# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' NOPFAA in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 440.60 _exptl_crystal_F_000 2068.00 _reflns_d_resolution_high 0.8410 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.8149 _cell_length_b 13.1047 _cell_length_c 32.0387 _cell_angle_alpha 90.000 _cell_angle_beta 96.620 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45585.24 44336.00 623.55 o 4 0 0 11676.68 10993.17 525.35 o 6 0 0 30913.20 29022.16 962.33 o 8 0 0 8551.42 8027.61 790.49 o 10 0 0 3480.35 3260.14 756.12 o 1 1 0 22508.83 21655.58 185.31 o 2 1 0 20257.05 20895.08 530.26 o 3 1 0 245.13 456.62 225.67 o 4 1 0 1305.81 1641.01 326.51 o 5 1 0 2433.18 2335.54 310.71 o 6 1 0 2292.76 2387.16 365.78 o 7 1 0 5484.02 4673.78 459.92 o 8 1 0 4109.60 4529.05 468.54 o 9 1 0 363.46 923.85 738.93 o 10 1 0 1140.11 1139.62 834.68 o 11 1 0 104.06 24.55 468.69 o 0 2 0 80206.66 78867.02 682.47 o 1 2 0 70.76 -98.65 189.19 o 2 2 0 8075.45 8214.19 432.07 o 3 2 0 5867.75 5940.93 446.80 o 4 2 0 15288.75 14523.35 579.36 o 5 2 0 265.83 648.10 373.15 o 6 2 0 9471.02 10364.71 643.19 o 7 2 0 3342.15 2091.60 623.55 o 8 2 0 11372.93 10875.33 878.86 o 9 2 0 1165.85 1531.88 613.73 o 10 2 0 3068.56 3049.02 800.31 o 11 2 0 215.88 294.59 662.83 o 1 3 0 47160.67 46292.82 506.88 o 2 3 0 2341.97 2911.54 378.06 o 3 3 0 47591.47 45980.80 869.04 o 4 3 0 5007.63 4919.68 456.62 o 5 3 0 8206.47 8179.82 584.27 o 6 3 0 2337.34 2376.37 540.08 o 7 3 0 8791.31 9196.16 741.39 o 8 3 0 351.93 584.27 564.63 o 9 3 0 3570.81 3589.10 707.02 o 10 3 0 170.83 991.79 623.55 o 11 3 0 825.71 1335.48 721.75 o 0 4 0 2585.17 2857.54 387.88 o 1 4 0 2030.20 2163.90 270.53 o 2 4 0 10266.88 9608.59 495.90 o 3 4 0 1650.10 1900.11 358.42 o 4 4 0 15648.15 15809.74 672.65 o 5 4 0 1626.16 1703.72 422.25 o 6 4 0 2666.58 1914.84 579.36 o 7 4 0 4785.50 5012.96 672.65 o 8 4 0 3521.63 3883.70 702.11 o 9 4 0 886.24 1389.49 682.47 o 10 4 0 594.94 -314.23 731.57 o 11 4 0 911.27 1315.84 707.02 o 1 5 0 34636.70 35207.90 550.21 o 2 5 0 2421.59 2135.79 378.06 o 3 5 0 62507.09 62630.12 1139.09 o 4 5 0 1682.42 1870.66 461.53 o 5 5 0 16778.36 15014.34 805.22 o 6 5 0 1081.60 1256.92 535.17 o 7 5 0 12906.67 12603.60 913.23 o 8 5 0 96.27 -34.37 579.36 o 9 5 0 6797.66 7242.04 849.41 o 10 5 0 1.39 -1055.62 638.28 