# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' kj21m in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 142.00 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7697 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 16.1716 _cell_length_b 8.4880 _cell_length_c 5.3893 _cell_angle_alpha 90.000 _cell_angle_beta 107.836 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 14270.26 10750.34 63.47 o 6 0 0 2521.15 2767.02 14.54 o 8 0 0 490.83 358.38 4.49 o 10 0 0 20.64 20.09 1.47 o 12 0 0 946.99 865.90 8.72 o 14 0 0 519.62 430.25 10.16 o 16 0 0 888.88 907.34 17.30 o 18 0 0 569.22 573.87 14.30 o 1 1 0 134.41 130.34 2.04 o 3 1 0 1402.33 1458.15 40.66 o 5 1 0 1544.87 1924.79 86.41 o 7 1 0 471.97 462.53 12.91 o 9 1 0 18.59 19.08 0.94 o 11 1 0 173.67 152.21 2.84 o 13 1 0 100.59 90.67 3.93 o 15 1 0 52.84 51.22 2.21 o 17 1 0 180.99 211.78 12.19 o 19 1 0 113.25 115.98 4.84 o 0 2 0 16990.58 15124.90 92.84 o 2 2 0 1625.97 1761.77 20.81 o 4 2 0 8435.39 7625.42 120.35 o 6 2 0 3.00 16.47 0.94 o 8 2 0 3896.55 3913.90 97.31 o 10 2 0 65.08 62.22 1.79 o 12 2 0 3285.58 2979.75 46.19 o 14 2 0 185.40 206.16 6.64 o 16 2 0 371.74 358.14 5.71 o 18 2 0 399.50 448.38 9.31 o 1 3 0 720.13 701.66 6.87 o 3 3 0 956.12 1008.54 11.47 o 5 3 0 743.41 767.79 6.29 o 7 3 0 3119.96 3243.08 49.31 o 9 3 0 29.42 29.16 1.45 o 11 3 0 241.82 226.06 3.73 o 13 3 0 181.90 172.82 7.92 o 15 3 0 10.62 11.13 2.26 o 17 3 0 26.25 25.74 2.03 o 0 4 0 367.62 462.20 8.64 o 2 4 0 611.98 723.63 13.05 o 4 4 0 1682.76 1733.55 15.89 o 6 4 0 682.06 828.92 11.98 o 8 4 0 8537.97 8341.08 103.43 o 10 4 0 1304.30 1274.60 10.68 o 12 4 0 2765.95 2698.68 41.91 o 14 4 0 1021.75 1087.47 13.17 o 16 4 0 675.60 750.19 11.49 o 18 4 0 275.68 285.24 7.39 o 1 5 0 30.70 34.15 0.90 o 3 5 0 102.32 107.48 2.86 o 5 5 0 187.65 214.80 6.81 o 7 5 0 642.21 639.51 12.09 o 9 5 0 352.38 304.23 9.38 o 11 5 0 270.59 282.36 4.98 o 13 5 0 232.02 231.04 5.45 o 15 5 0 0.24 0.52 1.46 o 17 5 0 203.20 229.49 6.70 o 0 6 0 1306.82 1231.60 10.99 o 2 6 0 578.39 534.88 5.55 o 4 6 0 2600.55 2456.57 56.38 o 6 6 0 1370.69 1313.89 24.50 o 8 6 0 986.25 1010.30 12.89 o 10 6 0 296.28 254.81 26.84 o 12 6 0 818.05 831.06 31.26 o 14 6 0 352.77 370.20 11.19 o 16 6 0 1233.50 1259.05 28.14 o 1 7 0 227.73 