Crystal Structure Communications

 

Acta Cryst. (2006). C62, i41-i42  [ doi:10.1107/S010827010601273X ]

A hexagonal 2a,c superstructure of Ba₇F₁₂Cl₂

A. Bernsteiner and F. Kubel

Synopsis: A new superstructure of Ba₇F₁₂Cl₂ has been synthesized under hydrothermal conditions.

Formula: Ba_4.67Cl_1.33F₈

Online 16 May 2006

 

Acta Cryst. (2006). C62, i43-i45  [ doi:10.1107/S0108270106008882 ]

Bis(ammonium) tris(hexaaquamagnesium) tetrakis(hydrogen phosphite)

K. I. Abdallah, S. Mohamed, R. Mohamed and G. Abdelhalim

Synopsis: The structure of (NH₄)₂[Mg(H₂O)₆]₃(HPO₃)₄ consists of a compact assembly of [Mg(H₂O)₆]²⁺, HPO₃^2- and NH₄⁺ ions held together by an intricate network of hydrogen bonds.

Formula: (NH₄)₂[Mg(H₂O)₆]₃(HPO₃)₄

Online 24 May 2006

 

Acta Cryst. (2006). C62, i46-i48  [ doi:10.1107/S0108270106011991 ]

PbZn_1/3Nb_2/3O₃ at 4.2 and 295 K

E. H. Kisi, J. S. Forrester and K. S. Knight

Synopsis: The relaxor ferroelectric Pb(Zn_1/3Nb_2/3)O₃, known as PZN, was found to be rhombohedral in R3m at both 4.2 and 295 K from very high resolution neutron powder diffraction data. Atomic coordinates at both temperatures show strong electric polarization.

Formula: PbZn_1/3Nb_2/3O₃

Online 24 May 2006

 

Acta Cryst. (2006). C62, i49-i52  [ doi:10.1107/S0108270106016350 ]

Dirubidium fluorotrioxophosphate, Rb₂PO₃F, at 290 and 130 K, and dicaesium fluorotrioxophosphate, Cs₂PO₃F, at 240 and 100 K

J. Fábry, M. Dusek, K. Fejfarová, R. Krupková, P. Vanek and I. Císarová

Synopsis: The title structures belong to the -K₂SO₄ family. Cs₂PO₃F is twinned owing to the proximity of its lattice parameters to those of the orthohexagonal cell. Phase transitions were observed in slightly humid samples at 175 and 177 K for Rb₂PO₃F and Cs₂PO₃F, respectively, but were not observed in well dried samples.

Formula: Rb₂PO₃F and Cs₂PO₃F

Online 24 May 2006

 

Acta Cryst. (2006). C62, m223-m226  [ doi:10.1107/S0108270106013199 ]

Bis(1-methyl-1H-tetrazol-5-yl)diazene and two its copper(I) chloride complexes poly[[[-1,2-bis(1-methyl-1H-tetrazol-5-yl)diazene-⁴N',N⁴:N,N^4']dicopper(I)]-di--chloro] and catena-poly[[chlorocopper(I)]--1,2-bis(1-methyl-1H-tetrazol-5-yl)diazene-⁴N',N⁴:N,N^4']

A. S. Lyakhov, T. V. Serebryanskaya, P. N. Gaponik, S. V. Voitekhovich and L. S. Ivashkevich

Formula: C₄H₆N₁₀, [Cu₂Cl₂(C₄H₆N₁₀)] and [CuCl(C₄H₆N₁₀)]

Online 16 May 2006

 

Acta Cryst. (2006). C62, m227-m228  [ doi:10.1107/S0108270106014132 ]

(Glycylglycinato-³O,N,N')(2-methyl-1H-benzimidazole-N³)copper(II) trihydrate

L. Li, M.-L. Zhu and L.-P. Lu

Formula: [Cu(C₄H₆N₂O₃)(C₈H₈N₂)]·3H₂O

Online 16 May 2006

 

Acta Cryst. (2006). C62, m229-m231  [ doi:10.1107/S0108270106014090 ]

Arene-perfluoroarene interactions in crystal engineering. XV. Ferrocene-decafluorobiphenyl (1/1)

A. S. Batsanov, J. C. Collings and T. B. Marder

Formula: [Fe(C₅H₅)₂]·C₁₂F₁₀

Online 16 May 2006

 

Acta Cryst. (2006). C62, m232-m233  [ doi:10.1107/S0108270106011826 ]

