# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' _050301a Cdbbtz NCS' _shelx_refln_list_code 4 _shelx_F_calc_maximum 366.86 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.8301 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 22.7485 _cell_length_b 9.5867 _cell_length_c 7.9484 _cell_angle_alpha 90.000 _cell_angle_beta 99.787 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 23419.40 24370.23 121.26 o 6 0 0 15325.45 15654.46 99.54 o 8 0 0 2455.39 2254.23 40.91 o 10 0 0 21381.76 21701.37 181.57 o 12 0 0 13671.56 12968.73 116.05 o 14 0 0 18960.24 19396.61 174.11 o 16 0 0 6461.05 6201.02 92.91 o 18 0 0 11784.38 11925.27 233.58 o 20 0 0 2165.89 1964.72 69.44 o 22 0 0 181.46 170.68 29.74 o 24 0 0 2121.62 2098.05 87.20 o 26 0 0 3325.80 3283.48 132.46 o 3 1 0 4112.07 3560.43 23.29 o 5 1 0 22911.32 22879.02 134.23 o 7 1 0 3530.75 3514.69 35.68 o 9 1 0 108.94 120.46 13.42 o 11 1 0 3721.84 3680.27 41.86 o 13 1 0 624.50 672.01 22.63 o 15 1 0 364.25 363.36 19.26 o 17 1 0 239.20 253.30 18.94 o 19 1 0 42.89 59.34 15.80 o 21 1 0 38.19 36.69 12.86 o 23 1 0 195.06 160.14 20.89 o 25 1 0 271.33 198.89 28.77 o 0 2 0 64791.39 61176.94 619.34 o 2 2 0 35520.34 35123.19 128.63 o 4 2 0 8817.16 8316.57 48.78 o 6 2 0 177.94 149.85 15.05 o 8 2 0 2857.98 2667.31 32.93 o 10 2 0 10533.83 10414.17 76.84 o 12 2 0 18980.66 19377.24 119.52 o 14 2 0 23032.98 22954.90 269.40 o 16 2 0 13168.30 13184.36 117.01 o 18 2 0 9391.94 9495.61 100.28 o 20 2 0 4088.55 3949.89 72.03 o 22 2 0 1100.97 1134.93 39.70 o 24 2 0 1362.05 1446.71 61.69 o 26 2 0 1355.67 1410.26 72.10 o 1 3 0 458.37 444.61 17.53 o 3 3 0 64.05 109.14 10.28 o 5 3 0 1424.22 1486.33 24.81 o 7 3 0 3438.23 3480.66 39.32 o 9 3 0 1.09 22.02 18.06 o 11 3 0 833.38 871.41 23.40 o 13 3 0 2170.69 2254.48 39.07 o 15 3 0 497.00 513.59 23.50 o 17 3 0 174.24 151.81 18.82 o 19 3 0 1304.05 1370.16 43.12 o 21 3 0 187.26 177.84 23.15 o 23 3 0 73.89 81.62 17.61 o 25 3 0 276.16 299.06 34.87 o 0 4 0 51958.66 50662.85 369.68 o 2 4 0 44967.21 45401.87 275.06 o 4 4 0 11481.93 11007.85 78.65 o 6 4 0 17023.36 17511.07 188.20 o 8 4 0 4253.39 3945.02 53.07 o 10 4 0 15071.48 15770.05 111.54 o 12 4 0 8560.29 8352.31 86.50 o 14 4 0 9358.13 9265.51 75.37 o 16 4 0 17058.91 17316.74 150.39 o 18 4 0 3694.94 3598.06 68.14 o 20 4 0 6221.81 6299.04 114.10 o 22 4 0 71.76 99.23 15.56 o 24 4 0 699.60 743.18 54.37 o 1 5 0 311.15 338.18 19.64 o 3 5 0 1780.21 1798.18 34.43 o 5 5 0 82.03 68.20 11.83 o 7 5 0 133.41 186.35 16.37 o 9 5 0 199.69 228.04 15.94 o 11 5 0 269.45 299.97 25.12 o 13 5 0 115.95 128.25 15.13 o 15 5 0 812.60 788.11 28.57 o 17 5 0 2163.55 2146.75 51.77 o 19 