o 0 6 0 91.25 -181.66 387.88 o 1 6 0 171.46 318.02 249.32 o 2 6 0 494.99 918.14 358.42 o 3 6 0 1644.55 1306.02 417.34 o 4 6 0 869.20 1610.43 427.16 o 5 6 0 601.49 294.59 486.08 o 6 6 0 233.27 -29.46 535.17 o 7 6 0 5404.81 5656.15 775.76 o 8 6 0 93.23 -628.46 608.82 o 9 6 0 1793.96 333.87 726.66 o 10 6 0 612.86 765.94 667.74 o 1 7 0 26705.23 25815.06 593.55 o 2 7 0 524.08 510.63 422.25 o 3 7 0 11997.88 11547.98 687.38 o 4 7 0 153.21 162.03 456.62 o 5 7 0 11361.41 11307.40 795.40 o 6 7 0 764.81 1065.44 564.63 o 7 7 0 11445.54 10389.25 972.15 o 8 7 0 46.04 309.32 564.63 o 9 7 0 2094.48 3333.79 756.12 o 10 7 0 15.61 495.90 628.46 o 0 8 0 39105.80 41296.80 1119.45 o 1 8 0 958.81 795.93 338.38 o 2 8 0 7414.68 6932.72 628.46 o 3 8 0 387.12 1139.09 486.08 o 4 8 0 2105.01 2204.53 520.44 o 5 8 0 478.91 412.43 535.17 o 6 8 0 4875.18 5415.57 687.38 o 7 8 0 156.53 260.22 544.99 o 8 8 0 1594.47 2027.77 726.66 o 9 8 0 206.50 230.76 667.74 o 1 9 0 4135.17 4588.59 423.39 o 2 9 0 331.50 -333.87 520.44 o 3 9 0 7592.82 7521.90 726.66 o 4 9 0 160.84 63.83 535.17 o 5 9 0 4325.58 4099.73 707.02 o 6 9 0 1085.89 -392.79 633.37 o 7 9 0 1710.74 878.86 657.92 o 8 9 0 870.39 1944.30 608.82 o 9 9 0 370.21 486.08 697.20 o 0 10 0 20117.99 20670.49 977.06 o 1 10 0 490.34 -14.73 427.03 o 2 10 0 20931.14 19197.54 1070.35 o 3 10 0 65.85 1065.44 599.00 o 4 10 0 9428.75 9073.41 839.59 o 5 10 0 387.95 427.16 584.27 o 6 10 0 4806.21 5386.11 795.40 o 7 10 0 4.45 132.57 623.55 o 8 10 0 2692.47 3731.49 751.21 o 1 11 0 308.75 499.76 405.45 o 2 11 0 56.46 0.00 554.81 o 3 11 0 0.77 716.84 569.54 o 4 11 0 1238.83 1625.16 594.09 o 5 11 0 23.99 -623.55 608.82 o 6 11 0 821.81 1011.43 618.64 o 7 11 0 1.06 -466.44 667.74 o 8 11 0 208.74 -98.20 697.20 o 0 12 0 7568.48 8219.10 859.22 o 1 12 0 593.68 1108.83 702.11 o 2 12 0 5907.29 7060.37 800.31 o 3 12 0 159.17 -1281.47 657.92 o 4 12 0 8516.16 9112.69 918.14 o 5 12 0 79.74 -422.25 702.11 o 6 12 0 2869.71 3760.95 741.39 o 7 12 0 48.02 947.60 667.74 o 1 13 0 1514.76 1629.51 480.38 o 2 13 0 296.75 1797.01 559.72 o 3 13 0 1235.85 1959.03 677.56 o 4 13 0 83.78 -88.38 672.65 o 5 13 0 1422.70 1350.21 815.04 o 6 13 0 233.28 -147.30 795.40 o 0 14 0 1522.12 1414.04 770.85 o 1 14 0 5.78 -377.93 473.43 o 2 14 0 2102.88 2582.58 657.92 o 3 14 0 247.51 1104.72 662.83 o 4 14 