Crystal Structure Communications

 

Acta Cryst. (2006). C62, i73-i75  [ doi:10.1107/S010827010602542X ]

Meta-barium borate, II-BaB₂O₄, at 163 and 293 K

S.-F. Lu, Z.-X. Huang and J.-L. Huang

Synopsis: The structural data at 163 and 293 K for II-BaB₂O₄, an excellent non-linear optical material, indicate a significant shortening of the c axial length in the unit cell at 163 K, whereas the a and b axial lengths essentially do not change.

Formula: Ba₃(B₃O₆)₂ and Ba₃(B₃O₆)₂

Online 11 August 2006

 

Acta Cryst. (2006). C62, i76-i78  [ doi:10.1107/S0108270106027193 ]

Lithium dioxobis[trioxoiodato(V)]vanadate, Li[VO₂(IO₃)₂]

X.-A. Chen, L. Zhang, X.-A. Chang, H.-G. Zang and W.-Q. Xiao

Synopsis: In Li[VO₂(IO₃)₂], distorted VO₆ octahedra are bridged by iodate groups to form two-dimensional [VO₂(IO₃)₂]^- layers that are separated by octahedrally coordinated Li⁺ cations.

Formula: Li[VO₂(IO₃)₂]

Online 11 August 2006

 

Acta Cryst. (2006). C62, i79-i82  [ doi:10.1107/S0108270106028253 ]

Triaquamanganese sulfite revisited

M. E. Díaz de Vivar, S. Baggio, M. T. Garland and R. Baggio

Synopsis: Orthorhombic Mn(SO₃)(H₂O)₃ crystallizes with P2₁2₁2₁ symmetry, as determined by the H-atom positions and the hydrogen-bond network.

Formula: Mn(SO₃)(H₂O)₃

Online 11 August 2006

 

Acta Cryst. (2006). C62, i83-i84  [ doi:10.1107/S0108270106026850 ]

-Alumina: a single-crystal X-ray diffraction study

L. Smrcok, V. Langer and J. Krestan

Synopsis: In addition to the spinel-type 16d and 8a positions of space group Fdm, a small fraction of the Al ions in -alumina also occupy the non-spinel 6c and 48f positions.

Formula: Al_2.67O₄

Online 23 August 2006

 

Acta Cryst. (2006). C62, m381-m385  [ doi:10.1107/S0108270106025972 ]

Tetrakis[2-(2-pyridyl)pyridinium] tetra-₃-iodo-hexa-₂-iodo-dodecaiodohexabismuthate and bis[tris(2,2'-bipyridine)ruthenium(II)] di-₄-iodo-octa-₂-iodo-dodecaiodohexabismuthate

A. M. Goforth, M. A. Tershansy, M. D. Smith, L. Peterson Jr and H.-C. zur Loye

Formula: (C₁₀H₉N₂)₄[Bi₆I₂₂] and [Ru(C₁₀H₈N₂)₃][Bi₆I₂₂]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m386-m388  [ doi:10.1107/S0108270106020191 ]

{2,5-Bis[3-(tert-butylaminoxyl)phenyl]-1,1-dimethyl-3,4-diphenylsilole-O}bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)manganese(II)

N. Roques, P. Gerbier, I. Imaz, P. Guionneau and J.-P. Sutter

Formula: [Mn(C₅HF₆O₂)₂(C₃₈H₄₂N₂O₂Si)₂]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m389-m391  [ doi:10.1107/S0108270106025625 ]

Poly[[diaquacadmium(II)]-₄-[N-(phosphonatomethyl)ammonio]acetato]

Q.-J. Deng, M.-H. Zeng, H. Liang and K.-L. Huang

Formula: [Cd(C₃H₆NO₅P)(H₂O)₂]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m392-m394  [ doi:10.1107/S0108270106026783 ]

catena-Poly[[aqua(2,2'-bipyridine-²N,N')cadmium(II)]--4-carboxylatophenoxyacetato-³O:O⁴,O^4']

Y. Yang, M.-H. Zeng, F.-Y. Meng and H. Liang

Formula: [Cd(C₉H₆O₅)(C₁₀H₈N₂)(H₂O)]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m395-m397  [ doi:10.1107/S0108270106026679 ]

Poly[aqua(₃-benzene-1,2-dicarboxylato)(₂-hydroxo)indium(III)]