5 0 484.82 539.28 34.10 o 21 5 0 311.88 308.43 26.81 o 23 5 0 0.38 -7.34 15.17 o 0 6 0 18660.14 19437.88 345.80 o 2 6 0 16139.00 16291.40 111.53 o 4 6 0 8080.85 8151.55 74.72 o 6 6 0 6247.15 6280.84 67.13 o 8 6 0 6218.71 6506.74 66.85 o 10 6 0 4050.57 3907.83 54.56 o 12 6 0 1392.83 1318.34 35.17 o 14 6 0 3738.85 3692.59 88.21 o 16 6 0 7501.25 7348.65 122.03 o 18 6 0 7534.74 7596.99 133.33 o 20 6 0 2207.67 2320.18 85.73 o 22 6 0 1026.19 948.29 53.79 o 1 7 0 1169.93 1240.23 32.69 o 3 7 0 2511.53 2494.98 43.53 o 5 7 0 2038.76 2055.52 39.84 o 7 7 0 8.50 33.32 10.86 o 9 7 0 120.16 174.50 19.25 o 11 7 0 1823.99 1805.61 44.06 o 13 7 0 502.46 478.48 26.59 o 15 7 0 154.09 110.35 20.45 o 17 7 0 123.59 111.48 22.07 o 19 7 0 0.74 31.78 13.55 o 21 7 0 18.89 41.87 46.17 o 0 8 0 5978.00 5928.89 97.63 o 2 8 0 5242.28 5253.24 69.54 o 4 8 0 12317.37 12886.57 118.96 o 6 8 0 3419.29 3363.10 63.21 o 8 8 0 5315.70 5434.57 83.84 o 10 8 0 6155.26 5813.85 79.37 o 12 8 0 983.34 1033.11 43.62 o 14 8 0 4229.63 4241.28 89.84 o 16 8 0 4830.78 4863.43 105.42 o 18 8 0 3560.91 3471.93 98.94 o 1 9 0 1142.32 1124.02 37.51 o 3 9 0 1019.28 1074.26 37.44 o 5 9 0 212.59 267.84 23.38 o 7 9 0 7.11 33.11 10.63 o 9 9 0 285.31 217.40 34.33 o 11 9 0 1018.56 988.41 46.41 o 13 9 0 163.29 111.43 24.75 o 15 9 0 13.46 50.79 15.55 o 0 10 0 3103.66 3180.81 152.83 o 2 10 0 3311.77 3413.64 81.16 o 4 10 0 2636.09 2520.71 61.34 o 6 10 0 2879.40 2845.85 73.64 o 8 10 0 4050.13 4302.03 100.83 o 10 10 0 2029.24 1854.20 70.38 o 12 10 0 1437.01 1290.76 69.15 o 1 11 0 173.27 142.72 26.18 o 3 11 0 365.20 413.65 37.51 o 5 11 0 130.84 123.09 23.63 o 7 11 0 37.17 10.92 27.24 o -27 1 1 4272.93 4452.07 196.13 o -25 1 1 2246.86 2483.23 67.98 o -23 1 1 3450.47 3618.06 69.81 o -21 1 1 1957.35 2039.97 43.75 o -19 1 1 1316.81 1322.43 41.30 o -17 1 1 1616.07 1612.00 32.85 o -15 1 1 15470.00 15701.96 108.57 o -13 1 1 32905.86 33061.01 180.07 o -11 1 1 34335.29 34154.94 184.58 o -9 1 1 29270.97 28179.49 151.39 o -7 1 1 6781.02 6309.08 53.56 o -5 1 1 537.49 692.24 23.48 o -3 1 1 52784.24 49651.82 247.80 o -1 1 1 29181.37 29137.29 102.79 o 1 1 1 10628.84 10500.01 49.64 o 3 1 1 60774.69 60002.63 306.79 o 5 1 1 60326.08 58707.78 207.48 o 7 1 1 43204.43 43827.72 172.15 o 9 1 1 15503.41 15408.31 101.34 o 11 1 1 7478.01 7575.76 63.24 o 13 1 1 1614.43 1541.68 32.75 o 15 1 1 8203.46 8432.82 81.89 o 17 1 1 12030.13 12198.33 120.76 o 19 1 1 5225.34 5429.74 82.60 o 21 1 1 5305.29 5250.04 94.47 o 23 1 1 5820.87 5615.11 131.68 o 25 1 1 346.61 329.10 39.56 o -26 2 1 88.51 92.09 23.68 o -24 2 1 191.68 167.54 26.30 o -22 2 1 251.18 287.85 20.56 o -20 2 1 134.40 