0 1802.91 721.75 795.40 o 5 14 0 59.05 353.51 682.47 o 1 15 0 3338.53 4123.11 702.11 o 2 15 0 18.91 1723.36 599.00 o 3 15 0 2771.35 1571.15 878.86 o -11 0 1 76.33 -476.26 662.83 o -9 0 1 2144.71 2214.35 657.92 o -7 0 1 3362.59 3495.82 535.17 o -5 0 1 5207.01 4413.96 500.81 o -3 0 1 40314.96 40712.53 741.39 o -1 0 1 26654.81 27587.18 251.69 o 1 0 1 90698.56 92002.55 451.33 o 3 0 1 58143.33 57671.17 869.04 o 5 0 1 22088.33 20852.16 741.39 o 7 0 1 8226.85 8523.51 711.93 o 9 0 1 8124.57 7757.57 824.86 o 11 0 1 4828.73 6147.14 864.13 o -11 1 1 3109.41 3466.99 1342.85 o -10 1 1 11.39 263.62 478.71 o -9 1 1 7495.09 6630.73 643.19 o -8 1 1 50.89 -4.39 601.46 o -7 1 1 14344.02 14450.95 607.44 o -6 1 1 60.93 -289.91 301.81 o -5 1 1 24570.13 22470.82 655.47 o -4 1 1 9280.30 9607.64 361.07 o -3 1 1 57247.05 58317.56 616.18 o -2 1 1 75324.47 76402.73 1048.26 o -1 1 1 12419.56 11787.62 311.82 o 1 1 1 14922.40 15196.34 182.90 o 2 1 1 768.13 1309.93 224.39 o 3 1 1 24233.31 24941.36 815.04 o 4 1 1 940.33 838.34 240.82 o 5 1 1 2660.26 2615.19 301.99 o 6 1 1 260.41 265.94 311.78 o 7 1 1 1032.00 1555.10 456.62 o 8 1 1 148.75 270.04 549.90 o 9 1 1 341.77 276.32 435.70 o 10 1 1 428.65 -250.40 463.47 o 11 1 1 2.43 -497.96 507.90 o -11 2 1 95.10 49.10 692.29 o -10 2 1 1812.17 2783.89 677.56 o -9 2 1 575.93 981.97 608.82 o -8 2 1 2219.07 1286.38 638.28 o -7 2 1 4299.89 4173.38 603.91 o -6 2 1 10145.38 9858.99 667.74 o -5 2 1 4107.62 2999.92 461.53 o -4 2 1 3802.56 3122.67 407.52 o -3 2 1 15579.14 16349.82 554.81 o -2 2 1 11693.46 11656.00 461.53 o -1 2 1 21030.39 21268.37 653.01 o 0 2 1 151.88 -218.49 173.59 o 1 2 1 130527.38 136853.08 1782.28 o 2 2 1 34528.57 33858.37 653.01 o 3 2 1 47249.00 46908.77 839.59 o 4 2 1 5545.34 5690.52 427.16 o 5 2 1 10469.96 10232.14 579.36 o 6 2 1 68.05 68.74 436.98 o 7 2 1 13870.47 13261.52 873.95 o 8 2 1 187.77 667.74 574.45 o 9 2 1 5961.99 6225.70 770.85 o 10 2 1 6.02 -599.00 662.83 o 11 2 1 2449.97 3333.79 785.58 o -11 3 1 947.53 -790.49 795.40 o -10 3 1 206.80 -171.84 623.55 o -9 3 1 3284.22 3377.98 702.11 o -8 3 1 1534.30 34.37 648.10 o -7 3 1 10386.90 8710.08 810.13 o -6 3 1 1802.22 878.86 520.44 o -5 3 1 1962.76 2238.89 427.16 o -4 3 1 6804.27 7080.01 500.81 o -3 3 1 1635.45 1998.31 338.78 o -2 3 1 3421.92 3181.59 373.15 o -1 3 1 35232.36 