Li and W.-H. Bi

Formula: [Cd(C10H8O4)(C5H6N2)2(H2O)]·2H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, m295-m297  [ doi:10.1107/S0108270105012497 ]

catena-Poly[[[N,N'-bis(salicylidene)propane-1,3-diaminato]cobalt(III)]-[mu]-azido] and catena-poly[[[N,N'-bis(salicylidene)propane-1,3-diaminato]cobalt(III)]-[mu]-thiocyanato]

Z.-L. You

Formula: [Co(C17H16N2O2)(N3)] and [Co(C17H16N2O2)(NCS)]

Online 13 May 2005


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Acta Cryst. (2005). C61, m298-m300  [ doi:10.1107/S0108270105013399 ]

Poly[[[diaquazinc(II)]-bis([mu]2-3-cyano-4-dicyanomethylene-5-oxo-4,5-dihydro-1H-pyrrol-2-olato-[kappa]2N3:N3')] dihydrate]

V. A. Tafeenko and V. V. Chernyshev

Formula: [Zn(C8HN4O2)2(H2O)2]·2H2O

Online 20 May 2005


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Acta Cryst. (2005). C61, m301-m303  [ doi:10.1107/S0108270105014277 ]

B-N bond cleavage by cobalt(II) in acetato(3,5-diphenylpyrazole)[tris(3,5-diphenylpyrazolyl)borato]cobalt(II)

D. J. Harding, H. Adams and T. Tuntulani

Formula: [Co(C45H34BN6)(C2H3O2)(C15H12N2)]

Online 20 May 2005


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Acta Cryst. (2005). C61, m304-m306  [ doi:10.1107/S0108270105010140 ]

Bis(4,4'-bipyridinium) hexacyanoplatinate(IV) bis(4,4'-bipyridine)

J. A. Schlueter, R. J. Funk and U. Geiser

Formula: (C10H9N2)2[Pt(CN)6]·2C10H8N2

Online 20 May 2005


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Acta Cryst. (2005). C61, m307-m310  [ doi:10.1107/S0108270105013375 ]

(2,2'-Biquinoline-[kappa]2N,N')dichloropalladium(II), -copper(II) and -zinc(II)

Y. Muranishi, Y. Wang, M. Odoko and N. Okabe

Formula: [PdCl2(C18H12N2)], [CuCl2(C18H12N2)] and [ZnCl2(C18H12N2)]

Online 20 May 2005


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Acta Cryst. (2005). C61, m311-m312  [ doi:10.1107/S0108270105009881 ]

Bis(thiocarbohydrazide)dithiocyanatoiron(II)

G.-Q. Xiang, W.-D. Wang, M.-L. Hu, Z.-M. Jin and Y.-P. Lü

Formula: [Fe(NCS)2(CH6N4S)2]

Online 20 May 2005


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Acta Cryst. (2005). C61, m313-m314  [ doi:10.1107/S010827010501317X ]

Tris(ethylenediamine)zinc(II) molybdate(VI), [Zn(en)3][MoO4]

G.-H. Han, B.-Z. Lin and Z. Li

Formula: [Zn(C2H8N2)3][MoO4]

Online 20 May 2005


 

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Acta Cryst. (2005). C61, m315-m317  [ doi:10.1107/S0108270105014290 ]

A layered fluorinated gallium phosphate organically templated by propane-1,3-diaminium, an analog of the aluminophosphate MIL-12: Ga2(PO4)F5·C3H12N2

T. Loiseau and G. Ferey

Synopsis: The title oxyfluorinated gallium phosphate exhibits a two-dimensional network intercalated by the diprotonated propane-1,3-diaminium moiety. This compound is isostructural with the aluminophosphate having the MIL-12 structure type.

Formula: (C3H12N2)[Ga2(PO4)F5]

Online 31 May 2005


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Acta Cryst. (2005). C61, m318-m320  [ doi:10.1107/S0108270105014538 ]

Bis{1-n-hexyl-3-methyl-4-[1-(phenylimino)propyl]-1H-pyrazol-5-olato}copper(II): a new copper(II) complex with a chelating alkylpyrazolone-based enamine

F. R. Pérez, J. Belmar, C. Jiménez, Y. Moreno, P. Hermosilla and R. Baggio

Formula: [Cu(C19H26N3O)2]

Online 31 May 2005


organic compounds


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Acta Cryst. (2005). C61, o345-o347  [ doi:10.1107/S0108270105011212 ]

N,N'-Butane-1,4-diylbis(bromoacetamide)