(Nitrato-²O,O')bis(triethanolamine-⁴N,O,O',O'')lanthanum(III) dinitrate

A. Fowkes and W. T. A. Harrison

Formula: [La(NO₃)(C₆H₁₅NO₃)₂](NO₃)₂

Online 16 May 2006

 

Acta Cryst. (2006). C62, m234-m237  [ doi:10.1107/S0108270106014429 ]

The diprotonated 2,2-(propane-1,3-diyl)bis(1,1,3,3-tetramethylguanidinium) cation: packing and conformational changes

U. Flörke, S. Herres-Pawlis, A. Heuwing, A. Neuba, O. Seewald and G. Henkel

Formula: Four C₁₃H₃₂N₆²⁺ salts

Online 16 May 2006

 

Acta Cryst. (2006). C62, m238-m240  [ doi:10.1107/S0108270106014417 ]

Octakis(3-propylammonium) octadecaiodopentaplumbate(II): a new layered stucture based on layered perovskites

D. G. Billing and A. Lemmerer

Formula: (C₃H₁₀N)₈[Pb₅I₁₈]

Online 16 May 2006

 

Acta Cryst. (2006). C62, m241-m242  [ doi:10.1107/S0108270106011590 ]

Sodium 2-oxo-3-semicarbazono-2,3-dihydro-1H-indole-5-sulfonate dihydrate

G. Pelosi, M. Belicchi Ferrari, M. C. Rodríguez-Argüelles, S. Mosquera-Vázquez and J. Sanmartín

Formula: Na⁺·C₉H₇N₄O₅S^-·2H₂O

Online 16 May 2006

 

Acta Cryst. (2006). C62, m243-m245  [ doi:10.1107/S0108270106014934 ]

(18-Crown-6)--oxo-hexakis(tetrahydroborato)diuranium(IV): an unprecedented asymmetric dinuclear complex

C. Villiers, P. Thuéry and M. Ephritikhine

Formula: [U₂(BH₄)₆O(C₁₂H₂₄O₆)]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m246-m248  [ doi:10.1107/S010827010601523X ]

A heterotrimetallic Cu-Co-Zn complex with the 2,2'-iminodiethanol ligand

D. S. Nesterov, V. N. Kokozay and B. W. Skelton

Formula: [CoCuZn(C₄H₉NO₂)₂(C₂H₃O₂)₃(C₄H₁₁NO₂)]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m249-m251  [ doi:10.1107/S0108270106013503 ]

cis-Amminedichloroisopropylamineplatinum(II) by X-ray powder diffraction analysis

S. D. Kirik, A. K. Starkov and G. A. Kozhuhovskay

Formula: [PtCl₂(C₃H₉N)(NH₃)]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m252-m254  [ doi:10.1107/S0108270106016052 ]

Bromo(⁴-cycloocta-1,5-diene)[1-(2,3,4,5,6-pentafluorobenzyl)-3-(2,4,6-trimethylbenzyl)benzimidazol-2-ylidene]rhodium(I)

M. Dinçer, N. Özdemir, S. Gülcemal, B. Çetinkaya and O. Büyükgüngör

Formula: [RhBr(C₈H₁₂)(C₂₄H₁₉F₅N₂)]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m255-m257  [ doi:10.1107/S0108270106016726 ]

Poly[(₂-1,3-di-4-pyridylpropane-²N:N')(₃-glutarato-³O:O':O'')dizinc(II)]

Q.-W. Zhang, Y.-H. Wen and Y.-L. Feng

Formula: [Zn₂(C₅H₆O₄)₂(C₁₃H₁₄N₂)]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m258-m260  [ doi:10.1107/S0108270106014582 ]

Poly[tetraaquadi-₃-malonato-calcium(II)zinc(II)]

X.-C. Fu, M.-T. Li, X.-Y. Wang, C.-G. Wang and X.-T. Deng

Formula: [CaZn(C₃H₂O₄)₂(H₂O)₄]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m261-m263  [ doi:10.1107/S0108270106013412 ]

An extended two-dimensional copper-molybdate compound with mixed dicarboxyl and organodiamine ligands

X.-Y. Wu, Q.-G. Zhai, L.-J. Chen and C.-Z. Lu

Formula: [Cu₂Mo₄(C₈H₄O₄)O₁₃(C₁₂H₈N₂)₂]

Online 24 May 2006

 

