Acta Crystallographica Section C

Crystal Structure Communications

Volume 62, Part 4 (April 2006)


organic compounds



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gg3003 scheme

Acta Cryst. (2006). C62, o222-o226    [ doi:10.1107/S0108270106006512 ]

Hydrogen-bonded framework structures in 4-[(4-chloro-3-nitrobenzoyl)hydrazinocarbonyl]pyridinium chloride and N-3,5-dinitrobenzoyl-N'-isonicotinoylhydrazine

T. R. A. Vasconcelos, M. V. N. de Souza, S. M. S. V. Wardell, J. L. Wardell, J. N. Low and C. Glidewell

Abstract: In 4-[(4-chloro-3-nitrobenzoyl)hydrazinocarbonyl]pyridinium chloride, C13H10ClN4O4+·Cl-, the component ions are linked into a three-dimensional framework structure by a combination of three N-H...Cl and five C-H...O hydrogen bonds. In N-3,5-dinitrobenzoyl-N'-isonicotinoylhydrazine, C13H9N5O6, the molecules are linked into a three-dimensional framework structure by one N-H...O and three C-H...O hydrogen bonds, augmented by an aromatic [pi]-[pi] stacking interaction.

Formula: C13H10ClN4O4+·Cl- and C13H9N5O6


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Structure factor file (CIF format) (157.2 kbytes)
[ doi:10.1107/S0108270106006512/gg3003Isup2.hkl ]
Contains datablock I


hkldisplay filedownload file

Structure factor file (CIF format) (148.6 kbytes)
[ doi:10.1107/S0108270106006512/gg3003IIsup3.hkl ]
Contains datablock II


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