Acta Crystallographica Section C

Crystal Structure Communications

Volume 62, Part 8 (August 2006)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: A packing view of bis(iminodiethylenediammonium) di-[mu]5-hydrogenphosphato-pentamolybdate(VI) tetrahydrate along the b axis, showing the arrangement of the [Mo5O15(HPO4)2]4- clusters (polyhedra), the (H2tren)2+ cations and the solvent water molecules in the crystal structure. The dashed lines denote the hydrogen-bonding interactions, and H atoms not involved in such interactions have been omitted for clarity. See Geng, Han & Lin [Acta Cryst.(2006), C62, m355-m357].

inorganic compounds


 

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Acta Cryst. (2006). C62, i67-i69  [ doi:10.1107/S010827010602347X ]

A new synthetic cobalt tellurate: Co3TeO6

R. Becker, M. Johnsson and H. Berger

Synopsis: The title structure is based on a (hhc)2 oxygen packing with TeVI atoms in octahedral sites and CoII atoms in octahedral as well as tetrahedral sites.

Formula: Co3TeO6

Online 22 July 2006


 

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Acta Cryst. (2006). C62, i70-i72  [ doi:10.1107/S0108270106014879 ]

Redetermination of the lanthanum iron sulfide La52Fe12S90

A. M. Mills, D. Bräunling and M. Ruck

Synopsis: A redetermination of the structure of `La32.66Fe11S60' in the trigonal space group R\\overline{3}m led to the new formula La52Fe12S90 and to a redefinition of the structure type.

Formula: La52Fe12S90

Online 22 July 2006


metal-organic compounds


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Acta Cryst. (2006). C62, m327-m330  [ doi:10.1107/S0108270106022438 ]

Propynylferrocene and (phenylethynyl)ferrocene

M. Zora, C. Açikgöz, T. A. Tumay, M. Odabasoglu and O. Büyükgüngör

Formula: [Fe(C5H5)(C8H7)] and [Fe(C5H5)(C13H9)]

Online 14 July 2006


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Acta Cryst. (2006). C62, m331-m333  [ doi:10.1107/S0108270106022323 ]

Tris(ethylenediamine)nickel(II) bis[2-cyano-2-(oxidoimino)acetamidato]nickelate(II) monohydrate

A. I. Buvaylo, N. M. Dudarenko, I. O. Fritsky and J. Swiatek-Kozlowska

Formula: [Ni(C2H8N2)3][Ni(C3HN3O2)2]·H2O

Online 14 July 2006


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Acta Cryst. (2006). C62, m334-m336  [ doi:10.1107/S0108270106020968 ]

Poly[[[bis(N,N'-dimethylformamide)zinc(II)]-[mu]3-5-hydroxybenzene-1,3-dicarboxylato] toluene solvate]

Y. H. Jhon and J. Kim

Formula: [Zn(C8H4O5)(C3H7NO)2]·0.5C7H8

Online 14 July 2006


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Acta Cryst. (2006). C62, m337-m339  [ doi:10.1107/S0108270106015769 ]

Hexakis[tris(ethylenediamine-[kappa]2N,N')nickel(II)] tricyanocuprate(I) bis{[mu]-cyano-bis[tricyanocuprate(I)]} nonahydrate

J. Kuchár, J. Cernák and W. Massa

Formula: [Ni(C2H8N2)3]6[Cu(CN)3][Cu2(CN)7]2·9H2O

Online 14 July 2006


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Acta Cryst. (2006). C62, m340-m342  [ doi:10.1107/S010827010601924X ]

Red and yellow solvates of chloro(2,2':6',2''-terpyridine)platinum(II) chloride and Pt...Pt interactions

C. S. Angle, A. G. DiPasquale, A. L. Rheingold and L. H. Doerrer

Formula: [PtCl(C15H11N3)]Cl·C2H6OS and [PtCl(C15H11N3)]Cl·2H2O

Online 14 July 2006


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Acta Cryst. (2006). C62, m343-m345  [ doi:10.1107/S0108270106019068 ]