M. Martínez-Palau, L. Urpí, M. Font-Bardia and J. Puiggalí

Formula: C8H14Br2N2O2

Online 13 May 2005


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Acta Cryst. (2005). C61, o348-o350  [ doi:10.1107/S0108270105009844 ]

1,3-Dibenzoylimidazolidine-2-thione and 1,3-dibenzoyl-3,4,5,6-tetrahydropyrimidine-2(1H)-thione

C. Kazak, V. T. Yilmaz, S. Servi, M. Koca and F. W. Heinemann

Formula: C17H14N2O2S and C18H16N2O2S

Online 13 May 2005


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Acta Cryst. (2005). C61, o351-o353  [ doi:10.1107/S0108270105010607 ]

X-ray investigations of bicyclic [alpha]-methylene-[delta]-valerolactones. III. trans-(4aR,8aR)-4a-Methoxy-3-methyleneperhydrochromen-2-one

J. Wojciechowski, H. Krawczyk, M. Sliwinski and W. M. Wolf

Formula: C11H16O3

Online 13 May 2005


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Acta Cryst. (2005). C61, o354-o357  [ doi:10.1107/S0108270105011881 ]

Three structures containing (E)-1,2-bis(benzimidazol-2-yl)ethene groups

R. T. Stibrany, H. J. Schugar and J. A. Potenza

Formula: C18H16N4, C20H20N4 and C20H21N4+·ClO4-

Online 13 May 2005


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Acta Cryst. (2005). C61, o358-o360  [ doi:10.1107/S0108270105011066 ]

(1S*,2S*,4S*,5S*)-Cyclohexane-1,2,4,5-tetrol monohydrate

G. Mehta, S. Sen and S. Dey

Formula: C6H12O4·H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, o361-o362  [ doi:10.1107/S0108270105010280 ]

5,10-dihydroxy-5H,10H-diimidazo[1,2-a:1',2'-d]pyrazine

L. E. Cheruzel, M. S. Mashuta and R. M. Buchanan

Formula: C8H8N4O2

Online 13 May 2005


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Acta Cryst. (2005). C61, o363-o365  [ doi:10.1107/S0108270105008449 ]

4,4'-Butane-1,4-diylbis[3-ethyl-1H-1,2,4-triazol-5(4H)-one] and 4-hydroxy-3-n-propyl-1H-1,2,4-triazol-5(4H)-one

N. Ocak Ískeleli, S. Isik, K. Sancak, S. Sasmaz, Y. Ünver and M. Er

Formula: C12H20N6O2 and C5H9N3O2

Online 13 May 2005


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Acta Cryst. (2005). C61, o366-o368  [ doi:10.1107/S0108270105009200 ]

Ammonium 3-cyano-4-(dicyanomethylene)-5-oxo-4,5-dihydro-1H-pyrrol-2-olate monohydrate

V. A. Tafeenko, R. Peschar, Y. S. Kajukov, K. N. Kornilov and L. A. Aslanov

Formula: NH4+·C8HN4O2-·H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, o369-o372  [ doi:10.1107/S0108270105010218 ]

The (1RS,2RS,7RS,8RS)- and (1RS,2SR,7SR,8RS)-diastereoisomers of 8,9,11,12-tetrachloro-N-ethyltricyclo[6.2.2.02,7]dodeca-9,11-diene-1,10-dicarboximide

F. M. Grimley, C. O'Donnell, A. C. Pratt, C. Long and R. A. Howie

Formula: Two isomers of C16H15Cl4NO2

Online 13 May 2005


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Acta Cryst. (2005). C61, o373-o376  [ doi:10.1107/S0108270105010887 ]

Polar hydrogen-bonded organic chains in 4,4'-bipyrazolium bromide and perchlorate monohydrates

K. V. Domasevitch and I. Boldog

Formula: C6H7N4+·Br-·H2O and C6H7N4+·ClO4-·H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, o377-o379  [ doi:10.1107/S0108270105009832 ]

Azinyl sulfides. LXXXI. 14-Phenyl-7-thiapyrano[2,3-c;6,5-c']diquinoline-14-carbonitrile

C. Besnard, C. Kloc, T. Siegrist, C. Svensson and K. Pluta

Formula: C26H15N3S

Online 13 May 2005


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Acta Cryst. (2005). C61, o380-o382  [ doi:10.1107/S010827010501245X ]

The perchlorate salt of the novel diprotonated dinucleating ligand 1,3-bis{[2-(2-pyridinio)ethyl][2-(2-pyridyl)ethyl]amino}benzene

G. Sutha Siluvai, B. Varghese and N. N. Murthy

Formula: C34H38N62+·2ClO4-·2H2O

Online 13 May 2005


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Acta Cryst. (2005). C61, o383-o385  [ doi:10.1107/S0108270105012485 ]

