# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' pmnhno3 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1330.91 _exptl_crystal_F_000 3103.27 _reflns_d_resolution_high 0.8090 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 32.7000 _cell_length_b 12.9260 _cell_length_c 16.0650 _cell_angle_alpha 90.000 _cell_angle_beta 104.730 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 102825.05 38855.93 1124.26 o 8 0 0 128158.76 136429.09 1152.20 o 10 0 0 10672.70 11681.09 186.47 o 12 0 0 15107.77 15354.28 337.67 o 14 0 0 1222.19 1787.61 82.82 o 16 0 0 66.39 178.43 61.49 o 18 0 0 64.65 98.93 58.01 o 20 0 0 3123.22 3173.97 129.41 o 22 0 0 167.98 240.84 83.87 o 24 0 0 18392.41 19258.75 464.66 o 26 0 0 75.31 185.69 105.61 o 28 0 0 1787.12 1801.03 231.45 o 30 0 0 1855.73 2032.18 290.94 o 32 0 0 3137.40 3833.39 521.69 o 34 0 0 705.05 697.85 379.84 o 36 0 0 92.19 189.60 313.45 o 38 0 0 1259.01 1931.51 750.76 o 5 1 0 1.01 24.42 14.14 o 7 1 0 21636.75 21416.74 422.92 o 9 1 0 25698.63 27984.09 185.88 o 11 1 0 2899.99 2763.37 54.92 o 13 1 0 19947.01 21864.73 164.28 o 15 1 0 0.79 78.64 32.21 o 17 1 0 962.16 980.87 48.11 o 19 1 0 4807.50 5391.31 88.89 o 21 1 0 1214.59 1409.35 103.80 o 23 1 0 77.95 84.23 58.36 o 25 1 0 4556.27 4639.94 180.83 o 27 1 0 40.48 79.08 72.13 o 29 1 0 0.59 63.66 82.22 o 31 1 0 2163.86 2335.21 282.90 o 33 1 0 201.84 136.82 113.23 o 35 1 0 169.10 277.43 247.07 o 37 1 0 23.26 334.58 287.38 o 39 1 0 2.75 336.00 296.80 o 0 2 0 2481.64 11.23 18.84 o 2 2 0 1318.63 17.19 15.24 o 4 2 0 76.82 232.23 51.96 o 6 2 0 598.20 676.96 34.69 o 8 2 0 6129.52 6389.87 96.43 o 10 2 0 6551.47 6699.77 87.11 o 12 2 0 874.51 1061.89 54.48 o 14 2 0 325.75 347.46 45.76 o 16 2 0 52.91 92.76 30.18 o 18 2 0 434.87 557.56 50.44 o 20 2 0 24.13 126.39 44.60 o 22 2 0 416.09 478.84 118.66 o 24 2 0 64.33 107.24 72.22 o 26 2 0 17.47 46.23 69.40 o 28 2 0 12.28 98.38 83.88 o 30 2 0 29.53 86.87 117.34 o 32 2 0 94.10 184.19 146.44 o 34 2 0 0.63 93.14 116.21 o 36 2 0 2.71 169.29 157.42 o 38 2 0 15.46 213.60 290.09 o 1 3 0 6.26 41.20 20.17 o 3 3 0 317.94 255.57 28.02 o 5 3 0 21711.50 22990.54 251.90 o 7 3 0 1531.25 1493.80 50.41 o 9 3 0 21055.93 22246.27 249.33 o 11 3 0 44.88 44.75 28.65 o 13 3 0 7196.53 7875.58 106.46 o 15 3 0 1.64 38.86 30.54 o 17 3 0 3172.48 3237.57 93.14 o 19 3 0 2900.60 3051.89 96.96 o 21 3 0 272.36 298.64 71.95 o 23 3 0 1047.90 1063.01 116.10 o 25 3 0 4268.33 4457.44 179.19 o 27 3 0 1416.79 1510.15 173.29 