Poly[[aquatetraimidazoledi-[mu]-phthalato-dicopper(II)] monohydrate]

X.-C. Fu, X.-Y. Wang, M.-T. Li, C.-G. Wang and X.-T. Deng

Formula: [Cu2(C8H4O4)2(C3H4N2)4(H2O)]·H2O

Online 14 July 2006


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Acta Cryst. (2006). C62, m346-m348  [ doi:10.1107/S0108270106020543 ]

A [mu]-chloro-bridged dinuclear ruthenium complex with 9H-carbazole: the formation of one-dimensional linear chains of star-shaped edge-fused rings

M. Dinçer, N. Özdemir, O. Dayan, B. Çetinkaya and O. Büyükgüngör

Formula: [Ru2Cl4(C10H14)2]·2C12H9N

Online 14 July 2006


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Acta Cryst. (2006). C62, m349-m351  [ doi:10.1107/S0108270106021160 ]

Bis(3-aminopyridine-[kappa]N)(4,4'-dimethyl-2,2'-bipyridine-[kappa]2N,N')(perchlorato-[kappa]O)copper(II) perchlorate

H.-F. Qian and W. Huang

Formula: [Cu(ClO4)(C5H6N2)2(C12H12N2)]ClO4

Online 14 July 2006


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Acta Cryst. (2006). C62, m352-m354  [ doi:10.1107/S0108270106010407 ]

trans-Aquachloro[(1R,4R,8S,11S)-6,13-diammonio-6,13-dimethyl-1,4,8,11-tetraazacyclotetradecane-[kappa]4N1,4,8,11]nickel(II) trichloride trihydrate

N. F. Curtis, R. Pawley and W. T. Robinson

Formula: [NiCl(C12H32N6)(H2O)]Cl3·3H2O

Online 22 July 2006


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Acta Cryst. (2006). C62, m355-m357  [ doi:10.1107/S0108270106023092 ]

Bis(iminodiethylenediammonium) di-[mu]5-hydrogenphosphato-pentamolybdate(VI) tetrahydrate

F. Geng, G.-H. Han and B.-Z. Lin

Formula: (C4H15N3)2[Mo5O15(HPO4)2]·4H2O

Online 22 July 2006


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Acta Cryst. (2006). C62, m358-m359  [ doi:10.1107/S0108270106022761 ]

(4-Bromo-2-formylphenolato)perchlorato(1,10-phenanthroline)copper(II)

H.-Y. Wu, Y.-F. Feng, S.-R. Wang and W.-P. Huang

Formula: [Cu(C7H4BrO2)(ClO4)(C12H8N2)]

Online 22 July 2006


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Acta Cryst. (2006). C62, m360-m362  [ doi:10.1107/S0108270106023833 ]

{4,10-Bis[2-(2-oxidobenzylideneamino-[kappa]2N,O)benzyl]-1,7-dioxa-4,10-diazacyclododecane-[kappa]4O1,N4,O3,N10}ytterbium(III) perchlorate acetonitrile solvate

M. González-Lorenzo, A. De Blas, D. Esteban-Gómez, C. Platas-Iglesias and T. Rodríguez-Blas

Formula: [Yb(C36H38N4O4)]ClO4·C2H3N

Online 22 July 2006


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Acta Cryst. (2006). C62, m363-m365  [ doi:10.1107/S0108270106024528 ]

A lithium ethylenediphosphonate containing lithium chains and symmetric hydrogen bonds

C.-Y. Cheng and K.-J. Lin

Formula: [Li(C2H7O6P2)]

Online 22 July 2006


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Acta Cryst. (2006). C62, m366-m368  [ doi:10.1107/S0108270106025091 ]

A polymeric solvent-free variant of a hydridomagnesium inverse crown

D. V. Graham, A. R. Kennedy, R. E. Mulvey and C. T. O'Hara

Formula: [Mg2Na2H2(C6H14N)4]

Online 22 July 2006


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Acta Cryst. (2006). C62, m369-m371  [ doi:10.1107/S0108270106026060 ]