221.15 3.49 o 3 7 0 50.21 48.43 2.18 o 5 7 0 137.38 146.13 3.52 o 7 7 0 11.74 16.01 2.16 o 9 7 0 35.00 48.47 3.05 o 11 7 0 14.43 12.70 2.12 o 13 7 0 161.78 169.90 4.45 o 15 7 0 36.12 28.01 3.53 o 0 8 0 2466.51 2375.31 31.36 o 2 8 0 940.18 924.09 13.69 o 4 8 0 1610.84 1493.73 37.06 o 6 8 0 534.57 497.65 11.25 o 8 8 0 362.68 362.65 7.69 o 10 8 0 33.88 25.23 2.78 o 12 8 0 248.32 262.50 7.34 o 1 9 0 19.22 16.22 2.16 o 3 9 0 31.88 30.39 2.21 o 5 9 0 206.46 209.49 5.79 o 7 9 0 47.21 49.55 3.34 o 9 9 0 414.74 392.86 8.61 o 11 9 0 15.87 20.85 3.03 o 0 10 0 215.66 218.93 8.57 o 2 10 0 1.80 0.98 1.53 o 4 10 0 906.32 900.23 26.31 o 6 10 0 41.99 39.35 4.47 o 8 10 0 875.97 837.91 27.11 o 1 11 0 15.54 10.49 2.26 o -19 1 1 1059.43 1091.11 14.50 o -17 1 1 25.02 33.63 2.64 o -15 1 1 1329.91 1235.39 32.92 o -13 1 1 574.37 474.21 6.70 o -11 1 1 5249.31 3497.22 446.48 o -9 1 1 88.58 104.02 1.85 o -7 1 1 12397.69 11380.50 55.78 o -5 1 1 2100.31 1949.20 59.01 o -3 1 1 20165.33 16743.46 110.90 o -1 1 1 4742.43 4714.76 30.77 o 1 1 1 18513.61 15614.53 45.68 o 3 1 1 708.79 787.34 19.99 o 5 1 1 144.36 234.13 5.80 o 7 1 1 83.58 64.19 1.92 o 9 1 1 17.76 11.49 0.92 o 11 1 1 371.53 342.45 11.38 o 13 1 1 1713.04 1597.69 17.08 o 15 1 1 761.30 732.01 14.85 o 17 1 1 364.76 378.61 17.52 o -20 2 1 394.78 391.82 14.81 o -18 2 1 8.31 5.33 2.22 o -16 2 1 190.59 180.60 4.10 o -14 2 1 254.91 238.65 4.48 o -12 2 1 1394.99 1472.75 23.36 o -10 2 1 44.29 48.09 1.58 o -8 2 1 1940.74 1996.63 21.33 o -6 2 1 9294.22 8426.26 478.97 o -4 2 1 1522.48 1375.89 48.23 o -2 2 1 154.38 188.37 3.89 o 0 2 1 105.45 153.88 3.17 o 2 2 1 5317.92 6044.78 114.18 o 4 2 1 23.65 21.22 1.06 o 6 2 1 375.15 389.12 7.10 o 8 2 1 40.84 54.61 1.73 o 10 2 1 258.86 275.76 14.22 o 12 2 1 169.83 169.37 3.63 o 14 2 1 2.82 2.95 1.15 o 16 2 1 9.21 7.72 1.92 o 18 2 1 106.58 100.63 4.53 o -19 3 1 1033.07 1046.98 11.89 o -17 3 1 64.58 58.04 3.50 o -15 3 1 1633.05 1751.75 41.15 o -13 3 1 5.00 1.52 1.04 o -11 3 1 4722.65 4646.54 151.21 o -9 3 1 635.35 658.44 5.31 o -7 3 1 3090.42 2857.77 42.16 o -5 3 1 1571.83 1734.81 12.41 o -3 3 1 350.71 257.43 5.26 o -1 3 1 1.66 12.97 0.56 o 1 3 1 4413.86 4227.97 36.52 o 3 3 1 279.89 413.29 13.43 o 5 3 1 9623.29 9801.29 31.68 o 7 3 1 2340.74 2302.82 45.82 o 