Acta Crystallographica Section C

Crystal Structure Communications

Volume 62, Part 7 (July 2006)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: A view of (borohydrido)(dibenzo-18-crown-6)(tetrahydrofuran)potassium, showing the atom-numbering scheme. Displacement ellipsoids are drawn at the 30% probability level and H atoms are shown as small spheres of arbitrary radii. See Villiers, Thuéry & Ephritikhine [Acta Cryst. (2006), C62, m275-m277].

inorganic compounds


 

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Acta Cryst. (2006). C62, i53-i56  [ doi:10.1107/S0108270106014880 ]

Rubidium dimolybdate, Rb2Mo2O7, and caesium dimolybdate, Cs2Mo2O7

Z. A. Solodovnikova and S. F. Solodovnikov

Synopsis: Rb2Mo2O7 and Cs2Mo2O7 represent new structure types with infinite chains of linked MoO4 tetrahedra and MoO6 octahedra. The chains in Cs2Mo2O7 resemble those in the Na2Mo2O7 structure. The orthorhombic pseudosymmetry of Cs2Mo2O7 implies a possible high-temperature transition P21/c[rightwards arrow]Pbca.

Formula: Rb2Mo2O7 and Cs2Mo2O7

Online 15 June 2006


 

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Acta Cryst. (2006). C62, i57-i58  [ doi:10.1107/S0108270106017586 ]

Ca0.8Y2.4Sn0.8O6, a quaternary oxide with mixed occupations of Ca/Y and Y/Sn

Y. Kaminaga, H. Yamane and T. Yamada

Synopsis: A new compound in the CaO-Y2O3-SnO2 system, Ca0.8Y2.4Sn0.8O6, is isotypic with Mg3TeO6 and crystallizes in the trigonal space group R{\\overline 3}. All cations are in sixfold coordination sites.

Formula: Ca0.8O6Sn0.8Y2.4

Online 15 June 2006


 

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Acta Cryst. (2006). C62, i59-i60  [ doi:10.1107/S0108270106017719 ]

Hexafluoroiodium(VII) hexafluoroarsenate

E. Goreshnik and Z. Mazej

Synopsis: IF6AsF6 crystallizes in the cubic space group Pa\\overline{3} with a simple NaCl-like ionic packing. The I and As atoms occupy the 4a and 4b Wyckoff positions, respectively, with \\overline{3} symmetry.

Formula: AsF12I

Online 15 June 2006


 

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Acta Cryst. (2006). C62, i61-i63  [ doi:10.1107/S0108270106016180 ]

Commensurate monoclinic form of Ca2Zn0.97Co0.03Ge2O7

G. J. Redhammer and G. Roth

Synopsis: The structure of the monoclinic form of dicalcium zinc germanate, obtained by slow cooling from the melt, is described and compared with that of the tetragonal form and with monoclinic Ca2ZnGe1.25Si0.75O7.

Formula: Ca2Zn0.97Co0.03Ge2O7

Online 30 June 2006


 

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Acta Cryst. (2006). C62, i64-i66  [ doi:10.1107/S0108270106021329 ]

Préparation et étude structurale de NH4Gd(PO3)4 et NH4GdP4O12

E. Ben Zarkouna, A. Driss and M. Férid

Synopsis: Chaque polyèdre GdO8 partage ses sommets avec quatre rubans (PO3)n dans le polyphosphate et six cycles P4O12 dans le cyclotétraphosphate. Ces assemblages forment des tunnels dans lesquels résident les ions NH4+.

Formula: NH4GdP4O12 et NH4Gd(PO3)4

Online 30 juin 2006


metal-organic compounds


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Acta Cryst. (2006). C62, m269-m271  [ doi:10.1107/S0108270106013953 ]

Poly[bis[2-(1-cyclohexenyl)ethylammonium] di-[mu]-iodo-diodoplumbate(II)]

D. G. Billing and A. Lemmerer

Formula: (C8H16N)2[PbI4]

Online 15 June 2006


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Acta Cryst. (2006). C62, m272-m274  [ doi:10.1107/S0108270106014788 ]

Iodo(picolinato-[kappa]2N,O)(picolinic acid-[kappa]2N,O)mercury(II)