130.87 13.75 o -18 2 1 112.31 98.91 14.14 o -16 2 1 8.22 51.69 10.50 o -14 2 1 44.34 122.68 16.63 o -12 2 1 556.14 605.44 17.84 o -10 2 1 1870.98 1966.29 26.60 o -8 2 1 284.66 361.56 14.83 o -6 2 1 0.14 16.43 23.72 o -4 2 1 15497.30 15253.87 68.39 o -2 2 1 1979.76 2081.60 23.74 o 0 2 1 21997.24 22728.86 106.77 o 2 2 1 606.14 723.76 16.68 o 4 2 1 10.76 12.53 9.32 o 6 2 1 384.52 476.78 19.82 o 8 2 1 2904.40 2906.50 36.73 o 10 2 1 130.75 167.12 14.63 o 12 2 1 945.24 956.12 26.51 o 14 2 1 15.12 25.49 11.42 o 16 2 1 191.89 179.46 17.78 o 18 2 1 337.88 375.18 22.72 o 20 2 1 1281.08 1301.01 44.41 o 22 2 1 13.28 62.95 15.98 o 24 2 1 57.04 36.95 21.06 o -25 3 1 2255.91 2526.59 99.45 o -23 3 1 2666.02 2786.19 76.24 o -21 3 1 2394.32 2516.71 86.31 o -19 3 1 51.44 76.55 11.64 o -17 3 1 2696.68 2584.34 42.32 o -15 3 1 5227.79 4999.62 50.26 o -13 3 1 20404.78 20930.93 141.27 o -11 3 1 27930.88 27555.42 151.81 o -9 3 1 14475.55 13718.78 80.36 o -7 3 1 11139.98 10486.72 104.65 o -5 3 1 13023.85 12785.88 89.80 o -3 3 1 17717.84 17257.37 93.37 o -1 3 1 6679.79 6368.37 47.23 o 1 3 1 32707.39 32024.00 207.87 o 3 3 1 45035.91 44453.88 195.45 o 5 3 1 24082.57 23313.72 155.68 o 7 3 1 27016.74 26540.85 153.97 o 9 3 1 3653.49 3759.40 45.91 o 11 3 1 2792.49 2885.01 43.03 o 13 3 1 5112.33 4993.48 59.54 o 15 3 1 4091.29 4087.14 56.14 o 17 3 1 9682.70 10022.56 101.16 o 19 3 1 7909.68 8022.72 94.99 o 21 3 1 7857.14 7946.25 138.44 o 23 3 1 2897.75 2743.93 69.71 o 25 3 1 2129.57 2100.00 79.46 o -24 4 1 742.38 703.23 74.28 o -22 4 1 131.02 119.47 16.34 o -20 4 1 60.87 55.24 10.09 o -18 4 1 794.74 696.08 30.36 o -16 4 1 12.97 31.54 9.02 o -14 4 1 720.43 675.24 23.62 o -12 4 1 2053.69 2272.69 37.90 o -10 4 1 40.65 60.84 7.69 o -8 4 1 777.60 813.67 22.84 o -6 4 1 3039.39 3205.13 39.32 o -4 4 1 1373.69 1477.21 27.58 o -2 4 1 4936.89 5161.98 47.60 o 0 4 1 467.13 555.25 18.19 o 2 4 1 358.60 380.88 16.50 o 4 4 1 1196.82 1279.28 24.46 o 6 4 1 3978.62 4058.32 43.05 o 8 4 1 2438.16 2637.52 38.16 o 10 4 1 13.29 34.11 9.48 o 12 4 1 1936.13 1915.39 39.97 o 14 4 1 4593.72 4537.19 60.61 o 16 4 1 131.66 170.66 17.80 o 18 4 1 97.88 102.15 17.99 o 20 4 1 137.89 195.49 31.76 o 22 4 1 21.05 46.70 13.43 o 24 4 1 35.01 55.48 23.85 o -23 5 1 1382.97 1344.34 76.94 o -21 5 1 2088.61 2140.37 73.71 o -19 5 1 2705.50 2843.67 63.90 o -17 5 1 4205.85 4361.82 75.90 o -15 5 1 2634.18 2735.80 44.62 o -13 5 1 18262.25 18140.76 135.15 o -11 5 1 15442.54 15462.02 117.33 o -9 5 1 19723.87 20273.53 135.46 o -7 5 1 10248.27 10086.12 83.98 o -5 5 1 2481.83 2446.72 35.77 o -3 5 1 11670.40 11601.06 83.06 o -1 5 1 12536.76 12450.40 79.68 o 1 5 1 