9 3 1 2841.72 2749.21 30.54 o 11 3 1 3696.88 3357.35 65.75 o 13 3 1 269.20 285.30 5.07 o 15 3 1 652.69 675.75 15.33 o 17 3 1 13.87 15.09 3.63 o -18 4 1 130.19 137.46 5.11 o -16 4 1 38.49 38.53 2.23 o -14 4 1 414.03 437.05 9.29 o -12 4 1 50.50 53.57 1.93 o -10 4 1 86.09 107.31 4.19 o -8 4 1 5.85 3.40 0.67 o -6 4 1 849.55 974.59 10.23 o -4 4 1 1754.22 1949.80 14.57 o -2 4 1 190.61 212.91 4.86 o 0 4 1 1781.60 1922.43 26.22 o 2 4 1 311.84 378.27 6.56 o 4 4 1 1.59 2.29 0.59 o 6 4 1 78.91 72.04 1.83 o 8 4 1 31.37 32.16 2.07 o 10 4 1 49.25 43.45 3.13 o 12 4 1 333.22 293.33 6.96 o 14 4 1 10.92 8.46 1.93 o 16 4 1 101.98 105.30 4.58 o -17 5 1 25.89 17.08 3.52 o -15 5 1 1221.13 1426.80 78.50 o -13 5 1 169.95 176.83 6.01 o -11 5 1 1242.70 1232.82 61.98 o -9 5 1 31.82 41.36 2.51 o -7 5 1 1611.18 1577.07 19.42 o -5 5 1 1591.07 1696.68 22.58 o -3 5 1 860.23 788.64 7.45 o -1 5 1 451.65 439.91 6.61 o 1 5 1 1711.01 1828.24 33.40 o 3 5 1 1064.31 1023.98 57.09 o 5 5 1 5182.71 5284.48 64.59 o 7 5 1 1685.32 1549.71 11.26 o 9 5 1 2961.71 3012.72 32.79 o 11 5 1 1239.21 1173.30 14.56 o 13 5 1 359.71 366.22 7.57 o 15 5 1 358.10 373.95 8.30 o -16 6 1 245.50 273.92 7.16 o -14 6 1 549.57 580.36 27.04 o -12 6 1 6.40 3.63 1.18 o -10 6 1 17.03 29.86 2.88 o -8 6 1 389.21 361.60 15.01 o -6 6 1 135.40 129.26 3.06 o -4 6 1 829.75 859.11 13.88 o -2 6 1 0.30 -0.47 0.56 o 0 6 1 552.85 598.65 6.30 o 2 6 1 404.84 375.95 4.80 o 4 6 1 27.97 30.53 1.86 o 6 6 1 516.94 528.92 6.48 o 8 6 1 11.41 14.75 2.46 o 10 6 1 3.30 4.95 1.67 o 12 6 1 4.58 2.65 1.31 o 14 6 1 128.57 132.95 4.72 o -15 7 1 821.58 957.27 21.33 o -13 7 1 150.15 142.74 5.15 o -11 7 1 277.58 256.91 6.34 o -9 7 1 13.02 6.74 2.81 o -7 7 1 1029.48 953.42 11.42 o -5 7 1 73.18 77.19 2.64 o -3 7 1 4471.52 4263.42 29.72 o -1 7 1 1448.40 1458.29 10.84 o 1 7 1 1032.67 1047.71 22.78 o 3 7 1 3594.53 3805.09 272.90 o 5 7 1 571.52 568.39 9.11 o 7 7 1 475.64 456.02 10.89 o 9 7 1 699.71 643.85 9.29 o 11 7 1 9.56 5.02 1.45 o 13 7 1 895.08 934.43 50.27 o -14 8 1 18.39 25.34 3.06 o -12 8 1 136.66 134.24 5.10 o -10 8 1 1.40 0.90 1.41 o -8 8 1 138.62 150.77 5.12 o -6 8 1 181.40 175.72 5.19 o -4 8 1 8.22 6.48 1.27 o -2 8 1 311.06 303.02 5.30 o 0 8 1 78.13 71.94 4.09 o 2 8 1 382.45 366.50 14.72 o 4 8 1 32.71 