Crystal Structure Communications

 

Acta Cryst. (2006). C62, i13-i15  [ doi:10.1107/S0108270105039041 ]

A new whitlockite, Ca_8.42Na_1.16V(PO₄)₇

A. A. Tsirlin, E. V. Dikarev, R. V. Shpanchenko and E. V. Antipov

Synopsis: Ca_8.42Na_1.16V(PO₄)₇ is the first whitlockite containing vanadium(III) in the M5 octahedral site. Calcium ions occupy eight- and nine-coordinated sites. Sodium ions partially occupy one octahedral position and share one nine-coordinated position with a Ca atom.

Formula: Ca_8.42Na_1.16V(PO₄)₇

Online 21 January 2006

 

Acta Cryst. (2006). C62, i16-i18  [ doi:10.1107/S0108270106000679 ]

MoCu₃TeO₇Cl₂·0.5H₂O

R. Takagi, F. Duc and M. Johnsson

Synopsis: The framework structure of MoCu₃TeO₇Cl₂·0.5H₂O is built up of layers of CuO₄Cl, CuO₃Cl₂ and TeO₃₊₁ polyhedra bridged by Mo₂O₈ polyhedra, with water molecules accommodated in channels parallel to [100].

Formula: MoCu₃TeO₇Cl₂·0.5H₂O

Online 21 January 2006

 

Acta Cryst. (2006). C62, i19-i20  [ doi:10.1107/S0108270105043076 ]

Cation distribution in the zirconium chloride cluster phase Cs[(Zr₆C)Cl₁₅]

H. W. Rohm and M. Köckerling

Synopsis: The synthesis and single-crystal X-ray structure of orthorhombic Cs[(Zr₆C)Cl₁₅], a phase which contains octahedral C-centered zirconium clusters which are three-dimensionally linked through Cl atoms, are reported. Caesium cations are distributed over several sites within the cluster network.

Formula: Cs[(Zr₆C)Cl₁₅]

Online 31 January 2006

 

Acta Cryst. (2006). C62, m27-m29  [ doi:10.1107/S0108270105039910 ]

A mixed-valence diacetate-bridged Mn^II-Mn^III complex incorporating a bridging phenolate ligand

A. J. Bortoluzzi, A. Neves, R. A. A. Couto and R. A. Peralta

Formula: [Mn₂(C₄₂H₄₉N₅O₂)(C₂H₃O₂)₂](C₂₄H₂₀B)

Online 14 January 2006

 

Acta Cryst. (2006). C62, m30-m32  [ doi:10.1107/S0108270105041661 ]

Bis[bis(3-phenylpyrazol-1-yl)(pyrazol-1-yl)methane]copper(II) bis(perchlorate) acetonitrile disolvate

M. S. Goodman, M. A. Goodman, A. Y. Kovalevsky, A. Y. Nazarenko and D. Pope

Formula: [Cu(C₂₂H₁₈N₆)₂](ClO₄)₂·2C₂H₃N

Online 14 January 2006

 

Acta Cryst. (2006). C62, m33-m36  [ doi:10.1107/S0108270105041247 ]

A one-dimensional iodine-bridged Pt^II/Pt^IV mixed-valence complex, catena-poly[[[bis(ethylenediamine)platinum(II)]--iodo-[bis(ethylenediamine)platinum(IV)]--iodo] hydrogenphosphate dihydrogenphosphate iodide trihydrate]

N. Matsushita

Formula: [Pt₂I₂(C₂H₈N₂)₄](HPO₄)(H₂PO₄)I·3H₂O

Online 14 January 2006

 

Acta Cryst. (2006). C62, m37-m40  [ doi:10.1107/S0108270105040114 ]

Disodium 2,5-bis(phenylamino)terephthalate decahydrate, an intermediate in the industrial synthesis of quinacridone pigments

M. U. Schmidt, T. Schmiermund and M. Bolte

Formula: 2Na⁺·C₂₀H₁₄N₂O₄^2-·10H₂O

Online 14 January 2006

 

Acta Cryst. (2006). C62, m41-m44  [ doi:10.1107/S0108270105042125 ]

A novel three-dimensional cadmium(II) coordination polymer incorporating 1,4-bis(1,2,4-triazol-1-ylmethyl)benzene and thiocyanate