Y.-L. Wang, Q.-Y. Liu and S.-L. Zhong

Formula: [In(C₈H₄O₄)(OH)(H₂O)]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m398-m400  [ doi:10.1107/S0108270106026916 ]

Dichloro[(1E,1'E)-1,1'-(pyridine-2,6-diyl)diethanone bis(O-methyloxime)-³N¹,N²,N⁶]cobalt(II)

N. Özdemir, M. Dinçer, O. Dayan and B. Çetinkaya

Formula: [CoCl₂(C₁₁H₁₅N₃O₂)]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m401-m403  [ doi:10.1107/S0108270106027880 ]

Bis(acesulfamato-²O⁴,N)bis(3-methylpyridine)copper(II)

N. Dege, H. Içbudak and E. Adiyaman

Formula: [Cu(C₄H₄O₄NS)₂(C₆H₇N)₂]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m404-m406  [ doi:10.1107/S0108270106021809 ]

An unusual eight-coordinated copper complex: bis(4,7-diphenyl-1,10-phenanthroline)dinitratocopper(II)

Y. Moreno, P. Hermosilla, M. T. Garland, O. Peña and R. Baggio

Formula: [Cu(NO₃)₂(C₂₄H₁₆N₂)₂]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m407-m410  [ doi:10.1107/S0108270106027314 ]

(Z)-1-Ferrocenyl-3-(3-hydroxyanilino)but-2-en-1-one and (Z)-1-ferrocenyl-3-(4-hydroxyanilino)but-2-en-1-one

Y.-C. Shi, S.-H. Zhang, H.-J. Cheng and W.-P. Sun

Formula: Two isomers of [Fe(C₅H₅)(C₁₅H₁₄NO₂)]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m411-m412  [ doi:10.1107/S0108270106028009 ]

catena-Poly[[(trifluoromethanesulfonato-O)silver(I)]--di-2-pyridylamine-²N²:N^2'], a chain polymer with short AgC contacts

P. G. Jones, O. Crespo, M. C. Gimeno and A. Laguna

Formula: [Ag(CF₃O₃S)(C₁₀H₉N₃)]

Online 11 August 2006

 

Acta Cryst. (2006). C62, m413-m415  [ doi:10.1107/S010827010602508X ]

Poly[propane-1,3-diyldiammonium tetra--selenito-trizinc dihydrate]

L. K. Ritchie and W. T. A. Harrison

Formula: (C₃H₁₂N₂)[Zn₃(SeO₃)₄]·2H₂O

Online 11 August 2006

 

Acta Cryst. (2006). C62, m416-m418  [ doi:10.1107/S0108270106028046 ]

Supramolecular structure and second harmonic generation in strontium bis(hydrogen L-malate) hexahydrate

E. de Matos Gomes, V. H. Rodrigues, M. M. R. R. Costa, E. Nogueira and M. S. Belsley

Formula: [Sr(C₄H₅O₅)₂(H₂O)₄]·2H₂O

Online 11 August 2006

 

Acta Cryst. (2006). C62, m419-m420  [ doi:10.1107/S0108270106026448 ]

Sodium trichloromethanesulfonate monohydrate

E. Damian, L. Eriksson and M. Sandström

Synopsis: The title compound crystallizes in P2₁/a with all the atoms located in general positions. The trichlate anion consists of pyramidal SO₃ and CCl₃ groups connected via an S-C bond in a staggered conformation with approximate C_3v symmetry.

Formula: Na⁺·CCl₃O₃S^-·H₂O

Online 11 August 2006

 

Acta Cryst. (2006). C62, m421-m423  [ doi:10.1107/S0108270106025030 ]

trans-Bis[3,5-bis(trifluoromethyl)-1H-pyrazole-N²]dichloropalladium(II) monohydrate

L. C. Spencer, I. A. Guzei, S. O. Ojwach and J. Darkwa

Formula: [PdCl₂(C₅H₂F₆N₂)₂]·H₂O

Online 23 August 2006

 

Acta Cryst. (2006). C62, m424-m427  [ doi:10.1107/S0108270106027491 ]

Partially oxidized ruthenium phosphine thiolates: [Ru(pySO₂)_0.33(pyS)_1.67(dppe)] and [Ru(pySO₂)_0.355(pyS)_1.645(dppp)]