35751.31 460.00 o 0 3 1 15258.26 15568.44 347.18 o 1 3 1 896.28 620.23 256.84 o 2 3 1 45753.71 42538.99 756.12 o 3 3 1 4601.86 4428.69 422.25 o 4 3 1 13935.22 14660.83 594.09 o 5 3 1 11374.81 12745.99 648.10 o 6 3 1 11589.54 10644.57 716.84 o 7 3 1 1738.95 893.59 569.54 o 8 3 1 6709.88 5936.02 805.22 o 9 3 1 243.55 1016.34 544.99 o 10 3 1 2299.14 1998.31 736.48 o 11 3 1 13.84 299.50 643.19 o -11 4 1 116.36 -299.50 707.02 o -10 4 1 3577.16 4271.57 770.85 o -9 4 1 252.94 -378.06 623.55 o -8 4 1 9866.93 8739.54 805.22 o -7 4 1 1157.68 1718.45 549.90 o -6 4 1 30054.81 29871.56 1065.44 o -5 4 1 661.92 392.79 441.89 o -4 4 1 38032.16 35861.59 923.05 o -3 4 1 179.80 407.52 358.42 o -2 4 1 8676.66 7752.66 451.71 o -1 4 1 392.00 289.68 236.08 o 0 4 1 35299.02 33810.39 802.76 o 1 4 1 14636.67 14914.78 380.05 o 2 4 1 7724.79 8857.38 466.44 o 3 4 1 12368.45 11508.70 594.09 o 4 4 1 10019.79 8602.07 579.36 o 5 4 1 6728.49 6854.16 589.18 o 6 4 1 7909.29 9235.44 741.39 o 7 4 1 2786.29 3078.48 633.37 o 8 4 1 73.31 -201.30 549.90 o 9 4 1 1544.27 2287.99 618.64 o 10 4 1 23.77 88.38 603.91 o 11 4 1 442.50 -657.92 751.21 o -11 5 1 52.41 878.86 707.02 o -10 5 1 688.55 1006.52 648.10 o -9 5 1 504.16 476.26 657.92 o -8 5 1 1082.71 0.00 594.09 o -7 5 1 26.83 63.83 574.45 o -6 5 1 14364.26 14150.21 873.95 o -5 5 1 2592.34 2155.43 549.90 o -4 5 1 16073.55 15829.38 721.75 o -3 5 1 1271.47 1271.65 378.06 o -2 5 1 11354.14 11317.22 520.44 o -1 5 1 7.87 -103.42 246.20 o 0 5 1 15028.92 14933.21 402.73 o 1 5 1 627.50 848.10 245.49 o 2 5 1 25077.16 23027.23 687.38 o 3 5 1 163.95 333.87 368.24 o 4 5 1 39262.07 38699.48 1016.34 o 5 5 1 56.27 -972.15 486.08 o 6 5 1 12899.40 12976.75 844.50 o 7 5 1 268.24 795.40 569.54 o 8 5 1 13000.40 13570.84 986.88 o 9 5 1 0.75 -805.22 653.01 o 10 5 1 3499.18 4021.17 736.48 o -10 6 1 2889.14 2518.76 883.77 o -9 6 1 311.94 333.87 643.19 o -8 6 1 6515.36 6598.85 761.03 o -7 6 1 1.99 -34.37 633.37 o -6 6 1 9726.21 9736.24 810.13 o -5 6 1 318.04 540.08 471.35 o -4 6 1 26515.86 25408.51 913.23 o -3 6 1 321.26 -54.01 407.52 o -2 6 1 20116.31 20189.33 711.93 o -1 6 1 197.74 -84.35 251.69 o 0 6 1 19676.99 20100.95 477.36 o 1 6 1 6175.06 7055.21 400.15 o 2 6 1 17926.71 17326.88 687.38 o 3 6 1 1644.53 1826.47 392.79 o 4 6 1 12490.68 12250.09 697.20 o 5 6 1 28.02 