Z. Popovic, G. Pavlovic and Z. Soldin

Formula: [Hg(C6H4NO2)I(C6H5NO2)]

Online 15 June 2006


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Acta Cryst. (2006). C62, m275-m277  [ doi:10.1107/S0108270106016507 ]

(Borohydrido)(18-crown-6)potassium and (borohydrido)(dibenzo-18-crown-6)(tetrahydrofuran)potassium

C. Villiers, P. Thuéry and M. Ephritikhine

Formula: [K(BH4)(C12H24O6)] and [K(BH4)(C4H8O)(C20H24O6)]

Online 15 June 2006


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Acta Cryst. (2006). C62, m278-m280  [ doi:10.1107/S0108270106018191 ]

Decamethylferrocenium bis(2-oxo-1,3-dithiole-4,5-dithiolato-[kappa]2S4,S5)nickelate(III) tetrahydrofuran solvate

S. Rabaça, I. C. Santos, M. T. Duarte and V. Gama

Formula: [Fe(C10H15)2][Ni(C3OS4)2]·C4H8O

Online 15 June 2006


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Acta Cryst. (2006). C62, m281-m283  [ doi:10.1107/S0108270106017720 ]

A three-dimensional framework of bis[tris(ethylenediamine)zinc] tetraiodocadmate diiodide assisted by N-H...I hydrogen bonds

O. V. Nesterova, S. R. Petrusenko, V. V. Dyakonenko, O. V. Shishkin and W. Linert

Formula: [Zn(C2H8N2)3][CdI4]I2

Online 15 June 2006


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Acta Cryst. (2006). C62, m284-m289  [ doi:10.1107/S0108270106018531 ]

Variation of hydrogen-bonded networks in hexafluorophosphate salts of amidate-bridged dirhodium(II,III) complexes with axial aqua ligands

M. Ebihara and Y. Fuma

Formula: [Rh2(C2H4NO)4(H2O)2]PF6, [Rh2(C2H4NO)4(H2O)2]PF6·2H2O, [Rh2(C3H6NO)4(H2O)2]PF6·2H2O and [Rh2(C4H8NO)4(H2O)2]PF6

Online 15 June 2006


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Acta Cryst. (2006). C62, m290-m292  [ doi:10.1107/S0108270106019469 ]

Bis(6-thioxo-1,6-dihydropurinium) tetrachlorozincate(II)

A. Valkonen, K. Ahonen and E. Kolehmainen

Formula: (C5H5N4S)2[ZnCl4]

Online 23 June 2006


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Acta Cryst. (2006). C62, m293-m296  [ doi:10.1107/S0108270106018695 ]

{Bis(3,5-Di-tert-butyl-2-oxidobenzyl)[2-(N,N-dimethylamino)ethyl]amine-[kappa]4N,N',O,O'}zinc(II) and {bis(3-tert-butyl-5-methyl-2-oxidobenzyl)[2-(N,N-dimethylamino)ethyl]amine-[kappa]4N,N',O,O'}(tetrahdyrofuran)zinc(II)

R. H. Howard, M. Bochmann and J. A. Wright

Formula: [Zn(C34H54N2O2)] and [Zn(C28H42N2O2)(C4H8O)]

Online 23 June 2006


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Acta Cryst. (2006). C62, m297-m302  [ doi:10.1107/S0108270106020087 ]

Two oxo complexes with tetranuclear [Fe4([mu]3-O)2]8+ and trinuclear [Fe3([mu]3-O)]7+ units

P. Cortés, A. M. Atria, M. T. Garland and R. Baggio

Formula: [Fe4(C2H3O2)7O2(C10H9N3)2(H2O)]Cl·1.25C2H6O·H2O and (C4H7N2)[Fe3(C2H3O2)7O(H2O)2]Cl·2H2O

Online 23 June 2006


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Acta Cryst. (2006). C62, m303-m305  [ doi:10.1107/S0108270106019317 ]

Two germatranes with bulky substituents

A. A. Korlyukov, E. A. Komissarov, N. V. Alekseev, K. V. Pavlov, O. V. Krivolapova and V. G. Lachtin

Formula: [Ge(C10H15)(C6H12NO3)] and [Ge(C6H12NO3)(C8H14NO2)]