Acta Cryst. (2006). C62, m264-m266  [ doi:10.1107/S0108270106016167 ]

catena-Poly[bis(tert-butylammonium) [plumbate(II)-tri--iodo] iodide dihydrate]

D. G. Billing and A. Lemmerer

Formula: (C₄H₁₂N)₂[PbI₃]I·2H₂O

Online 24 May 2006

 

Acta Cryst. (2006). C62, m267-m268  [ doi:10.1107/S0108270106016398 ]

Aqua(di-2-pyridylamine)oxalatocopper(II) monohydrate

S. Youngme, J. Phatchimkun and N. Chaichit

Formula: [Cu(C₂O₄)(C₁₀H₉N₃)(H₂O)]·H₂O

Online 24 May 2006

 

Acta Cryst. (2006). C62, o307-o309  [ doi:10.1107/S0108270106013138 ]

2-Formylbenzonitrile

D. Britton and C. J. Cramer

Formula: C₈H₅NO

Online 16 May 2006

 

Acta Cryst. (2006). C62, o310-o311  [ doi:10.1107/S0108270106013461 ]

The cocrystal of 3-hydroxy-2-naphthoic acid and 4,4'-bipyridine

B.-Y. Lou, X.-D. Huang and X.-C. Lin

Formula: C₁₁H₈O₃·0.5C₁₀H₈N₂

Online 16 May 2006

 

Acta Cryst. (2006). C62, o312-o314  [ doi:10.1107/S0108270106013473 ]

Formation of ladders from R₄⁴(8) and R₆⁶(12) rings in 8-hydroxyquinolinium chloride monohydrate: comparisons with the supramolecular arrangements in related salts

J. M. S. Skakle, J. L. Wardell and S. M. S. V. Wardell

Formula: C₉H₈NO⁺·Cl^-·H₂O

Online 16 May 2006

 

Acta Cryst. (2006). C62, o315-o317  [ doi:10.1107/S0108270106013175 ]

A novel potent non-nucleoside reverse transcriptase inhibitor acylthiocarbamate derivative with extensive intramolecular - interactions

A. Mugnoli, A. Borassi, A. Spallarossa and S. Cesarini

Formula: C₂₅H₁₉N₃O₆S

Online 16 May 2006

 

Acta Cryst. (2006). C62, o318-o320  [ doi:10.1107/S0108270106013114 ]

2,4-Dinitrophenylhydrazine, redetermined at 120 K: a three-dimensional framework built from N-HO, N-H(O)₂, N-H(arene) and C-HO hydrogen bonds

J. L. Wardell, J. N. Low and C. Glidewell

Formula: C₆H₆N₄O₄

Online 16 May 2006

 

Acta Cryst. (2006). C62, o321-o323  [ doi:10.1107/S0108270106014284 ]

Hydrogen-bonded chains of rings linked by iodo-carbonyl interactions in 5-iodoisatin and hydrogen-bonded sheets in 7-trifluoromethylisatin

S. J. Garden, A. C. Pinto, J. L. Wardell, J. N. Low and C. Glidewell

Formula: C₈H₄INO₂ and C₉H₄F₃NO₂

Online 16 May 2006

 

Acta Cryst. (2006). C62, o324-o327  [ doi:10.1107/S0108270106013874 ]

Sheets built from C-HO and C-H(arene) hydrogen bonds in (2RS,6SR)-N-diphenylacetyl-2,6-diphenylpiperidin-4-one and (2RS,3SR,5RS,6SR)-3,5-dimethyl-N-phenylacetyl-2,6-diphenylpiperidin-4-one

K. Thanikasalam, R. Jeyaraman, K. Panchanatheswaran, J. N. Low and C. Glidewell

Formula: C₃₁H₂₇NO₂ and C₂₇H₂₇NO₂

Online 16 May 2006

 

Acta Cryst. (2006). C62, o328-o330  [ doi:10.1107/S0108270106014491 ]

L-Phenylalanyl-L-tryptophan 0.75-hydrate

C. H. Görbitz

Formula: C₂₀H₂₁N₃O₃·0.75H₂O

Online 16 May 2006

 

Acta Cryst. (2006). C62, o331-o332  [ doi:10.1107/S0108270106014223 ]

(1Z,2Z)-1,2-Bis(3-methyl-2,3-dihydro-1,3-benzothiazol-2-ylidene)hydrazine

T. Nakano, H. Kakuda, Y. Mori and M. Shiro

Formula: C₁₆H₁₄N₄S₂

Online 24 May 2006

 