G. Von Poelhsitz, B. L. Rodrigues and A. A. Batista

Formula: [Ru(C₅H₄NO₂S)_0.33(C₅H₄NS)_1.67(C₂₆H₂₄P₂)] and [Ru(C₅H₄NO₂S)_0.33(C₅H₄NS)_1.67(C₂₆H₂₄P₂)]

Online 23 August 2006

 

Acta Cryst. (2006). C62, m428-m430  [ doi:10.1107/S0108270106030198 ]

A one-dimensional mixed-anion lead(II) coordination polymer: catena-poly[[(1,10-phenanthroline)lead(II)]--benzoato--nitrato-[(1,10-phenanthroline)lead(II)]-di--benzoato]

L.-G. Zhu

Formula: [Pb₂(C₇H₅O₂)₃(NO₃)(C₁₂H₈N₂)₂]

Online 23 August 2006

 

Acta Cryst. (2006). C62, m431-m433  [ doi:10.1107/S0108270106029866 ]

Poly[tetra--aqua-hexaaquadi-₃-malonato-dinitratodibarium(II)nickel(II)]

M.-L. Guo and H.-X. Cao

Formula: [Ba₂Ni(C₃H₂O₄)₂(NO₃)₂(H₂O)₁₀]

Online 23 August 2006

 

Acta Cryst. (2006). C62, m434-m436  [ doi:10.1107/S0108270106029854 ]

Diaquabis(ethylenediamine)cadmium(II) bis(4-aminonaphthalene-1-sulfonate) dihydrate

M.-T. Li, C.-G. Wang and X.-C. Fu

Formula: [Cd(C₂H₈N₂)₂(H₂O)₂](C₁₀H₈NO₃S)₂·2H₂O

Online 23 August 2006

 

Acta Cryst. (2006). C62, m437-m439  [ doi:10.1107/S0108270106028903 ]

An unusual example of a linearly coordinated acetone ligand in a six-coordinate iron(II) complex

C. A. Kilner and M. A. Halcrow

Formula: [Fe(C₁₉H₂₅N₅)(C₃H₆O)(H₂O)₂](BF₄)₂·2C₃H₆O

Online 31 August 2006

 

Acta Cryst. (2006). C62, m440-m442  [ doi:10.1107/S0108270106027582 ]

A novel 8-carboxyindeno[1,2-b]quinoxalin-11-one thiosemicarbazone zinc(II) Schiff base complex

X.-Q. Che, Y.-X. Gao and J.-W. Wang

Formula: [Zn₂(C₁₇H₉N₅O₂S)₂(C₂H₆OS)₂]·3C₂H₆OS

Online 31 August 2006

 

Acta Cryst. (2006). C62, m443-m447  [ doi:10.1107/S0108270106025339 ]

Two-dimensional square-grid frameworks formed by self-associating copper(II) complexes with 1-(3-pyridyl)- and 1-(4-pyridyl)-substituted butane-1,3-diones

K. V. Domasevitch, V. D. Vreshch, A. B. Lysenko and H. Krautscheid

Formula: [Cu(C₉H₈NO₂)₂] and [Cu(C₉H₈NO₂)₂]·CH₄O

Online 31 August 2006

 

Acta Cryst. (2006). C62, m448-m450  [ doi:10.1107/S0108270106031520 ]

catena-Poly[[[triaquasulfatocobalt(II)]--4,4'-bipyridine] ethane-1,2-diol solvate]

W.-J. Lu, Y.-M. Zhu and K.-L. Zhong

Formula: [Co(SO₄)(C₁₀H₈N₂)(H₂O)₃]·C₂H₆O₂

Online 31 August 2006

 

Acta Cryst. (2006). C62, m451-m454  [ doi:10.1107/S0108270106030320 ]

Paddlewheel dirhodium complexes bridged by para-substituted benzoates

M. Ebihara, K. Yamada and T. Kawamura

Formula: [Rh₂(C₁₁H₁₄NO₂)₄(C₇H₅N)₂] and [Rh₂(C₇H₄NO₄)₄(C₅H₅N)(CH₄O)]

Online 31 August 2006

 

Acta Cryst. (2006). C62, o537-o539  [ doi:10.1107/S0108270106024711 ]