34.51 2.17 o 6 8 1 132.61 136.65 5.61 o 8 8 1 39.89 35.02 2.91 o 10 8 1 155.10 162.44 5.73 o 12 8 1 36.31 37.45 3.21 o -11 9 1 358.32 367.76 8.46 o -9 9 1 59.17 65.70 3.69 o -7 9 1 661.31 671.33 25.44 o -5 9 1 107.48 121.31 4.65 o -3 9 1 1480.68 1499.46 20.46 o -1 9 1 22.19 19.26 2.44 o 1 9 1 708.96 707.69 9.34 o 3 9 1 769.34 785.04 25.44 o 5 9 1 592.99 602.55 8.22 o 7 9 1 190.00 189.21 6.19 o 9 9 1 534.07 499.07 13.65 o -8 10 1 211.21 203.63 6.35 o -6 10 1 130.07 131.66 5.13 o -4 10 1 75.37 66.80 3.82 o -2 10 1 281.90 283.28 11.95 o 0 10 1 76.01 77.56 3.94 o 2 10 1 110.60 108.77 6.68 o 4 10 1 68.94 63.59 3.07 o 6 10 1 151.11 151.03 6.90 o -20 0 2 21.48 27.06 4.54 o -18 0 2 2684.02 2641.51 32.01 o -16 0 2 9.17 9.61 2.51 o -14 0 2 3253.07 3262.51 31.96 o -12 0 2 1442.28 1348.20 17.72 o -10 0 2 4127.80 3511.20 28.62 o -8 0 2 2.64 5.69 1.49 o -6 0 2 6202.32 6367.31 30.35 o -2 0 2 11.17 22.53 2.08 o 0 0 2 7209.05 8224.00 52.23 o 2 0 2 58.48 87.23 2.35 o 4 0 2 1938.27 1804.74 23.30 o 6 0 2 306.58 359.33 5.14 o 8 0 2 618.97 591.65 26.56 o 10 0 2 1225.73 1098.63 16.51 o 12 0 2 3632.96 3281.63 32.36 o 14 0 2 1128.74 1180.21 20.29 o 16 0 2 1824.57 1820.50 26.55 o -19 1 2 25.02 29.33 3.08 o -17 1 2 30.65 29.63 1.97 o -15 1 2 232.89 217.96 4.21 o -13 1 2 2.47 4.11 1.07 o -11 1 2 2120.24 2166.45 16.39 o -9 1 2 1098.31 1051.62 16.70 o -7 1 2 625.83 683.28 5.03 o -5 1 2 175.33 214.98 7.48 o -3 1 2 1864.69 2194.94 13.47 o -1 1 2 4121.68 4475.16 76.05 o 1 1 2 127.32 139.84 2.83 o 3 1 2 2303.70 2697.98 14.07 o 5 1 2 337.08 381.59 4.77 o 7 1 2 404.52 372.24 4.39 o 9 1 2 18.26 24.21 1.95 o 11 1 2 122.19 119.12 12.71 o 13 1 2 52.40 49.07 2.96 o 15 1 2 49.75 55.57 3.30 o 17 1 2 26.23 36.60 6.95 o -20 2 2 63.96 71.93 3.13 o -18 2 2 1925.95 1918.94 25.70 o -16 2 2 82.83 85.06 2.97 o -14 2 2 1366.16 1370.13 15.20 o -12 2 2 433.24 393.60 10.26 o -10 2 2 3925.49 3928.42 32.03 o -8 2 2 565.43 456.94 34.81 o -6 2 2 2605.92 2603.76 37.55 o -4 2 2 33.57 36.20 1.11 o -2 2 2 1182.98 1194.23 18.74 o 0 2 2 4188.44 4236.48 81.70 o 2 2 2 1417.86 1549.88 10.94 o 4 2 2 2116.06 1932.29 134.73 o 6 2 2 585.32 575.58 14.65 o 8 2 2 3308.97 3225.74 16.82 o 10 2 2 54.21 58.86 2.30 o 12 2 2 2012.49 1808.41 15.39 o 14 2 2 302.31 301.89 6.85 o 16 2 2 