B.-Z. Li, X.-G. Liu, Y.-F. Peng, B.-L. Li and Y. Zhang

Formula: [Cd(NCS)₂(C₁₂H₁₂N₆)]

Online 14 January 2006

 

Acta Cryst. (2006). C62, m45-m47  [ doi:10.1107/S0108270105042113 ]

Bis{[phthalocyaninato(2-)]arsenic(III)} octaiododiarsenic(III)

J. Janczak and G. J. Perpétuo

Formula: [As(C₃₂H₁₆N₈)]₂[As₂I₈]

Online 14 January 2006

 

Acta Cryst. (2006). C62, m48-m50  [ doi:10.1107/S0108270105042575 ]

A novel nickel(II) coordination polymer incorporating 1,4-phenylenediacetic acid and 1,10-phenanthroline

Z.-L. Chen, Y.-Z. Zhang and F.-P. Liang

Formula: [Ni₃(C₁₀H₈O₄)₃(C₁₂H₈N₂)₂]·2H₂O

Online 14 January 2006

 

Acta Cryst. (2006). C62, m51-m53  [ doi:10.1107/S0108270105043088 ]

Tris(1,10-phenanthroline)copper(II) di--iodo-bis(diiodomercurate) dimethyl sulfoxide monohydrate

M.-J. Oh, Y.-M. Lee, S. J. Lee, S. K. Kang and S.-N. Choi

Formula: [Cu(C₁₂H₈N₂)₃][Hg₂I₆]·C₂H₆OS·H₂O

Online 14 January 2006

 

Acta Cryst. (2006). C62, m54-m55  [ doi:10.1107/S0108270105042484 ]

Dichloro(1,2-dimethoxyethane)bis(tosylimido)molybdenum(VI), a versatile nitrene transfer reagent

K. A. Rufanov and B. Ziemer

Formula: [Mo(C₇H₇NO₂S)₂Cl₂(C₄H₁₀O₂)]

Online 14 January 2006

 

Acta Cryst. (2006). C62, m56-m59  [ doi:10.1107/S0108270106000540 ]

Two one-dimensional zinc(II) coordination polymers: catena-poly[[bis(pentane-2,4-dionato-²O,O')zinc]--1,4-bis(x-pyridyl)-2,3-diazabuta-1,3-diene] (x = 3, 4)

J. Granifo, M. T. Garland and R. Baggio

Formula: Two isomers of [Zn(C₅H₇O₂)₂(C₁₂H₁₀N₄)]

Online 21 January 2006

 

Acta Cryst. (2006). C62, m60-m62  [ doi:10.1107/S0108270105042241 ]

Tetrapiperidinium di--methoxy-di-₅-oxo-tetra-₃-oxo-dodeca-₂-oxo-octaoxodecavanadate

F. Sun, Y.-T. Li, Z.-Y. Wu, D.-Q. Wang and J.-M. Dou

Formula: (C₅H₁₂N)₄[V₁₀(CH₃O)₂O₂₆]

Online 21 January 2006

 

Acta Cryst. (2006). C62, m63-m66  [ doi:10.1107/S0108270105041570 ]

Insights into crystallization mechanism: a synchrotron study of polymorphism in a cobalt acetate cluster compound

J. C. Burley and T. J. Prior

Formula: Two polymorphs of [Co₃(C₂H₃O₂)₄(C₅H₅N)₈](PF₆)₂

Online 21 January 2006

 

Acta Cryst. (2006). C62, m67-m69  [ doi:10.1107/S0108270106000680 ]

Bis(-diphenylphosphinato-²O:O')bis[aqua(diphenylphosphinato-O)bis(pyridine-N)cobalt(II)]

L. de Oliveira Diehl, M. R. Siqueira and R. A. Burrow

Formula: [Co₂(C₁₂H₁₀O₂P)₄(C₅H₅N)₄(H₂O)₂]

Online 21 January 2006

 

Acta Cryst. (2006). C62, m70-m73  [ doi:10.1107/S0108270106001181 ]

Cadmium nitrate coordination polymers with substituted pyridazino[4,5-d]pyridazines

K. V. Domasevitch, P. V. Solntsev and J. Sieler

Formula: [Cd(NO₃)₂(C₁₂H₁₂N₄)(H₂O)] and [Cd(NO₃)₂(C₁₂H₁₂N₄)]·CHCl₃

Online 31 January 2006

 