A long Nb=O double bond in bis(pyridinium) tetrachlorooxo(pyridine-[kappa]N)niobate(V) chloride

I. A. Guzei and D. A. Saulys

Formula: (C5H6N)2[NbCl4O(C5H5N)]Cl

Online 29 July 2006


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Acta Cryst. (2006). C62, m372-m374  [ doi:10.1107/S0108270106024309 ]

Poly[(2,2'-bipyridine-[kappa]2N,N')([mu]2-dihydrogen phosphato-[kappa]2O:O')([mu]2-hydrogen phosphato-[kappa]2O:O')aluminium(III)], Al(2,2'-bipy)(HPO4)(H2PO4), a layered inorganic-organic hybrid material

A. M. Chippindale

Formula: [Al(HPO4)(H2PO4)(C10H8N2)]

Online 29 July 2006


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Acta Cryst. (2006). C62, m375-m377  [ doi:10.1107/S0108270106025467 ]

Unusual O-coordination of caffeine in tetrakis([mu]-3,5-dinitrobenzoato-[kappa]2O:O')bis[(caffeine-[kappa]O)copper(II)]

P. Stachová, J. Moncol, D. Valigura and T. Lis

Formula: [Cu2(C7H3N2O6)4(C8H10N4O2)2]

Online 29 July 2006


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Acta Cryst. (2006). C62, m378-m380  [ doi:10.1107/S0108270106025662 ]

(2S,4S,SFc)-2-[2-(Diphenylthiophosphinoyl)ferrocenyl]-4-methoxymethyl-1,3-dioxane

J.-C. Daran, E. Manoury, L. Routaboul and F. Rivals

Formula: [Fe(C5H5)(C23H24O3PS)]

Online 29 July 2006


organic compounds


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Acta Cryst. (2006). C62, o447-o449  [ doi:10.1107/S0108270106021603 ]

Methyl 4-O-benzoyl-2,3-O-isopropylidene-[alpha]-L-rhamnopyranoside

K. H. M. Jonsson, L. Eriksson and G. Widmalm

Formula: C17H22O6

Online 14 July 2006


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Acta Cryst. (2006). C62, o450-o453  [ doi:10.1107/S0108270106021068 ]

Brucinium 3,5-dinitrobenzoate methanol solvate, methanol disolvate and trihydrate

A. Bialonska and Z. Ciunik

Formula: C23H27N2O4+·C7H3N2O6-·CH4O, C23H27N2O4+·C7H3N2O6-·2CH4O and C23H27N2O4+·C7H3N2O6-·3H2O

Online 14 July 2006


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Acta Cryst. (2006). C62, o454-o457  [ doi:10.1107/S0108270106018750 ]

Two modifications of L-alanyl-L-tyrosyl-L-alanine with different solvent molecules in the crystal lattice

L. Checinska, D. Förster, W. Morgenroth and P. Luger

Formula: C15H21N3O5·2.628H2O and C15H21N3O5·C2H6O

Online 14 July 2006


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Acta Cryst. (2006). C62, o458-o460  [ doi:10.1107/S0108270106019524 ]

Hydrated forms of N-[(3R)-3-(4-methyl-3,5-dioxo-1,2,4-triazolidin-1-yl)-2-methylenebutanoyl]-(1S,2R)-bornane-10,2-sultam and its enantiomer

Y. Elemes and K. W. Muir

Formula: C18H26N4O5S·0.151H2O and C18H26N4O5S·0.3485H2O

Online 14 July 2006


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Acta Cryst. (2006). C62, o461-o463  [ doi:10.1107/S0108270106021524 ]

4-(2,4-Dinitrophenylsulfanyl)morpholine

I. Brito, M. López-Rodríguez, A. Cárdenas and D. Vargas

Formula: C10H11N3O5S

Online 14 July 2006


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Acta Cryst. (2006). C62, o464-o466  [ doi:10.1107/S0108270106020804 ]

2,3,4,5,6-Pentanitroaniline 1,2-dichloroethane disolvate: `push-pull' deformation of aromatic rings by intramolecular charge transfer