274.95 456.62 o 6 6 1 4450.42 3166.86 603.91 o 7 6 1 852.39 -166.94 628.46 o 8 6 1 23.53 1035.98 540.08 o 9 6 1 403.14 122.75 638.28 o 10 6 1 212.98 49.10 677.56 o -10 7 1 340.94 -49.10 677.56 o -9 7 1 1164.94 1394.40 707.02 o -8 7 1 31.31 152.21 564.63 o -7 7 1 2226.51 3098.12 662.83 o -6 7 1 2030.31 1870.66 599.00 o -5 7 1 3450.70 3962.25 574.45 o -4 7 1 7955.00 6986.73 648.10 o -3 7 1 1463.60 2396.01 422.25 o -2 7 1 14025.02 12716.53 682.47 o -1 7 1 1611.00 1355.12 280.96 o 0 7 1 11622.40 12455.79 447.50 o 1 7 1 381.73 351.05 277.74 o 2 7 1 9125.63 8803.37 594.09 o 3 7 1 1908.70 1772.46 456.62 o 4 7 1 25907.30 26331.56 996.70 o 5 7 1 702.76 918.14 500.81 o 6 7 1 5764.62 5337.01 736.48 o 7 7 1 61.63 -1266.74 633.37 o 8 7 1 5817.69 5641.42 844.50 o 9 7 1 819.22 88.38 672.65 o 10 7 1 2976.06 3702.03 790.49 o -9 8 1 1130.23 1065.44 731.57 o -8 8 1 3003.92 4035.90 805.22 o -7 8 1 322.46 220.94 608.82 o -6 8 1 3541.83 4585.81 692.29 o -5 8 1 96.78 -525.35 554.81 o -4 8 1 7911.24 6240.43 726.66 o -3 8 1 3618.68 3486.00 544.99 o -2 8 1 8600.71 8248.56 618.64 o -1 8 1 3677.42 3588.99 366.16 o 0 8 1 5973.11 5880.40 405.09 o 1 8 1 3849.92 3730.79 392.13 o 2 8 1 7900.11 6127.50 628.46 o 3 8 1 15616.46 16570.76 869.04 o 4 8 1 2492.33 1600.61 623.55 o 5 8 1 3585.16 3760.95 672.65 o 6 8 1 419.22 -594.09 603.91 o 7 8 1 1064.10 1526.97 579.36 o 8 8 1 39.93 250.40 628.46 o 9 8 1 1895.73 1252.01 765.94 o -9 9 1 1353.69 2641.50 736.48 o -8 9 1 116.24 618.64 633.37 o -7 9 1 3342.68 2376.37 741.39 o -6 9 1 1585.57 2057.23 648.10 o -5 9 1 12028.31 12962.02 918.14 o -4 9 1 3003.13 2705.33 643.19 o -3 9 1 10435.60 10394.17 785.58 o -2 9 1 821.19 1836.29 490.99 o -1 9 1 2977.40 2644.86 403.92 o 0 9 1 7535.81 7252.41 473.66 o 1 9 1 9439.98 8781.29 883.77 o 2 9 1 3641.53 2612.04 608.82 o 3 9 1 8992.62 9466.20 780.67 o 4 9 1 2001.55 1625.16 569.54 o 5 9 1 1703.87 1816.65 584.27 o 6 9 1 1935.09 1939.39 677.56 o 7 9 1 298.25 476.26 589.18 o 8 9 1 1004.79 1109.63 687.38 o 9 9 1 300.25 1129.27 741.39 o -8 10 1 480.60 284.77 613.73 o -7 10 1 1036.01 810.13 687.38 o -6 10 1 40.85 -427.16 648.10 o -5 10 1 2587.03 3746.22 653.01 o -4 10 1 404.25 451.71 638.28 o -3 10 1 6448.17 6029.30 756.12 o -2 10 1 2830.69 3166.86 643.19 o -1 10 1 11568.02 11456.73 588.28 o 0 10 1 1397.42 1618.86 426.35 