Online 23 June 2006


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Acta Cryst. (2006). C62, m306-m310  [ doi:10.1107/S0108270106021470 ]

Two polymorphs of potassium trichloro[diethyl (methylsulfinylmethyl)phosphonate-[kappa]S]platinum(II) with Z' = 1 and 3 in the space group P212121

C. Pacifico, M. Laforgia, F. P. Intini, G. Padovano and G. Natile

Formula: Two polymorphs of K[PtCl3(C6H15O4PS)]

Online 30 June 2006


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Acta Cryst. (2006). C62, m311-m314  [ doi:10.1107/S0108270106021354 ]

Three oxo complexes with a tetranuclear [Cu4([mu]2-Cl)6([mu]4-O)] unit

P. Cortés, A. M. Atria, M. T. Garland and R. Baggio

Formula: (C9H9N2)[Cu4Cl7O(C9H8N2)3]·H2O, [Cu4Cl6O(C5H5NO)4] and [Cu4Cl6O(C4H6N2)4]·3CH4O

Online 30 June 2006


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Acta Cryst. (2006). C62, m315-m318  [ doi:10.1107/S010827010601969X ]

Dichloro[(1E,1'E)-1,1'-(pyridine-2,6-diyl)diethanone bis(O-methyloxime)-[kappa]3N1,N2,N6]copper(II)

N. Özdemir, M. Dinçer, O. Dayan and B. Çetinkaya

Formula: [CuCl2(C11H15N3O2)]

Online 30 June 2006


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Acta Cryst. (2006). C62, m319-m322  [ doi:10.1107/S0108270106018932 ]

Transition metal complexes with thiosemicarbazide-based ligands. LIII. [4-(2-Diphenylphosphino-[alpha]-ethoxybenzyl-[kappa]P)-S-methyl-1-(4-oxidopent-3-en-4-ylidene-[kappa]O)thiosemicarbazido-[kappa]2N1,N4]nickel(II)

B. M. Draskovic, G. A. Bogdanovic, V. M. Leovac, I. D. Brceski and D. Poleti

Formula: [Ni(C28H30N3O2PS)]

Online 30 June 2006


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Acta Cryst. (2006). C62, m323-m326  [ doi:10.1107/S010827010601910X ]

Tetrakis[phthalocyaninato(2-)antimony(III)] docosaiodohexaantimony(III)

J. Janczak and G. J. Perpétuo

Formula: [Sb(C32H16N8)]4[Sb6I22]

Online 30 June 2006


organic compounds


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Acta Cryst. (2006). C62, o369-o371  [ doi:10.1107/S0108270106017422 ]

Two polymorphs of N,N'-diphenethylterephthalamide

J. Ossowski, P. Kus, C. Näther and P. G. Jones

Formula: C24H24N2O2

Online 15 June 2006


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Acta Cryst. (2006). C62, o372-o375  [ doi:10.1107/S0108270106015873 ]

Two crystals of doubly protonated melaminium salts: melaminium bis(trifluoroacetate) trihydrate and melaminium bis(trichloroacetate) dihydrate

G. J. Perpétuo and J. Janczak

Formula: C3H8N62+·2C2F3O2-·3H2O and C3H8N62+·2C2Cl3O2-·2H2O

Online 15 June 2006


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Acta Cryst. (2006). C62, o376-o378  [ doi:10.1107/S0108270106017707 ]

2-Bromo-1,3-bis(bromomethyl)benzene, with Z' = 1.5: whole-molecule disorder of one of the two independent molecules

P. Kirsop, J. M. D. Storey and W. T. A. Harrison

Formula: C8H7Br3

Online 15 June 2006


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Acta Cryst. (2006). C62, o379-o381  [ doi:10.1107/S010827010601818X ]

7-Deaza-2,8-diazaadenosine

W.-Q. Lin, X. Ming, H. Eickmeier and F. Seela

Formula: C9H12N6O4

Online 15 June 2006


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Acta Cryst. (2006). C62, o382-o385  [ doi:10.1107/S0108270106018038 ]