Acta Cryst. (2006). C62, o333-o335  [ doi:10.1107/S0108270106013527 ]

Three chiral vinyldioxazaborocanes

M. M. Olmstead, J. C. Fettinger, S. Gamsey, J. W. Clary and B. Singaram

Formula: C₂₇H₃₀BNO₂, C₂₄H₃₂BNO₂ and C₂₇H₃₀BNO₂

Online 24 May 2006

 

Acta Cryst. (2006). C62, o336-o338  [ doi:10.1107/S0108270106015174 ]

Hydrogen-bonded 1:1 adduct of 1,1'-(p-phenylene)dipyridin-4(1H)-one with terephthalic acid

C. Li, P. D. Robinson and D. J. Dyer

Formula: C₁₆H₁₂N₂O₂·C₈H₆O₄

Online 24 May 2006

 

Acta Cryst. (2006). C62, o339-o343  [ doi:10.1107/S010827010601420X ]

cis-(6RS,13RS)-3,3,10,10-Tetramethyl-6,13-diphenyl-1,8-dioxa-4,11-diazacyclotetradecane-2,5,9,12-tetraone and two of its precursors

A. Linden, B. Iliev and H. Heimgartner

Formula: C₁₃H₁₇NO₄, C₁₃H₁₅NO₃ and C₂₆H₃₀N₂O₆

Online 24 May 2006

 

Acta Cryst. (2006). C62, o344-o345  [ doi:10.1107/S0108270106015460 ]

Molecular packing in (5-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-yl)acetamide

T. Borowiak, G. Dutkiewicz and J. Spychala

Formula: C₇H₉N₃O₃

Online 24 May 2006

 

Acta Cryst. (2006). C62, o346-o349  [ doi:10.1107/S0108270106016374 ]

Solid-state architecture of saccharin salts of some diamines

R. Banerjee, B. K. Saha and G. R. Desiraju

Formula: H₅N₂⁺·C₇H₄NO₃S^-, C₂H₁₀N₂²⁺·2C₇H₄NO₃S^- and C₄H₁₄N₂²⁺·2C₇H₄NO₃S^-

Online 24 May 2006

 

Acta Cryst. (2006). C62, o350-o352  [ doi:10.1107/S0108270106017409 ]

Mammeigin

A. C. Doriguetto, J. Ellena, M. H. Dos Santos, M. E. C. Moreira and T. J. Nagem

Formula: C₂₅H₂₄O₅

Online 24 May 2006

 

Acta Cryst. (2006). C62, o353-o357  [ doi:10.1107/S0108270106017288 ]

Brucine salts of L--hydroxy acids: brucinium hydrogen (S)-malate pentahydrate and anhydrous brucinium hydrogen (2R,3R)-tartrate at 130 K

G. Smith, U. D. Wermuth and J. M. White

Formula: C₂₃H₂₇N₂O₄⁺·C₄H₅O₅^-·5H₂O and C₂₃H₂₇N₂O₄⁺·C₄H₅O₆^-

Online 24 May 2006

 

Acta Cryst. (2006). C62, o358-o361  [ doi:10.1107/S0108270106015149 ]

Two salts of di-p-toluoyltartaric acid with aromatic amines

L. R. Nassimbeni and H. Su

Formula: 2C₈H₁₂N⁺·C₂₀H₁₆O₈^2-·2CH₄O·H₂O and 2C₇H₁₀N⁺·C₂₀H₁₆O₈^2-·2H₂O

Online 31 May 2006

 

Acta Cryst. (2006). C62, o362-o363  [ doi:10.1107/S0108270106012571 ]

Form I of desloratadine, a tricyclic antihistamine

P. M. Bhatt and G. R. Desiraju

Formula: C₁₉H₁₉ClN₂

Online 31 May 2006

 

Acta Cryst. (2006). C62, o364-o368  [ doi:10.1107/S0108270106017598 ]

Four 2-aryl-8,8-dimethyl-6,7,8,9-tetrahydropyrazolo[2,3-a]quinazolin-6-ones: isolated molecules, hydrogen-bonded dimers, and -stacked chains of hydrogen-bonded dimers

S. Cruz, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C₁₉H₁₈ClN₃O, C₂₀H₂₁N₃O₂, C₂₄H₂₀ClN₃O and C₁₉H₁₉N₃O·H₂O

Online 31 May 2006