o 29 3 0 815.17 814.65 158.55 o 31 3 0 1317.90 1180.85 212.58 o 33 3 0 0.25 114.50 160.57 o 35 3 0 4.69 139.70 168.55 o 37 3 0 21.41 145.17 228.65 o 0 4 0 1771325.38 1681623.25 18450.95 o 2 4 0 428303.47 439242.53 4766.14 o 4 4 0 233.72 111.02 55.52 o 6 4 0 250975.80 270331.44 937.57 o 8 4 0 9373.55 9641.02 369.67 o 10 4 0 233.03 258.10 60.90 o 12 4 0 3.81 88.38 44.05 o 14 4 0 496.86 561.29 63.53 o 16 4 0 18.97 77.54 43.44 o 18 4 0 1293.07 1393.01 84.50 o 20 4 0 6640.98 6509.13 136.45 o 22 4 0 608.75 576.81 94.10 o 24 4 0 16676.57 18416.43 313.51 o 26 4 0 61.40 180.50 86.76 o 28 4 0 780.14 629.86 136.70 o 30 4 0 1400.48 1496.03 280.42 o 32 4 0 2432.47 2885.63 357.12 o 34 4 0 38.84 148.08 212.33 o 36 4 0 54.98 173.39 221.62 o 1 5 0 14668.60 14775.93 120.77 o 3 5 0 1105.31 1084.04 61.17 o 5 5 0 7872.41 8674.63 128.66 o 7 5 0 5054.38 5683.42 87.83 o 9 5 0 3298.08 3113.39 69.28 o 11 5 0 2496.26 3123.91 72.33 o 13 5 0 1782.76 1749.56 83.37 o 15 5 0 296.53 303.15 67.49 o 17 5 0 3.39 64.85 41.87 o 19 5 0 252.00 302.07 62.90 o 21 5 0 583.53 584.98 90.38 o 23 5 0 1790.16 1927.98 139.24 o 25 5 0 5194.99 5027.53 203.12 o 27 5 0 9.22 132.90 99.80 o 29 5 0 110.60 191.78 138.43 o 31 5 0 247.65 241.83 211.66 o 33 5 0 813.78 832.30 297.08 o 35 5 0 230.40 220.93 206.35 o 37 5 0 11.87 74.67 182.06 o 0 6 0 61.46 92.29 48.16 o 2 6 0 1354.99 1275.41 55.28 o 4 6 0 3245.06 2871.16 81.29 o 6 6 0 53.76 107.87 41.28 o 8 6 0 4146.62 4604.35 88.36 o 10 6 0 2239.41 2113.47 68.03 o 12 6 0 352.15 253.46 71.34 o 14 6 0 873.01 777.31 89.87 o 16 6 0 0.90 77.36 48.81 o 18 6 0 167.99 188.27 75.88 o 20 6 0 245.05 289.63 93.58 o 22 6 0 19.26 60.59 74.26 o 24 6 0 55.16 96.78 74.16 o 26 6 0 100.07 154.57 102.53 o 28 6 0 300.79 201.60 106.66 o 30 6 0 4.66 133.29 126.93 o 32 6 0 1.24 132.92 190.77 o 34 6 0 29.64 115.43 206.52 o 36 6 0 106.70 159.20 193.40 o 1 7 0 448.97 356.02 50.78 o 3 7 0 5.81 41.52 25.59 o 5 7 0 10541.52 11297.58 145.15 o 7 7 0 1480.47 1891.80 81.18 o 9 7 0 888.69 787.47 90.55 o 11 7 0 535.19 771.86 100.70 o 13 7 0 1041.44 1003.42 105.19 o 15 7 0 107.72 91.37 53.03 o 17 7 0 704.83 687.91 98.66 o 19 7 0 454.98 579.80 115.37 o 21 7 0 465.72 386.21 86.20 o 23 7 0 239.00 218.38 113.05 o 25 7 0 3136.97 3152.00 194.81 o 27 7 0 325.14 213.03 108.79 o 29 7 0 164.71 185.44 142.02 o 31 7 0 567.19 605.45 199.78 o 33 7 0 39.15 266.72 217.02 o 35 7 0 23.56 160.24 216.66 o 0 8 0 296167.13 316962.78 3984.85 o 2 8 0 47707.78 50475.27 407.47 o 4 