Three substituted (Z)-5-benzylidene-2-thioxothiazolidin-4-ones: hydrogen-bonded dimers that can be effectively isolated or linked into chains either by aromatic [pi]-[pi] stacking interactions or by dipolar carbonyl-carbonyl interactions

P. Delgado, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C10H6FNOS2, C10H6FNOS2 and C13H13NO4S2

Online 15 June 2006


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Acta Cryst. (2006). C62, o386-o388  [ doi:10.1107/S0108270106004677 ]

4-(4-Chlorophenyl)-3-(4-phenylpent-4-enyloxy)-1,3-thiazole-2(3H)-thione

J. Hartung, M. Schwarz, E. F. Paulus, I. Svoboda and H. Fuess

Formula: C20H18ClNOS2

Online 15 June 2006


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Acta Cryst. (2006). C62, o389-o393  [ doi:10.1107/S0108270106017252 ]

(Z)-6-{[1,3-Dihydroxy-2-(hydroxymethyl)propan-2-yliminio]methyl}-2-ethoxyphenolate, (Z)-6-{[1,3-dihydroxy-2-(hydroxymethyl)propan-2-yliminio]methyl}-4-nitratocyclohexa-2,4-dienone monohydrate and (R,E)-2-[(1-hydroxybutan-2-ylimino)methyl]phenol

S. Yüce, Ç. Albayrak, M. Odabasoglu and O. Büyükgüngör

Formula: C13H19NO5, C11H14N2O6·H2O and C11H15NO2

Online 15 June 2006


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Acta Cryst. (2006). C62, o394-o396  [ doi:10.1107/S010827010601136X ]

(-)-3,7-Dioxo-5[beta]-cholanic acid: dual hydrogen-bonding modes in a diketonic bile-acid derivative

E. M. Kikolski, R. A. Lalancette and H. W. Thompson

Formula: C24H36O4

Online 15 June 2006


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Acta Cryst. (2006). C62, o397-o398  [ doi:10.1107/S0108270106017677 ]

(+)-3,11-Dioxo-5[alpha]-androstanecarboxylic acid: catemeric hydrogen bonding in a steroidal diketo acid

E. M. Kikolski, H. W. Thompson and R. A. Lalancette

Formula: C20H28O4

Online 15 June 2006


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Acta Cryst. (2006). C62, o399-o401  [ doi:10.1107/S0108270106018397 ]

Cadaverinium dichloride: a case of centro-non-centrosymmetric ambiguity

I. Pospieszna-Markiewicz, W. Radecka-Paryzek and M. Kubicki

Formula: C5H16N22+·2Cl-

Online 15 June 2006


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Acta Cryst. (2006). C62, o402-o404  [ doi:10.1107/S010827010601821X ]

Mixed dicationic and monocationic benzidine species in the proton-transfer compound of benzidine with 3,5-dinitrosalicylic acid

G. Smith, U. D. Wermuth and J. M. White

Formula: C12H14N22+·2C12H13N2+·4C7H3N2O7-·2C2H6O

Online 15 June 2006


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Acta Cryst. (2006). C62, o405-o409  [ doi:10.1107/S0108270106017811 ]

Different nucleobase orientations in two cyclic 2',3'-phosphates of purine ribonucleosides: Et3NH(2',3'-cAMP) and Et3NH(2',3'-cGMP)·H2O

K. Sieroslawski, K. Slepokura, T. Lis, M. Bogucka, J. Lutomska and A. Kraszewski

Formula: C6H16N+·C10H11N5O6P- and C6H16N+·C10H11N5O7P-·H2O

Online 15 June 2006


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Acta Cryst. (2006). C62, o410-o411  [ doi:10.1107/S010827010601866X ]

3,3'-Dihydroxy-5,5,5',5'-tetramethyl-2,2'-thiodicyclohex-2-en-1-one

F. Imashiro

Formula: C16H22O4S

Online 23 June 2006


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Acta Cryst. (2006). C62, o412-o415  [ doi:10.1107/S0108270106019688 ]