Acta Cryst. (2006). C62, m74-m77  [ doi:10.1107/S0108270106001387 ]

Dichloro[(3,5-dimethyl-1H-pyrazol-1-yl)methane]zinc(II) and di--chloro-bis{chloro[(3,5-dimethyl-1H-pyrazol-1-yl)methane]cadmium(II)}

M.-L. Cheng, H.-X. Li, Y. Zang and J.-P. Lang

Formula: [ZnCl₂(C₁₁H₁₆N₄)] and [Cd₂Cl₄(C₁₁H₁₆N₄)₂]

Online 31 January 2006

 

Acta Cryst. (2006). C62, m78-m80  [ doi:10.1107/S0108270105042940 ]

A cobalt(III) compound of a 13-membered cyclic tetraamine: trans-(12,12-dimethyl-1,4,7,10-tetraazacyclotetradecane)diisothiocyanatocobalt(III) tetraisothiocyanatozinc(II) ethanol solvate

N. F. Curtis, K. Flood and W. T. Robinson

Formula: [Co(NCS)₂(C₁₁H₂₆N₄)]₂[Zn(NCS)₄]·C₂H₆O

Online 31 January 2006

 

Acta Cryst. (2006). C62, o53-o57  [ doi:10.1107/S0108270105041235 ]

Three 4-aminoquinolines of antimalarial interest

S. A. Bourne, K. De Villiers and T. J. Egan

Formula: C₁₅H₂₀IN₃, C₁₅H₂₀BrN₃·2H₂O and C₁₅H₂₂ClN₃²⁺·2H₂O₄P^-·H₃O₄P

Online 14 January 2006

 

Acta Cryst. (2006). C62, o58-o61  [ doi:10.1107/S0108270105040928 ]

Hydrogen bonding and - stacking in 7-{2-[4-(4-methoxyphenyl)piperazin-1-yl]ethoxy}-4-methyl-2H-chromen-2-one monohydrate

X. Zhou, X.-B. Wang and L.-Y. Kong

Formula: C₂₃H₂₆N₂O₄·H₂O

Online 14 January 2006

 

Acta Cryst. (2006). C62, o62-o64  [ doi:10.1107/S0108270105041211 ]

An azo dye molecule having a pyridine-2,6-dione backbone

H.-F. Qian and W. Huang

Formula: C₂₁H₂₄N₄O₆

Online 14 January 2006

 

Acta Cryst. (2006). C62, o65-o67  [ doi:10.1107/S0108270105041089 ]

Three-in-one: the novel packing and structures of three independent molecules of a tricyclic boron compound

G. J. Gainsford and N. Al-Salim

Formula: C₁₅H₃₆B₃N₃O₆

Online 14 January 2006

 

Acta Cryst. (2006). C62, o68-o70  [ doi:10.1107/S010827010504093X ]

Naphthalene-1,3-diol

B. Marciniak, E. Rozycka-Sokolowska and V. Pavlyuk

Formula: C₁₀H₈O₂

Online 14 January 2006

 

Acta Cryst. (2006). C62, o71-o72  [ doi:10.1107/S0108270105040953 ]

Glycinium trichloroacetate

V. H. Rodrigues, A. Matos Beja, J. A. Paixão and M. M. R. R. Costa

Formula: C₂H₆NO₂⁺·C₂Cl₃O₂^-

Online 14 January 2006

 

Acta Cryst. (2006). C62, o73-o75  [ doi:10.1107/S0108270105041934 ]

Tris(methylammonium) hydrogenphosphate dihydrogenphosphate

J. Fábry, R. Krupková, P. Vanek and M. Dusek

Formula: 3CH₆N⁺·HPO₄^2-·H₂PO₄^-

Online 14 January 2006

 

Acta Cryst. (2006). C62, o76-o78  [ doi:10.1107/S0108270105042204 ]

An oximino tautomer of 1-n-decyl-4-hydroxyimino-3-methyl-1H-pyrazol-5(4H)-one

J. Belmar, C. Jiménez, L. Ortiz, M. T. Garland and R. Baggio

Formula: C₁₄H₂₅N₃O₂

Online 14 January 2006

 

Acta Cryst. (2006). C62, o79-o81  [ doi:10.1107/S0108270105041983 ]