13043.18 12732.93 80.19 o 3 5 1 26694.74 26576.42 132.36 o 5 5 1 29812.78 29929.77 288.62 o 7 5 1 25631.67 26121.11 154.42 o 9 5 1 5652.71 5660.59 68.95 o 11 5 1 1820.86 1753.17 36.42 o 13 5 1 4847.40 4955.33 66.12 o 15 5 1 4159.15 4040.35 69.06 o 17 5 1 8443.76 8382.06 96.96 o 19 5 1 1633.66 1580.15 62.66 o 21 5 1 2914.86 2781.96 69.54 o 23 5 1 2124.92 2117.59 80.66 o -22 6 1 273.47 220.75 48.96 o -20 6 1 106.45 125.25 23.06 o -18 6 1 70.88 69.77 11.47 o -16 6 1 45.52 46.16 16.32 o -14 6 1 1421.71 1366.91 35.78 o -12 6 1 392.31 354.88 23.07 o -10 6 1 365.81 411.61 20.68 o -8 6 1 767.88 757.25 25.32 o -6 6 1 691.57 682.38 24.94 o -4 6 1 1985.49 2037.48 37.26 o -2 6 1 824.12 844.30 27.86 o 0 6 1 4818.63 5076.55 55.20 o 2 6 1 138.67 152.97 17.19 o 4 6 1 318.12 289.18 17.44 o 6 6 1 1366.04 1282.06 34.21 o 8 6 1 2842.27 2791.82 56.82 o 10 6 1 475.14 463.46 25.18 o 12 6 1 689.13 652.00 31.68 o 14 6 1 139.50 166.70 18.93 o 16 6 1 277.64 314.41 23.84 o 18 6 1 84.19 69.89 22.81 o 20 6 1 95.06 58.03 21.57 o 22 6 1 411.98 416.73 44.74 o -21 7 1 1067.60 1099.52 80.79 o -19 7 1 3163.81 3280.54 83.42 o -17 7 1 2547.34 2732.59 66.23 o -15 7 1 2350.48 2252.89 60.18 o -13 7 1 5721.17 5721.38 72.44 o -11 7 1 9069.02 9187.80 102.73 o -9 7 1 4932.78 4660.52 64.19 o -7 7 1 3777.68 3740.19 54.93 o -5 7 1 5982.41 6067.05 74.15 o -3 7 1 904.35 889.81 29.48 o -1 7 1 3421.84 3431.65 46.54 o 1 7 1 8652.58 8672.17 74.86 o 3 7 1 8279.95 8227.70 69.67 o 5 7 1 13943.46 14429.77 142.88 o 7 7 1 12024.88 12198.38 122.17 o 9 7 1 4178.97 4223.27 61.86 o 11 7 1 1445.32 1546.68 41.99 o 13 7 1 5201.14 5228.26 75.50 o 15 7 1 4475.95 4724.35 99.35 o 17 7 1 2485.36 2468.56 77.19 o 19 7 1 3699.49 3841.66 118.85 o -18 8 1 22.10 54.21 20.82 o -16 8 1 408.66 362.45 38.32 o -14 8 1 1.40 11.34 13.77 o -12 8 1 24.30 33.55 8.77 o -10 8 1 721.64 712.64 31.05 o -8 8 1 2650.42 2671.08 53.90 o -6 8 1 199.44 192.40 19.32 o -4 8 1 378.47 406.99 27.28 o -2 8 1 1641.63 1585.49 41.76 o 0 8 1 1436.61 1459.90 37.30 o 2 8 1 1211.49 1181.93 32.76 o 4 8 1 678.97 669.35 27.04 o 6 8 1 660.56 608.05 28.22 o 8 8 1 30.77 29.37 9.58 o 10 8 1 150.12 162.36 21.37 o 12 8 1 113.82 112.68 20.89 o 14 8 1 541.80 578.91 45.95 o 16 8 1 290.25 347.06 59.40 o 18 8 1 235.13 165.12 27.95 o -17 9 1 1299.11 1254.18 61.65 o -15 9 1 1629.11 1563.68 66.48 o -13 9 1 3510.13 3339.73 85.24 o -11 9 1 5206.02 5097.91 90.27 o -9 9 1 3252.52 3345.74 73.92 o -7 9 1 5907.58 5804.60 99.30 o -5 9 1 7082.95 7184.12 113.29 o -3 9 1 6484.92 6429.86 89.09 o -1 9 1 3852.01 3916.99 63.45 o 1 9 1 6835.64 7068.15 83.93 o 3 9 1 5969.43 6134.89 78.04 o 5 9 1 4662.48 4927.03 88.64 