685.37 699.90 28.68 o -19 3 2 66.06 69.84 3.15 o -17 3 2 3.68 5.40 1.98 o -15 3 2 437.64 418.94 6.31 o -13 3 2 233.24 279.62 4.95 o -11 3 2 1742.77 1747.88 24.90 o -9 3 2 23.51 43.02 1.42 o -7 3 2 14.63 13.50 1.41 o -5 3 2 249.08 305.48 5.84 o -3 3 2 625.58 649.71 10.49 o -1 3 2 3894.35 4388.54 51.00 o 1 3 2 1.56 4.08 0.76 o 3 3 2 943.50 1019.69 16.56 o 5 3 2 342.64 304.62 10.20 o 7 3 2 442.90 415.19 4.66 o 9 3 2 22.58 23.51 1.76 o 11 3 2 222.32 207.79 5.42 o 13 3 2 224.10 203.46 18.43 o 15 3 2 47.54 42.51 4.32 o -18 4 2 403.14 396.14 7.06 o -16 4 2 97.40 108.24 5.94 o -14 4 2 821.85 817.84 33.99 o -12 4 2 272.73 250.67 3.33 o -10 4 2 1453.30 1446.86 31.27 o -8 4 2 1138.73 1152.99 12.53 o -6 4 2 2095.54 2078.00 9.62 o -4 4 2 2419.79 2327.88 39.23 o -2 4 2 1953.31 1888.68 11.83 o 0 4 2 730.30 818.57 21.53 o 2 4 2 5942.47 6052.98 135.42 o 4 4 2 2841.64 2802.76 31.70 o 6 4 2 1875.25 1931.82 33.18 o 8 4 2 2830.25 2682.41 56.50 o 10 4 2 20.30 30.69 2.24 o 12 4 2 902.56 829.77 18.02 o 14 4 2 28.75 25.85 2.91 o -17 5 2 645.31 690.56 7.91 o -15 5 2 42.15 42.65 2.77 o -13 5 2 85.71 103.33 2.43 o -11 5 2 0.94 3.65 1.68 o -9 5 2 850.88 789.27 9.87 o -7 5 2 96.87 103.13 2.09 o -5 5 2 73.48 76.51 1.94 o -3 5 2 2466.90 2557.37 38.79 o -1 5 2 1105.48 1044.88 23.00 o 1 5 2 51.42 51.53 3.74 o 3 5 2 186.55 178.64 13.71 o 5 5 2 1555.28 1469.15 19.04 o 7 5 2 179.58 165.69 3.87 o 9 5 2 99.25 88.59 4.31 o 11 5 2 42.91 42.73 2.95 o 13 5 2 0.50 0.41 1.49 o 15 5 2 48.50 41.35 4.82 o -16 6 2 177.17 205.54 6.18 o -14 6 2 796.17 877.37 16.09 o -12 6 2 123.65 121.66 4.41 o -10 6 2 1050.85 990.47 49.99 o -8 6 2 1642.13 1572.10 69.95 o -6 6 2 1205.63 1158.90 20.17 o -4 6 2 3028.61 3118.65 50.67 o -2 6 2 2801.82 2651.90 32.69 o 0 6 2 1576.95 1580.96 11.00 o 2 6 2 752.99 825.43 19.54 o 4 6 2 763.41 738.16 18.42 o 6 6 2 1164.54 1181.30 10.51 o 8 6 2 448.66 469.74 18.19 o 10 6 2 495.63 494.07 16.54 o 12 6 2 198.18 206.43 5.09 o -15 7 2 10.56 11.54 3.55 o -13 7 2 102.66 103.54 4.33 o -11 7 2 22.88 28.29 2.83 o -9 7 2 9.14 5.55 3.65 o -7 7 2 3.79 4.10 1.45 o -5 7 2 341.73 359.40 5.49 o -3 7 2 68.59 82.41 2.74 o -1 7 2 563.35 558.36 8.52 o 1 7 2 0.05 -0.92 0.92 o 3 7 2 302.76 288.60 4.98 o 5 7 2 97.59 71.62 6.88 o 7 7 2 26.25 26.30 2.12 o 9 7 