8 0 827.38 1189.14 86.02 o 6 8 0 21891.36 23901.44 319.60 o 8 8 0 3255.66 2915.93 136.08 o 10 8 0 98.74 104.76 63.55 o 12 8 0 190.37 209.79 74.41 o 14 8 0 278.60 398.73 87.99 o 16 8 0 195.14 133.86 68.69 o 18 8 0 18.23 133.76 81.73 o 20 8 0 441.74 353.59 103.58 o 22 8 0 0.12 121.02 88.60 o 24 8 0 4584.18 4116.70 257.28 o 26 8 0 231.50 235.34 117.67 o 28 8 0 108.35 137.69 127.20 o 30 8 0 457.33 455.85 185.79 o 32 8 0 676.16 693.64 237.15 o 1 9 0 5776.04 5749.01 172.89 o 3 9 0 1750.40 1980.46 105.96 o 5 9 0 136.82 81.10 59.20 o 7 9 0 1822.47 2062.83 121.34 o 9 9 0 3211.00 3395.59 154.21 o 11 9 0 10.15 59.98 58.31 o 13 9 0 24.31 106.88 68.33 o 15 9 0 0.30 101.46 69.14 o 17 9 0 350.04 691.69 133.12 o 19 9 0 7.43 117.96 79.87 o 21 9 0 103.90 146.80 98.89 o 23 9 0 116.77 177.25 116.92 o 25 9 0 392.29 337.75 126.82 o 27 9 0 539.23 431.81 150.60 o 29 9 0 252.36 231.35 174.18 o 31 9 0 225.55 206.35 196.52 o 0 10 0 2679.38 3147.40 205.09 o 2 10 0 1376.08 1190.84 172.09 o 4 10 0 100.80 227.17 117.13 o 6 10 0 1640.46 1229.87 146.52 o 8 10 0 113.69 175.52 73.61 o 10 10 0 695.83 920.52 120.48 o 12 10 0 484.64 548.25 109.75 o 14 10 0 727.38 978.58 156.41 o 16 10 0 12.73 95.58 74.39 o 18 10 0 0.67 88.43 78.17 o 20 10 0 113.07 185.99 89.85 o 22 10 0 22.35 127.54 109.52 o 24 10 0 196.98 244.89 138.68 o 26 10 0 17.63 109.89 113.46 o 28 10 0 356.05 260.39 214.05 o 30 10 0 2.89 164.18 191.84 o 1 11 0 493.00 748.08 156.60 o 3 11 0 643.23 653.09 141.36 o 5 11 0 1.50 81.71 75.26 o 7 11 0 27.82 120.19 91.91 o 9 11 0 175.61 98.71 90.23 o 11 11 0 118.61 201.87 86.40 o 13 11 0 194.50 294.40 112.73 o 15 11 0 24.81 111.56 74.31 o 17 11 0 7.45 87.43 77.65 o 19 11 0 273.59 278.83 107.03 o 21 11 0 828.94 459.10 135.51 o 23 11 0 18.81 182.01 114.82 o 25 11 0 724.68 462.89 147.88 o 27 11 0 437.14 401.98 199.99 o 0 12 0 44770.01 45975.80 1456.05 o 2 12 0 3121.05 3032.00 228.86 o 4 12 0 286.45 226.63 146.29 o 6 12 0 1277.15 1162.35 184.41 o 8 12 0 1424.08 851.30 148.51 o 10 12 0 23.47 132.39 93.39 o 12 12 0 0.03 96.22 85.73 o 14 12 0 0.76 111.11 97.94 o 16 12 0 0.15 141.23 114.29 o 18 12 0 0.77 159.25 100.88 o 20 12 0 2.97 138.64 116.73 o 22 12 0 251.05 158.50 122.66 o 24 12 0 294.30 221.20 143.57 o 1 13 0 797.04 730.71 158.24 o 3 13 0 260.65 354.75 156.41 o 5 13 0 1.28 138.98 133.44 o 7 13 0 489.11 408.52 197.81 o 9 13 0 159.24 188.34 105.83 o 11 13 0 72.87 183.04 109.56 o 13 13 0 5.28 134.35 108.97 o 15 13 0 39.43 129.04 112.45 o 17 13 0 