6-Methyl-2-pyridone: an elusive structure finally solved

G. S. Nichol and W. Clegg

Formula: C6H7NO

Online 13 May 2005


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Acta Cryst. (2005). C61, o386-o389  [ doi:10.1107/S0108270105013661 ]

2',4'-Dihydroxy-3-methoxy-[alpha],[beta]-dihydrochalcone and 2',4-dihydroxy-[alpha],[beta]-dihydrochalcone: supramolecular structures formed by O-H...O, C-H...O and stacking interactions

J. Marek, K. Lunerová, J. Tousek, V. Suchý and R. Marek

Formula: C16H16O4 and C15H14O3

Online 20 May 2005


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Acta Cryst. (2005). C61, o390-o392  [ doi:10.1107/S0108270105007833 ]

Two new chiral nucleoside analogues: (4R,5R)-4-(4,6-dimethylpyrimidin-2-ylsulfanyl)-5-[(2S,5R)-2-isopropyl-5-methylcyclohexyloxy]-2,3,4,5-tetrahydrofuran-2-one and (4R,5R)-5-[(2S,5R)-isopropyl-5-methylcyclohexyloxy]-4-(4-methyl-1,3-thiazol-2-ylamino)-2,3,4,5-tetrahydrofuran-2-one

L. He, Y.-M. Liu, W. Zhang and Q.-H. Chen

Formula: C20H30N2O3S and C18H28N2O3S

Online 20 May 2005


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Acta Cryst. (2005). C61, o393-o395  [ doi:10.1107/S0108270105005251 ]

3,4-Bis[(4-methoxybenzoyl)methylsulfanyl]thiophene

S. Özbey, F. B. Kaynak, E. Ertas and T. Ozturk

Formula: C22H20O4S3

Online 20 May 2005


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Acta Cryst. (2005). C61, o396-o397  [ doi:10.1107/S010827010501022X ]

N,N:N',N'-Bis(2,2'-dihydroxybiphenyl-3,3'-dimethylidene)benzene-1,2-diamine dimethyl sulfoxide tetrasolvate

P. Plitt, F. Rominger and R. Krämer

Formula: C40H28N4O4·4C2H6OS

Online 20 May 2005


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Acta Cryst. (2005). C61, o398-o403  [ doi:10.1107/S0108270105013260 ]

Two isomeric pairs of dihydrobenzopyrazoloquinazolines: centrosymmetric dimers, chains and sheets built from C-H...N and C-H...[pi](arene) hydrogen bonds and [pi]-[pi] stacking interactions

J. Portilla, J. Quiroga, J. Cobo, M. Nogueras, J. N. Low and C. Glidewell

Formula: C21H17N3 and C22H19N3

Online 20 May 2005


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Acta Cryst. (2005). C61, o404-o407  [ doi:10.1107/S010827010501379X ]

1-Benzyl-4-(4-nitrophenyl)-2,3-dihydro-1H-1,5-benzodiazepine: a three-dimensional framework structure generated by two C-H...O hydrogen bonds and one C-H...[pi](arene) hydrogen bond

H. Torres, B. Insuasty, J. Cobo, J. N. Low and C. Glidewell

Formula: C22H19N3O2

Online 20 May 2005


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Acta Cryst. (2005). C61, o408-o410  [ doi:10.1107/S0108270105014265 ]

2'-Deoxy-5-fluorotubercidin

F. Seela, K. Xu and H. Eickmeier

Formula: C11H13FN4O3

Online 20 May 2005


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Acta Cryst. (2005). C61, o411-o413  [ doi:10.1107/S010827010501437X ]

1[lambda]4,4[lambda]4,8[lambda]4,11[lambda]4-Tetrathiacyclotetradecane-1,4,7,10-tetraylidenetetraaminium tetrakis(2,4,6-trimethylbenzenesulfonate)

S. H. Dale, M. R. J. Elsegood, L. M. Gilby, K. E. Holmes and P. F. Kelly

Formula: C10H28N4S44+·4C9H11O3S-

Online 31 May 2005


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Acta Cryst. (2005). C61, o414-o416  [ doi:10.1107/S0108270105014435 ]

Hydrogen-bonded chains in 3-(5-chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)-1-(4-methoxyphenyl)propenone and 3-(5-chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)-1-(3,4,5-trimethoxyphenyl)propenone

J. Trilleras, J. Quiroga, J. Cobo, J. N. Low and C. Glidewell

Formula: C20H17ClN2O2 and C22H21ClN2O4

Online 31 May 2005


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