o 1 10 1 14058.38 13764.26 631.84 o 2 10 1 20.54 1556.42 540.08 o 3 10 1 12041.71 13772.15 918.14 o 4 10 1 250.83 653.01 623.55 o 5 10 1 7897.93 7870.50 854.31 o 6 10 1 677.88 -39.28 672.65 o 7 10 1 3412.36 2322.36 810.13 o 8 10 1 4.96 810.13 648.10 o -8 11 1 0.54 -859.22 726.66 o -7 11 1 2867.51 2258.53 736.48 o -6 11 1 4.06 1050.71 603.91 o -5 11 1 5648.84 5233.91 829.77 o -4 11 1 34.46 579.36 599.00 o -3 11 1 5475.83 5356.65 721.75 o -2 11 1 137.71 -34.37 599.00 o -1 11 1 8779.36 8234.78 607.56 o 0 11 1 106.12 661.49 418.25 o 1 11 1 6592.35 5521.15 523.93 o 2 11 1 1.45 417.34 579.36 o 3 11 1 1929.23 2587.49 603.91 o 4 11 1 69.66 -34.37 594.09 o 5 11 1 931.98 932.87 643.19 o 6 11 1 62.19 -83.47 608.82 o 7 11 1 420.98 -417.34 697.20 o 8 11 1 0.19 152.21 643.19 o -7 12 1 635.14 996.70 697.20 o -6 12 1 789.77 957.42 716.84 o -5 12 1 1288.51 721.75 707.02 o -4 12 1 115.84 -677.56 662.83 o -3 12 1 1610.94 795.40 662.83 o -2 12 1 14.67 -648.10 608.82 o -1 12 1 3570.63 3304.12 900.96 o 0 12 1 184.78 255.67 812.58 o 1 12 1 5108.69 5162.04 518.61 o 2 12 1 890.51 972.15 618.64 o 3 12 1 3744.79 4124.28 775.76 o 4 12 1 311.88 795.40 623.55 o 5 12 1 4956.62 5386.11 824.86 o 6 12 1 192.56 -829.77 721.75 o 7 12 1 2515.88 2513.85 765.94 o -6 13 1 903.89 495.90 800.31 o -5 13 1 2739.58 3161.95 756.12 o -4 13 1 190.41 962.33 672.65 o -3 13 1 3492.33 2916.45 844.50 o -2 13 1 384.26 1080.17 628.46 o -1 13 1 1234.22 1485.34 1116.99 o 0 13 1 1307.71 2086.33 449.35 o 1 13 1 1720.57 1795.56 584.27 o 2 13 1 1319.77 2125.97 657.92 o 3 13 1 1232.20 1718.45 657.92 o 4 13 1 638.08 132.57 702.11 o 5 13 1 383.83 -186.57 721.75 o 6 13 1 1015.57 947.60 707.02 o -5 14 1 510.82 1423.86 677.56 o -4 14 1 1741.51 1394.40 780.67 o -3 14 1 1487.36 1792.10 770.85 o -2 14 1 1950.19 849.41 707.02 o -1 14 1 1315.05 1279.47 492.56 o 0 14 1 643.80 993.90 480.08 o 1 14 1 783.97 976.60 482.43 o 2 14 1 1042.60 1963.94 672.65 o 3 14 1 1971.25 923.05 805.22 o 4 14 1 612.75 530.26 697.20 o 5 14 1 1157.61 260.22 810.13 o -3 15 1 359.39 353.51 746.30 o -2 15 1 1106.62 1129.27 761.03 o -1 15 1 169.55 265.13 489.52 o 0 15 1 1366.84 1263.57 996.70 o 1 15 1 222.79 474.00 603.91 o 2 15 1 2877.44 3643.11 829.77 o 3 15 1 163.05 -1271.65 805.22 o -10 0 2 1537.84 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