157.03 256.21 130.21 o 19 13 0 3.93 126.67 117.05 o 21 13 0 4.27 147.35 139.50 o 0 14 0 204.42 300.49 246.36 o 2 14 0 7.20 46.29 68.44 o 4 14 0 129.07 125.12 152.53 o 6 14 0 0.45 89.23 127.00 o 8 14 0 293.39 273.94 155.01 o 10 14 0 35.24 90.69 134.50 o 12 14 0 59.25 118.84 117.32 o 14 14 0 4.00 156.30 138.05 o 16 14 0 50.25 133.46 136.89 o 18 14 0 24.74 151.82 134.46 o 1 15 0 5.49 261.68 142.45 o 3 15 0 5.29 149.63 134.97 o 5 15 0 114.38 201.12 154.82 o 7 15 0 3.71 160.73 131.16 o 9 15 0 90.43 327.49 189.58 o 11 15 0 106.95 267.88 173.44 o 13 15 0 1.29 165.50 161.85 o -39 1 1 11.24 207.29 242.18 o -37 1 1 4.05 276.52 264.40 o -35 1 1 304.69 218.09 218.62 o -33 1 1 1276.76 1417.55 328.33 o -31 1 1 31.07 114.74 88.17 o -29 1 1 13962.44 14595.66 289.47 o -27 1 1 1411.20 1216.75 150.84 o -25 1 1 4141.42 4432.16 176.78 o -23 1 1 8029.20 8946.70 155.21 o -21 1 1 2.32 79.50 39.82 o -19 1 1 15.00 40.27 26.78 o -17 1 1 12080.61 13867.48 121.20 o -15 1 1 7460.11 8431.03 78.92 o -13 1 1 4523.54 4539.32 66.16 o -11 1 1 2198.29 2188.54 53.34 o -9 1 1 2588.60 2837.22 48.76 o -7 1 1 1303.56 1503.39 33.46 o -5 1 1 5522.67 476.49 102.53 o 3 1 1 3214.57 16.11 10.85 o 5 1 1 967.77 564.02 50.63 o 7 1 1 211.93 166.80 27.58 o 9 1 1 8666.23 8248.26 75.34 o 11 1 1 54915.96 58620.57 465.12 o 13 1 1 1267.96 1415.19 42.74 o 15 1 1 12.45 43.21 21.42 o 17 1 1 3979.76 4020.77 69.50 o 19 1 1 2166.72 2396.45 85.27 o 21 1 1 681.49 637.36 84.28 o 23 1 1 2026.13 2049.72 121.27 o 25 1 1 1091.96 991.86 151.71 o 27 1 1 2873.44 2484.13 166.78 o 29 1 1 3618.81 3522.33 270.78 o 31 1 1 1495.72 1616.44 239.87 o 33 1 1 100.61 147.43 148.41 o 35 1 1 65.03 161.36 219.16 o 37 1 1 36.08 197.57 206.28 o -38 2 1 729.51 720.92 429.49 o -36 2 1 825.51 724.12 237.17 o -34 2 1 14.44 88.35 121.26 o -32 2 1 1993.19 2109.32 251.90 o -30 2 1 4309.62 4262.98 235.85 o -28 2 1 933.77 915.24 166.20 o -26 2 1 847.83 730.83 133.91 o -24 2 1 1452.78 1147.55 106.54 o -22 2 1 3955.93 4377.78 118.85 o -20 2 1 0.27 55.40 34.44 o -18 2 1 6848.72 8034.66 115.63 o -16 2 1 249.43 235.77 51.46 o -14 2 1 4440.32 5152.67 92.10 o -12 2 1 4312.15 4461.53 80.29 o -10 2 1 3438.43 3558.21 69.85 o -8 2 1 11973.53 12881.41 183.15 o -6 2 1 15875.88 16092.49 379.20 o -4 2 1 34000.62 14730.39 2103.75 o -2 2 1 5564.53 35.25 15.28 o 0 2 1 7114.26 24.08 14.77 o 2 2 1 233370.09 4928.22 839.03 o 4 2 1 168995.48 135199.94 10565.76 o 6 2 1 10718.27 10468.65 190.53 o 8 2 1 53071.30 55783.48 775.81 o 10 