o 7 9 1 6721.57 6898.94 122.31 o 9 9 1 1500.70 1496.00 60.72 o 11 9 1 1436.47 1460.17 67.33 o 13 9 1 2042.97 2051.64 95.23 o 15 9 1 1381.09 1406.59 70.14 o -12 10 1 63.08 37.61 14.46 o -10 10 1 0.11 28.48 14.61 o -8 10 1 597.44 633.72 45.09 o -6 10 1 242.02 201.41 22.54 o -4 10 1 204.03 140.62 20.28 o -2 10 1 82.02 63.70 18.68 o 0 10 1 61.29 41.96 12.74 o 2 10 1 20.82 46.58 12.42 o 4 10 1 34.67 38.30 23.18 o 6 10 1 724.37 741.82 58.16 o 8 10 1 228.10 282.29 34.47 o 10 10 1 354.36 286.51 54.84 o 12 10 1 48.29 32.62 16.39 o -7 11 1 935.24 844.98 54.38 o -5 11 1 1033.81 945.41 51.22 o -3 11 1 2241.89 2096.98 126.73 o -1 11 1 2458.16 2419.78 78.87 o 1 11 1 795.17 736.54 46.67 o 3 11 1 975.78 977.15 53.56 o 5 11 1 2871.33 3041.78 160.48 o 7 11 1 3144.40 3110.30 123.00 o -26 0 2 1905.49 1630.98 155.07 o -24 0 2 2995.30 2817.52 76.61 o -22 0 2 5937.30 6174.21 131.86 o -20 0 2 3276.71 3185.11 71.27 o -18 0 2 4166.18 4083.89 117.04 o -16 0 2 5298.59 5285.57 98.56 o -14 0 2 5467.73 5801.75 109.76 o -12 0 2 7269.87 7233.24 87.54 o -10 0 2 61875.38 62836.81 361.66 o -8 0 2 21931.29 21908.00 121.80 o -6 0 2 125374.97 122881.36 1275.62 o -4 0 2 134588.27 133750.81 1244.18 o -2 0 2 389.83 446.90 21.09 o 0 0 2 11098.22 11336.51 79.80 o 2 0 2 2852.92 3368.16 67.19 o 4 0 2 57334.95 55396.45 310.22 o 6 0 2 12444.57 11947.57 99.91 o 8 0 2 51370.25 51295.31 493.56 o 10 0 2 15154.09 14680.51 196.24 o 12 0 2 1253.93 1187.97 44.75 o 14 0 2 14045.25 14337.31 164.38 o 16 0 2 55.76 81.71 17.47 o 18 0 2 2436.34 2645.05 81.84 o 20 0 2 9907.08 10369.46 218.33 o 22 0 2 6043.68 6556.57 261.50 o 24 0 2 1854.58 1738.97 99.81 o -27 1 2 107.10 193.81 60.78 o -25 1 2 6.84 40.73 17.03 o -23 1 2 78.40 79.89 12.61 o -21 1 2 0.02 18.38 5.96 o -19 1 2 19.51 15.72 14.60 o -17 1 2 35.48 37.99 7.82 o -15 1 2 1231.42 1289.92 22.72 o -13 1 2 27.55 30.64 8.68 o -11 1 2 1264.05 1349.29 29.09 o -9 1 2 662.12 548.90 21.74 o -7 1 2 265.44 276.71 19.44 o -5 1 2 17573.77 17625.85 100.34 o -3 1 2 1632.68 1869.75 22.26 o -1 1 2 1185.19 1217.45 27.06 o 1 1 2 25091.73 25621.69 105.51 o 3 1 2 1015.84 972.99 20.50 o 5 1 2 7982.41 8360.22 55.43 o 7 1 2 403.61 473.52 23.64 o 9 1 2 1157.40 1258.16 27.17 o 11 1 2 259.96 303.84 19.91 o 13 1 2 132.39 128.13 14.76 o 15 1 2 54.67 57.88 13.64 o 17 1 2 472.33 452.34 26.67 o 19 1 2 253.01 275.93 26.14 o 21 1 2 76.05 131.17 24.94 o 23 1 2 5.50 15.44 17.99 o 25 1 2 8.27 61.65 17.49 o -26 2 2 1765.78 1581.21 119.74 o -24 2 2 7280.14 7247.06 177.53 o -22 2 2 4602.33 4607.04 83.92 o -20 2 2 3808.05 3819.36 57.89 o -18 2 2 4743.92 4748.28 56.10 o -16 2 2 2143.96 2179.80 46.23 o -14 2 2 2704.87 