2 41.61 48.27 4.59 o 11 7 2 23.16 21.45 2.24 o -14 8 2 1096.19 1097.35 15.05 o -12 8 2 256.39 269.84 7.23 o -10 8 2 285.54 281.39 13.98 o -8 8 2 430.52 415.15 8.21 o -6 8 2 872.30 854.51 22.33 o -4 8 2 1306.50 1348.32 12.00 o -2 8 2 1654.24 1670.84 26.37 o 0 8 2 628.28 629.36 9.81 o 2 8 2 190.87 195.51 5.67 o 4 8 2 823.87 832.77 21.81 o 6 8 2 200.58 195.69 5.93 o 8 8 2 97.70 105.98 5.19 o 10 8 2 623.10 611.97 32.39 o -11 9 2 73.98 80.43 4.30 o -9 9 2 939.16 977.87 13.53 o -7 9 2 76.32 69.83 3.66 o -5 9 2 421.55 393.71 11.70 o -3 9 2 290.56 264.08 22.00 o -1 9 2 57.68 70.99 6.56 o 1 9 2 2.18 1.79 1.19 o 3 9 2 32.51 34.62 2.99 o 5 9 2 381.40 374.34 8.69 o 7 9 2 152.85 160.34 5.95 o -8 10 2 127.86 132.99 5.41 o -6 10 2 258.07 271.37 10.61 o -4 10 2 131.22 126.52 7.16 o -2 10 2 674.79 693.01 11.63 o 0 10 2 131.39 130.52 4.15 o 2 10 2 191.42 193.51 8.59 o 4 10 2 588.58 600.37 33.63 o -19 1 3 291.89 296.52 7.62 o -17 1 3 2485.12 2384.05 110.00 o -15 1 3 510.03 478.79 8.34 o -13 1 3 244.18 258.32 4.08 o -11 1 3 1985.73 1861.66 30.08 o -9 1 3 16.62 16.84 1.39 o -7 1 3 1110.36 1030.80 8.17 o -5 1 3 197.31 169.52 3.85 o -3 1 3 2182.68 2115.01 24.75 o -1 1 3 0.91 8.49 1.42 o 1 1 3 8178.87 8421.73 72.17 o 3 1 3 299.96 332.26 3.80 o 5 1 3 3523.25 3597.94 23.65 o 7 1 3 316.89 303.08 10.54 o 9 1 3 2040.67 1944.32 20.48 o 11 1 3 81.92 83.35 3.64 o 13 1 3 1802.89 1743.11 17.48 o 15 1 3 8.35 10.08 2.42 o -20 2 3 34.87 35.14 3.31 o -18 2 3 56.27 56.85 3.49 o -16 2 3 0.05 -1.27 1.27 o -14 2 3 307.98 290.77 5.16 o -12 2 3 372.55 387.80 8.24 o -10 2 3 1.65 1.64 0.95 o -8 2 3 19.56 19.34 1.95 o -6 2 3 4432.60 4537.49 71.91 o -4 2 3 1796.01 1945.93 29.29 o -2 2 3 218.76 206.44 13.62 o 0 2 3 716.87 831.24 8.31 o 2 2 3 649.02 667.03 8.04 o 4 2 3 1102.21 1113.35 22.50 o 6 2 3 28.67 35.46 2.06 o 8 2 3 1935.72 1798.93 12.73 o 10 2 3 212.39 193.57 9.49 o 12 2 3 6.08 8.39 2.81 o 14 2 3 17.71 20.56 4.22 o -19 3 3 431.01 429.79 7.48 o -17 3 3 282.92 292.25 4.99 o -15 3 3 96.31 105.72 3.19 o -13 3 3 782.74 856.27 8.99 o -11 3 3 714.75 729.43 10.45 o -9 3 3 2245.29 2233.99 21.47 o -7 3 3 3366.75 3382.76 22.46 o -5 3 3 1108.56 1133.40 8.92 o -3 3 3 2900.43 3037.04 85.54 o -1 3 3 90.77 81.95 2.28 o 1 3 3 3456.10 3542.70 35.43 o 3 3 3 245.37 