2 1 35377.01 36619.69 439.18 o 12 2 1 13312.20 13917.96 103.17 o 14 2 1 3594.28 3565.89 77.24 o 16 2 1 13387.13 14551.49 244.65 o 18 2 1 3773.01 3480.12 79.36 o 20 2 1 20670.66 23340.82 247.56 o 22 2 1 1885.98 1804.51 123.70 o 24 2 1 10.75 121.34 75.76 o 26 2 1 23921.39 24670.80 570.77 o 28 2 1 106.16 103.46 116.10 o 30 2 1 47.51 55.35 109.25 o 32 2 1 629.04 650.09 209.62 o 34 2 1 28.34 152.33 161.05 o 36 2 1 8.18 156.82 208.60 o 38 2 1 313.81 238.91 335.47 o -37 3 1 149.34 143.23 228.01 o -35 3 1 188.57 207.62 242.64 o -33 3 1 200.04 260.53 203.47 o -31 3 1 3145.62 3519.40 234.79 o -29 3 1 2103.90 2453.49 207.99 o -27 3 1 2064.13 1829.78 167.94 o -25 3 1 93.06 171.71 70.91 o -23 3 1 12952.23 14249.78 223.74 o -21 3 1 21.49 85.66 50.57 o -19 3 1 1931.76 1828.19 91.52 o -17 3 1 10009.29 11245.97 145.66 o -15 3 1 4267.85 4543.13 95.53 o -13 3 1 51.07 102.55 47.14 o -11 3 1 862.40 981.18 69.43 o -9 3 1 148.97 143.17 39.72 o -7 3 1 4984.96 5615.18 92.09 o -5 3 1 432.03 489.48 37.99 o -3 3 1 1110.74 1191.48 32.81 o -1 3 1 28626.06 28145.03 430.21 o 1 3 1 8395.61 8366.25 96.73 o 3 3 1 315.40 277.09 40.00 o 5 3 1 32371.07 34009.95 268.96 o 7 3 1 19706.27 21719.20 182.78 o 9 3 1 2825.25 2773.66 68.10 o 11 3 1 9186.71 10058.14 140.82 o 13 3 1 7116.20 8012.32 105.73 o 15 3 1 111.23 139.26 38.78 o 17 3 1 3598.04 3920.36 79.04 o 19 3 1 1633.80 1761.13 96.29 o 21 3 1 1129.25 1134.11 114.38 o 23 3 1 956.80 944.75 107.05 o 25 3 1 441.81 483.66 105.41 o 27 3 1 6105.51 5635.48 278.94 o 29 3 1 442.78 293.57 131.44 o 31 3 1 72.80 225.71 146.76 o 33 3 1 175.08 296.72 187.30 o 35 3 1 323.13 487.07 295.35 o 37 3 1 274.92 257.10 204.05 o -38 4 1 9.23 319.23 290.49 o -36 4 1 1.01 54.86 169.79 o -34 4 1 1.78 165.91 197.10 o -32 4 1 591.78 656.18 345.76 o -30 4 1 163.27 207.56 146.34 o -28 4 1 1291.27 1224.47 148.97 o -26 4 1 206.57 318.56 88.48 o -24 4 1 146.80 212.30 81.85 o -22 4 1 1473.80 1399.82 94.00 o -20 4 1 554.17 566.48 76.33 o -18 4 1 68.56 90.27 43.56 o -16 4 1 450.83 505.01 71.20 o -14 4 1 513.13 421.58 61.85 o -12 4 1 244.06 339.00 64.42 o -10 4 1 45.52 57.63 34.29 o -8 4 1 765.63 788.45 58.80 o -6 4 1 854.44 1005.67 63.10 o -4 4 1 4109.23 4421.76 67.19 o -2 4 1 4716.96 4701.92 86.85 o 0 4 1 7294.99 7777.65 229.93 o 2 4 1 4973.50 5402.25 93.00 o 4 4 1 5.29 59.15 35.04 o 6 4 1 66.71 58.51 36.38 o 8 4 1 7501.42 7519.20 97.06 o 10 4 1 2127.85 2244.25 70.43 o 12 4 1 5810.27 6221.56 102.81 o 14 4 1 924.62 867.63 70.29 o 16 4 