S. V. Rosokha, J. J. Lu, S. M. Dibrov and J. K. Kochi

Formula: C6H2N6O10·C2H4Cl2

Online 14 July 2006


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Acta Cryst. (2006). C62, o467-o469  [ doi:10.1107/S0108270106021512 ]

4-(4-Chlorobenzylideneamino)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one and 4-(2-chlorobenzylideneamino)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

Y.-X. Sun, R. Zhang, Q.-M. Jin, X.-J. Zhi and X.-M. Lü

Formula: C18H16ClN3O

Online 14 July 2006


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Acta Cryst. (2006). C62, o470-o472  [ doi:10.1107/S0108270106022104 ]

The anilinium chloride adduct of 4-bromo-N-phenylbenzenesulfonamide

T. Gelbrich, T. L. Threlfall and M. B. Hursthouse

Formula: C6H8N+·Cl-·C12H10BrNO2S

Online 14 July 2006


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Acta Cryst. (2006). C62, o473-o475  [ doi:10.1107/S0108270106021706 ]

[beta]-Lapachone

M. S. S. Cunha-Filho, M. Landin, R. Martinez-Pacheco and B. Dacunha-Marinho

Formula: C15H14O3

Online 14 July 2006


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Acta Cryst. (2006). C62, o476-o477  [ doi:10.1107/S0108270106020580 ]

1-(Isopropylideneamino)guanidinium 2-nitrobenzoate: formation of corrugated sheets from R22(8) and R64(16) rings

J. M. S. Skakle, J. L. Wardell and S. M. S. V. Wardell

Formula: C4H11N4+·C7H4NO4-

Online 14 July 2006


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Acta Cryst. (2006). C62, o478-o482  [ doi:10.1107/S0108270106022256 ]

Moxifloxacinium chloride-water-methanol (2/1/1), a novel antibacterial agent

K. Ravikumar and B. Sridhar

Formula: C21H25FN3O4+·Cl-·0.5H2O·0.5CH4O

Online 14 July 2006


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Acta Cryst. (2006). C62, o483-o485  [ doi:10.1107/S010827010602052X ]

(Z)-6-{[1,3-Dihydroxy-2-(hydroxymethyl)propan-2-ylamino]methylene}-2-methoxy-4-[(E)-o-tolyldiazenyl]cyclohexa-2,4-dienone

C. C. Ersanli, Ç. Albayrak, M. Odabasoglu and O. Büyükgüngör

Formula: C19H23N3O5

Online 14 July 2006


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Acta Cryst. (2006). C62, o486-o488  [ doi:10.1107/S0108270106014776 ]

2-Hydroxyacetophenone 4-phenylthiosemicarbazone

E. B. Seena, E. Manoj and M. R. P Kurup

Formula: C15H15N3OS

Online 22 July 2006


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Acta Cryst. (2006). C62, o489-o491  [ doi:10.1107/S0108270106022359 ]

5-Methylsulfanyl-3H-1,2,3-triazolo[4,5-d]pyrimidin-7(6H)-one (2-methylthio-8-azaxanthine) monohydrate

C. R. Maldonado, M. Quirós and J. M. Salas

Formula: C5H5N5OS·H2O

Online 22 July 2006


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Acta Cryst. (2006). C62, o492-o494  [ doi:10.1107/S0108270106022943 ]

The 2:1 cocrystal of benzamide and pentafluorobenzoic acid

W. Jankowski, M. Gdaniec and T. Polonski

Formula: 2C7H7NO·C7HF5O2

Online 22 July 2006


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Acta Cryst. (2006). C62, o495-o497  [ doi:10.1107/S0108270106023675 ]

Chains of edge-fused hydrogen-bonded R33(22) rings in 5,3'-dihydroxy-3,6,7,4',5'-pentamethoxyflavone

G. Y. S. K. Swamy, K. Ravikumar, B. Sridhar, I. Mahender and K. V. N. S. Srinivas

Formula: C20H20O9

Online 22 July 2006


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Acta Cryst. (2006). C62, o498-o500  [ doi:10.1107/S0108270106022827 ]