2623.19 48.20 o -12 2 2 2890.82 2767.18 47.23 o -10 2 2 5075.04 4903.50 56.04 o -8 2 2 23064.53 21442.90 148.28 o -6 2 2 55022.15 52923.08 190.96 o -4 2 2 21146.54 20718.83 91.67 o -2 2 2 105.37 115.80 12.03 o 0 2 2 3654.05 3394.67 29.48 o 2 2 2 10335.33 9345.30 58.56 o 4 2 2 23653.43 22850.91 100.44 o 6 2 2 38013.88 37770.41 204.66 o 8 2 2 41913.28 41953.23 198.05 o 10 2 2 26409.12 26845.62 168.24 o 12 2 2 14066.32 13937.40 108.49 o 14 2 2 3901.98 3832.39 64.91 o 16 2 2 1183.45 1211.76 38.45 o 18 2 2 4490.63 4625.07 85.42 o 20 2 2 6066.92 6304.86 146.44 o 22 2 2 4684.79 4706.00 138.92 o 24 2 2 2903.08 2862.30 95.12 o -25 3 2 88.68 85.87 29.14 o -23 3 2 125.18 154.58 27.07 o -21 3 2 665.62 693.26 46.56 o -19 3 2 727.56 768.11 42.85 o -17 3 2 2356.43 2288.40 57.57 o -15 3 2 614.33 569.03 28.06 o -13 3 2 5.74 12.15 17.26 o -11 3 2 1382.83 1273.62 20.33 o -9 3 2 635.18 650.70 17.10 o -7 3 2 5183.91 5480.70 49.00 o -5 3 2 325.90 341.83 16.88 o -3 3 2 1.10 7.86 12.07 o -1 3 2 580.64 668.33 29.94 o 1 3 2 3254.67 3356.82 46.22 o 3 3 2 4404.64 4470.79 44.63 o 5 3 2 13.87 28.43 8.59 o 7 3 2 614.26 600.34 20.13 o 9 3 2 45.36 98.62 13.48 o 11 3 2 434.17 479.87 21.98 o 13 3 2 282.68 332.84 20.62 o 15 3 2 33.16 30.77 10.81 o 17 3 2 82.64 90.24 13.59 o 19 3 2 106.09 104.56 21.37 o 21 3 2 1288.15 1161.44 57.29 o 23 3 2 142.43 142.23 33.02 o -24 4 2 3837.74 3950.43 126.63 o -22 4 2 4443.26 4418.00 107.20 o -20 4 2 6542.18 6700.11 139.93 o -18 4 2 633.78 644.45 46.48 o -16 4 2 6883.79 6853.80 114.00 o -14 4 2 2004.93 2120.58 31.28 o -12 4 2 10676.72 10629.20 88.93 o -10 4 2 15165.28 15410.93 112.63 o -8 4 2 21555.01 20481.60 121.66 o -6 4 2 48811.61 50311.59 220.77 o -4 4 2 12745.52 12349.39 112.67 o -2 4 2 14012.56 14208.19 100.92 o 0 4 2 5096.48 5032.90 61.22 o 2 4 2 12987.83 13291.25 120.18 o 4 4 2 17250.85 16681.71 111.28 o 6 4 2 24121.30 24957.20 144.28 o 8 4 2 10369.21 9789.17 90.61 o 10 4 2 22214.08 23217.01 171.53 o 12 4 2 5701.03 5648.17 61.70 o 14 4 2 3337.49 3345.09 57.40 o 16 4 2 1678.50 1713.35 49.24 o 18 4 2 344.22 360.44 25.62 o 20 4 2 5222.65 5135.38 103.07 o 22 4 2 1446.09 1515.25 66.57 o -23 5 2 503.78 530.15 59.49 o -21 5 2 64.02 121.22 31.40 o -19 5 2 2302.45 2195.93 59.26 o -17 5 2 91.49 103.01 10.93 o -15 5 2 243.76 243.18 21.71 o -13 5 2 996.96 953.58 27.64 o -11 5 2 515.84 540.11 22.64 o -9 5 2 373.23 355.03 18.73 o -7 5 2 1434.17 1530.44 30.77 o -5 5 2 1477.48 1518.78 28.79 o -3 5 2 2.25 29.38 6.62 o -1 5 2 1851.26 1882.18 27.38 o 1 5 2 1472.00 1523.65 22.88 o 3 5 2 434.02 479.26 15.86 o 5 5 2 83.24 93.86 13.90 o 7 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