N⁸-(2'-O-Methylribofuranosyl)-8-aza-7-deazaadenine monohydrate

X. Zhang, S. Budow, P. Leonard, H. Eickmeier and F. Seela

Formula: C₁₁H₁₅N₅O₄·H₂O

Online 14 January 2006

 

Acta Cryst. (2006). C62, o82-o85  [ doi:10.1107/S010827010504254X ]

Methyl 4-O--L-galactopyranosyl--D-glucopyranoside (methyl -L-lactoside)

Q. Pan, B. C. Noll and A. S. Serianni

Formula: C₁₃H₂₄O₁₁

Online 21 January 2006

 

Acta Cryst. (2006). C62, o86-o88  [ doi:10.1107/S0108270106000874 ]

7-Hydroxy-6-methoxy-3-[(2-oxo-2H-1-benzopyran-7-yl)oxy]-2H-1-benzopyran-2-one

T.-Z. Zhang, C.-Y. Wei, G.-H. Xu and S.-W. Park

Formula: C₁₉H₁₂O₇

Online 21 January 2006

 

Acta Cryst. (2006). C62, o89-o91  [ doi:10.1107/S0108270106001053 ]

Hydrogen bonding in meso-4,5-diphenyl-3,6-diazaoctane-1,8-diol: the formation of one-dimensional linear chains of edge-fused rings

M. Dinçer, N. Özdemir, S. Saydam, O. Bekaroglu and O. Büyükgüngör

Formula: C₁₈H₂₄N₂O₂

Online 21 January 2006

 

Acta Cryst. (2006). C62, o92-o94  [ doi:10.1107/S0108270106001065 ]

(2RS,5SR,6SR)-Methyl 4-{cis-2-[3-fluoro-5-(4-methoxy-3,4,5,6-tetrahydro-2H-pyran-4-yl)phenoxymethyl]-6-hydroxy-3-phenylmorpholino}benzenesulfinate

C. Charlier, A. Delayen, B. Norberg, J.-P. Hénichart and J. Wouters

Formula: C₃₀H₃₄FNO₇S

Online 21 January 2006

 

Acta Cryst. (2006). C62, o95-o97  [ doi:10.1107/S0108270105043052 ]

2,2,4,4-Tetra-tert-butyl-1,3,5,2,4-benzotrioxadisilepine-7-carbaldehyde

L. C. R. Andrade, J. A. Paixão, M. J. M. de Almeida, C. Siquet and F. Borges

Formula: C₂₃H₄₀O₄Si₂

Online 21 January 2006

 

Acta Cryst. (2006). C62, o98-o100  [ doi:10.1107/S0108270106000023 ]

(±)-1-Methyl-1,3,6-triphenyl-7-(2-phenylpropenyl)-1,2-dihydronaphthalene

Y. Sui, C. Barnes and R. Glaser

Formula: C₃₈H₃₂

Online 31 January 2006

 

Acta Cryst. (2006). C62, o101-o103  [ doi:10.1107/S0108270106001119 ]

The absolute configuration of (2S,4S)- and (2R,4R)-2-tert-butyl-4-methyl-3-(4-tolylsulfonyl)-1,3-oxazolidine-4-carbaldehyde

S. Flock, C. Bruhn, H. Fink and H. Frauenrath

Formula: C₁₆H₂₃NO₄S

Online 31 January 2006

 

Acta Cryst. (2006). C62, o104-o106  [ doi:10.1107/S0108270106001545 ]

A zwitterion of 1,5-bis(2-hydroxybenzamido)-3-azapentane: a two-dimensional hydrogen-bonding network involving dimers

H.-M. Liu, L. He, X.-L. Luo and W.-Q. Zhang

Formula: C₁₈H₂₁N₃O₄

Online 31 January 2006

 

Acta Cryst. (2006). C62, o107-o110  [ doi:10.1107/S0108270105037856 ]

Hydrogen-bonding patterns in trimethoprim picolinate and 2-amino-4,6-dimethylpyrimidinium picolinate hemihydrate

M. Hemamalini, P. T. Muthiah and D. E. Lynch

Formula: C₁₄H₁₉N₄O₃⁺·C₆H₄NO₂^- and C₆H₁₀N₃⁺·C₆H₄NO₂^-·0.5H₂O

Online 31 January 2006