6-(2-Chloroacetamido)hexanoic acid

C. Gastone, J. Puiggalí, M. Font-Bardia and L. Urpí

Formula: C8H14ClNO3

Online 22 July 2006


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Acta Cryst. (2006). C62, o501-o504  [ doi:10.1107/S0108270106022554 ]

Tetrathiafulvalene revisited

A. S. Batsanov

Formula: C6H4S4, C6H4S4 and C6H4S4

Online 22 July 2006


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Acta Cryst. (2006). C62, o505-o509  [ doi:10.1107/S0108270106025157 ]

1,4-Bis(triisopropylsilyl)buta-1,3-diyne and 1,4-bis(biphenyl-4-yl)buta-1,3-diyne

E. C. Constable, D. Gusmeroli, C. E. Housecroft, M. Neuburger and S. Schaffner

Formula: C22H42Si2 and C28H18

Online 22 July 2006


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Acta Cryst. (2006). C62, o510-o514  [ doi:10.1107/S0108270106023754 ]

3,5-Dichloro-4-cyanobenzoic acid: two polymorphs and the 0.25-hydrate, exhibiting two-dimensional ribbons and nets involving hydrogen-bonding and intermolecular Cl...N interactions

D. Britton

Formula: Two polymorphs of C8H3Cl2NO2, and C8H3Cl2NO2·0.25H2O

Online 22 July 2006


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Acta Cryst. (2006). C62, o515-o517  [ doi:10.1107/S0108270106026011 ]

Anhydrous guanine: a synchrotron study

K. Guille and W. Clegg

Formula: C5H5N5O

Online 29 July 2006


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Acta Cryst. (2006). C62, o518-o520  [ doi:10.1107/S0108270106025583 ]

3-(5-Chloro-3-methyl-1-phenylpyrazol-4-yl)-1,5-diphenylpentane-1,5-dione: sheets built from C-H...O and C-H...[pi](arene) hydrogen bonds

J. Trilleras, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C27H23ClN2O2

Online 29 July 2006


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Acta Cryst. (2006). C62, o521-o524  [ doi:10.1107/S0108270106025893 ]

A hydrogen-bonded chain of rings in 7-amino-5-tert-butyl-2-methylpyrazolo[1,5-a]pyrimidine, and a hydrogen-bonded framework structure in 3,7-diamino-2,5-dimethylpyrazolo[1,5-a]pyrimidine monohydrate

J. Portilla, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C11H16N4 and C8H11N5·H2O

Online 29 July 2006


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Acta Cryst. (2006). C62, o525-o527  [ doi:10.1107/S0108270106025522 ]

3-(4-Methoxyphenyl)-7,7-dimethyl-1,6,7,8-tetrahydropyrazolo[3,4-b]quinolin-5-one: a chain of centrosymmetric rings built from N-H...N and C-H...[pi](arene) hydrogen bonds

S. Cruz, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C19H19N3O2

Online 29 July 2006


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Acta Cryst. (2006). C62, o528-o530  [ doi:10.1107/S0108270106024188 ]

1,6,11,16-Tetraoxacycloeicosane-2,5,12,15-tetraone

K. Noguchi, H. Kondo, Y. Ichikawa, J. Washiyama and K. Okuyama

Formula: C16H24O8

Online 29 July 2006


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Acta Cryst. (2006). C62, o531-o533  [ doi:10.1107/S0108270106025108 ]

Double-helix pattern in a model compound of non-linear optical polymers

R. Centore, A. Carella, A. Pugliese, A. Sirigu and A. Tuzi

Formula: C18H18N4O6

Online 29 July 2006


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Acta Cryst. (2006). C62, o534-o536  [ doi:10.1107/S0108270106024802 ]

(R)-N-[(R)-1-(2-Hydroxy-5-methylphenyl)-2-phenylethyl]-2-methyl-1-phenylpropylammonium chloride

G.-Y. Zhang, W.-H. Wang, J.-Y. Zhao and X.-B. Wang

Formula: C25H30NO+·Cl-

Online 29 July 2006


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