1 382.13 433.45 66.49 o 18 4 1 1732.17 1464.47 80.30 o 20 4 1 14.21 59.59 50.87 o 22 4 1 4.57 74.85 57.14 o 24 4 1 244.27 265.09 91.18 o 26 4 1 31.96 155.10 101.48 o 28 4 1 25.33 138.29 107.74 o 30 4 1 160.32 217.40 193.80 o 32 4 1 1.98 164.37 215.09 o 34 4 1 52.47 197.42 213.10 o 36 4 1 1.16 244.25 258.21 o -37 5 1 27.49 150.21 225.00 o -35 5 1 6.08 165.53 218.57 o -33 5 1 541.23 384.45 252.53 o -31 5 1 128.45 114.24 125.02 o -29 5 1 5218.34 5605.01 237.35 o -27 5 1 61.94 104.93 99.17 o -25 5 1 2265.74 2559.61 182.08 o -23 5 1 8502.55 9774.18 322.62 o -21 5 1 77.46 118.54 58.82 o -19 5 1 678.87 590.97 93.13 o -17 5 1 2096.82 2456.89 122.26 o -15 5 1 907.14 1073.52 93.11 o -13 5 1 2714.69 2750.99 107.10 o -11 5 1 1052.84 1275.55 88.40 o -9 5 1 2301.76 2759.34 83.72 o -7 5 1 5024.69 5800.39 99.89 o -5 5 1 1822.45 1995.46 47.17 o -3 5 1 20425.90 22011.02 114.95 o -1 5 1 3830.44 3676.43 70.46 o 1 5 1 8129.65 9254.26 110.26 o 3 5 1 13323.89 14119.28 138.92 o 5 5 1 18445.79 19548.08 297.55 o 7 5 1 3729.10 4175.19 87.96 o 9 5 1 9487.54 10238.50 196.16 o 11 5 1 13092.44 14496.71 131.64 o 13 5 1 948.02 1145.36 74.65 o 15 5 1 1647.37 1436.86 83.71 o 17 5 1 4188.40 4062.65 110.98 o 19 5 1 756.15 728.23 81.34 o 21 5 1 770.78 631.90 104.30 o 23 5 1 240.64 186.92 84.44 o 25 5 1 54.50 124.97 87.51 o 27 5 1 1740.55 1800.87 236.83 o 29 5 1 1542.52 1405.05 227.22 o 31 5 1 285.08 344.73 252.02 o 33 5 1 6.78 58.95 160.37 o 35 5 1 129.35 141.62 216.68 o -36 6 1 181.84 152.58 212.80 o -34 6 1 19.80 107.58 203.94 o -32 6 1 1925.37 1960.40 326.46 o -30 6 1 727.27 696.56 140.55 o -28 6 1 1524.03 1492.32 165.75 o -26 6 1 577.48 461.64 139.44 o -24 6 1 3536.52 4255.59 210.33 o -22 6 1 11.36 74.25 61.41 o -20 6 1 649.97 659.58 99.91 o -18 6 1 680.66 738.83 96.29 o -16 6 1 83.92 151.09 76.64 o -14 6 1 103.11 113.23 55.40 o -12 6 1 527.26 524.05 84.12 o -10 6 1 1553.68 1806.54 99.24 o -8 6 1 4013.78 4093.02 107.38 o -6 6 1 8498.02 9097.04 102.84 o -4 6 1 40571.89 44850.98 414.82 o -2 6 1 196.51 97.28 36.93 o 0 6 1 60.24 62.21 33.15 o 2 6 1 7169.28 7601.25 115.77 o 4 6 1 199.74 309.02 52.13 o 6 6 1 747.73 850.65 74.76 o 8 6 1 14275.42 16011.86 201.20 o 10 6 1 19152.74 20236.31 239.55 o 12 6 1 2296.87 1827.21 81.72 o 14 6 1 375.10 338.12 86.51 o 16 6 1 3784.58 3836.90 126.70 o 18 6 1 0.53 101.49 60.85 o 20 6 1 3536.77 4547.69 221.59 o 22 6 1 483.86 469.91 128.86 o 24 6 1 242.91 276.37 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