5-Fluorouracil and thymine form a crystalline solid solution

S. A. Barnett, A. T. Hulme and D. A. Tocher

Formula: Three forms of C4H3FN2O2·C5H6N2O2

Online 23 June 2006


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Acta Cryst. (2006). C62, o416-o418  [ doi:10.1107/S0108270106019238 ]

2-(4-Hydroxyphenyl)-4,4-dimethyl-2-oxazoline: X-ray and density functional theory study

V. Langer, D. Gyepesová, E. Scholtzová, J. Luston, J. Kronek and M. Koós

Formula: C11H13NO2

Online 23 June 2006


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Acta Cryst. (2006). C62, o419-o422  [ doi:10.1107/S0108270106019664 ]

2,2',3,3',4,4',5,5',6,6'-Decafluorodiphenylamine and its 1:1 cocrystal with diphenylamine

M. Grzegorczyk and M. Gdaniec

Formula: C12HF10N and C12HF10N·C12H11N

Online 23 June 2006


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Acta Cryst. (2006). C62, o423-o425  [ doi:10.1107/S0108270106019408 ]

4-Iodo-N,N-bis(2-nitrophenylsulfonyl)aniline: a three-dimensional framework structure built from six independent C-H...O hydrogen bonds

J. N. Low, J. M. S. Skakle, J. L. Wardell and C. Glidewell

Formula: C18H12IN3O8S2

Online 23 June 2006


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Acta Cryst. (2006). C62, o426-o428  [ doi:10.1107/S0108270106018373 ]

Pyridoxinium picrate

K. Anitha, S. Athimoolam and S. Natarajan

Formula: C8H12NO3+·C6H2N3O7-

Online 23 June 2006


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Acta Cryst. (2006). C62, o429-o431  [ doi:10.1107/S0108270106020567 ]

4-Benzoyloxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide 1,1-dioxide

T. N. Drebushchak, N. N. Pankrushina, T. P. Shakhtshneider and S. A. Apenina

Formula: C22H17N3O5S

Online 23 June 2006


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Acta Cryst. (2006). C62, o432-o434  [ doi:10.1107/S0108270106018336 ]

(1SR,2SR,3SR,4RS,5RS,6RS,7SR,8RS)-7,8-Dichlorobicyclo[4.2.0]octa-2,3,4,5-tetrayl tetraacetate

E. Sahin, L. Kelebekli, Y. Kara and M. Balci

Formula: C16H20Cl2O8

Online 23 June 2006


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Acta Cryst. (2006). C62, o435-o437  [ doi:10.1107/S0108270106016520 ]

1-(1-Amino-4-bromo-9,10-dioxo-9,10-dihydroanthracen-2-ylcarbonyl)-1,3-dicyclohexylurea

L. Wu, H.-M. Liu, W.-T. Zhao and W.-Q. Zhang

Formula: C28H30BrN3O4

Online 23 June 2006


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Acta Cryst. (2006). C62, o438-o440  [ doi:10.1107/S0108270106015915 ]

1,2-Bis(diphenylphosphino)benzene and two related mono-methiodides, [o-C6H4(PR2)(PR2Me)]I (R = Ph or Me)

W. Levason, G. Reid and M. Webster

Formula: C30H24P2, C31H27P2+·I- and C11H19P2+·I-

Online 30 June 2006


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Acta Cryst. (2006). C62, o441-o443  [ doi:10.1107/S0108270106020373 ]

N-(2-Hydroxy-3-iodo-5-nitrobenzylidene)-3-nitroaniline: conformational isomers linked into complex sheets by five C-H...O hydrogen bonds and a two-centre iodo-nitro interaction

J. N. Low, J. M. S. Skakle, S. J. Garden, J. L. Wardell and C. Glidewell

Formula: C13H8IN3O5

Online 30 June 2006


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Acta Cryst. (2006). C62, o444-o446  [ doi:10.1107/S0108270106020634 ]

2,4-Dimethylbenzaldehyde isonicotinoylhydrazone trihydrate: a three-dimensional hydrogen-bonded framework structure

J. N. Low, S. M. S. V. Wardell, M. V. N. de Souza, J. L. Wardell and C. Glidewell

Formula: C15H15N3O·3H2O

Online 30 June 2006


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