262.21 4.12 o 5 3 3 2209.45 2218.17 36.92 o 7 3 3 0.99 -0.07 1.15 o 9 3 3 1194.05 1176.23 13.39 o 11 3 3 42.85 35.72 2.71 o 13 3 3 494.46 489.43 13.88 o -18 4 3 3.72 2.84 1.33 o -16 4 3 1.92 0.63 1.08 o -14 4 3 3.46 2.03 1.04 o -12 4 3 1.73 0.74 0.81 o -10 4 3 195.82 204.62 4.22 o -8 4 3 408.39 369.24 4.29 o -6 4 3 143.93 139.94 2.65 o -4 4 3 284.89 293.71 12.60 o -2 4 3 342.83 300.99 5.51 o 0 4 3 294.10 240.50 7.31 o 2 4 3 356.27 332.25 6.30 o 4 4 3 45.60 34.81 2.70 o 6 4 3 484.35 469.57 12.26 o 8 4 3 233.06 233.73 13.10 o 10 4 3 58.72 62.49 3.47 o 12 4 3 27.47 28.90 3.25 o -17 5 3 89.68 85.94 4.02 o -15 5 3 492.92 579.24 7.60 o -13 5 3 1146.77 1271.10 11.73 o -11 5 3 1149.44 1196.76 34.89 o -9 5 3 1652.06 1683.94 25.80 o -7 5 3 2480.28 2621.08 23.23 o -5 5 3 965.22 1056.96 27.15 o -3 5 3 2133.75 2111.25 13.37 o -1 5 3 592.33 566.13 15.93 o 1 5 3 500.03 552.79 9.23 o 3 5 3 229.04 268.52 7.59 o 5 5 3 1099.07 1092.52 18.72 o 7 5 3 1.84 2.70 1.61 o 9 5 3 811.86 783.24 16.24 o 11 5 3 50.86 52.41 3.49 o -16 6 3 84.50 56.01 5.70 o -14 6 3 93.48 95.12 6.31 o -12 6 3 3.76 1.41 1.12 o -10 6 3 126.02 122.49 3.51 o -8 6 3 22.98 22.92 1.89 o -6 6 3 103.49 118.29 3.39 o -4 6 3 1197.55 1201.99 19.06 o -2 6 3 14.17 10.57 1.54 o 0 6 3 927.84 869.84 10.24 o 2 6 3 692.47 631.82 7.64 o 4 6 3 113.34 128.03 4.18 o 6 6 3 173.06 174.80 4.54 o 8 6 3 7.02 7.57 2.50 o 10 6 3 99.42 95.35 4.47 o -15 7 3 1560.85 1728.42 28.44 o -13 7 3 578.85 566.61 19.80 o -11 7 3 971.71 887.47 15.98 o -9 7 3 238.85 213.71 5.71 o -7 7 3 698.03 719.21 10.08 o -5 7 3 339.73 346.16 7.00 o -3 7 3 876.09 889.23 27.55 o -1 7 3 1083.95 1134.49 19.35 o 1 7 3 340.17 344.18 10.16 o 3 7 3 16.59 20.40 2.10 o 5 7 3 501.23 522.11 16.35 o 7 7 3 22.72 20.37 2.19 o 9 7 3 697.45 672.01 9.34 o -12 8 3 424.40 419.21 8.84 o -10 8 3 57.77 57.55 3.41 o -8 8 3 272.35 261.89 6.44 o -6 8 3 30.41 34.44 3.07 o -4 8 3 74.64 83.46 3.96 o -2 8 3 7.56 10.38 4.94 o 0 8 3 3.11 2.67 1.72 o 2 8 3 117.02 131.20 4.97 o 4 8 3 62.01 60.57 3.82 o 6 8 3 0.12 -0.11 1.60 o 8 8 3 46.08 43.32 2.85 o -9 9 3 86.14 74.14 3.86 o -7 9 3 186.79 169.36 7.75 o -5 9 3 227.54 235.54 9.76 o -3 9 3 872.43 935.32 13.13 o -1 9 3 323.64 330.42 7.92 o 1 9 3 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