Isomorphous crystals of strychninium 4-chlorobenzoate and strychninium 4-nitrobenzoate

A. Bialonska and Z. Ciunik

Formula: C₂₁H₂₃N₂O₂⁺·C₇H₄ClO₂^- and C₂₁H₂₃N₂O₂⁺·C₇H₄NO₄^-

Online 11 August 2006

 

Acta Cryst. (2006). C62, o540-o543  [ doi:10.1107/S010827010602378X ]

4-(4-Fluoro-3-phenoxyphenyl)-6-(4-fluorophenyl)-2-oxo-1,2-dihydropyridine-3-carbonitrile and the 6-(4-methylphenyl)- analogue

D. Chopra, T. P. Mohan, B. Vishalakshi and T. N. Guru Row

Formula: C₂₄H₁₄F₂N₂O₂ and C₂₅H₁₇FN₂O₂

Online 11 August 2006

 

Acta Cryst. (2006). C62, o544-o546  [ doi:10.1107/S0108270106025571 ]

2-Anilinomethylene-3-oxobutanenitrile: an X-ray and density functional theory study

V. Langer, E. Scholtzová, P. Mach, T. Solcan and L. Smrcok

Formula: C₁₁H₁₀N₂O

Online 11 August 2006

 

Acta Cryst. (2006). C62, o547-o549  [ doi:10.1107/S0108270106026084 ]

Host-guest interaction in a thiourea-dimethyl oxalate (2/1) complex at 300 and 100 K

R. Chitra, P. Roussel and R. R. Choudhury

Formula: 2CH₄N₂S·C₄H₆O₄ and 2CH₄N₂S·C₄H₆O₄

Online 11 August 2006

 

Acta Cryst. (2006). C62, o550-o553  [ doi:10.1107/S0108270106026874 ]

Three substituted (E)-3-aryl-2-(thienyl)acrylonitriles: isolated molecules, simple hydrogen-bonded chains and hydrogen-bonded sheets

D. Cobo, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C₁₆H₁₅NO₃S, C₁₃H₈BrNS and C₁₃H₉NS

Online 11 August 2006

 

Acta Cryst. (2006). C62, o554-o556  [ doi:10.1107/S0108270106027557 ]

5-(2-Hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-3-methyl-2-(methylsulfanyl)-6-phenyl-7H-pyrrolo[2,3-d]pyrimidin-4(3H)-one monohydrate: complex sheets generated by multiple hydrogen bonds

S. Cruz, J. Quiroga, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C₂₂H₂₃N₃O₃S·H₂O

Online 11 August 2006

 

Acta Cryst. (2006). C62, o557-o560  [ doi:10.1107/S0108270106025819 ]

4-Dimethylamino--nitrostyrene and 4-dimethylamino--ethyl--nitrostyrene at 100 K

L. Hamdellou, O. Hernandez and J. Meinnel

Formula: C₁₀H₁₂N₂O₂ and C₁₂H₁₆N₂O₂

Online 11 August 2006

 

Acta Cryst. (2006). C62, o561-o562  [ doi:10.1107/S0108270106026928 ]

N,N'-Bis(2-methoxyphenyl)naphthalene-1,4-dicarboxamide

L.-H. Jing, D.-B. Qin, S.-J. Gu, H.-X. Zhang and G. Lei

Formula: C₂₆H₂₂N₂O₄

Online 11 August 2006

 

Acta Cryst. (2006). C62, o563-o566  [ doi:10.1107/S0108270106024814 ]

4-Acetamido-3,3,5,5-[²H₄]-2,2,6,6-tetra([²H₃]methyl)piperidin-1-yloxyl 0.33-hydrate

J. Duskova, J. Labsky, I. Cisarova, T. Skalova, J. Dohnalek and J. Hasek

Formula: C₁₁H₅D₁₆N₂O₂·0.33H₂O

Online 11 August 2006

 

Acta Cryst. (2006). C62, o567-o570  [ doi:10.1107/S0108270106029209 ]

L-Prolinium picrate and 2-methylpyridinium picrate

K. Anitha, S. Athimoolam and S. Natarajan

Formula: C₅H₁₀NO₂⁺·C₆H₂N₃O₇^- and C₆H₈N⁺·C₆H₂N₃O₇^-

Online 23 August 2006

 

Acta Cryst. (2006). C62, o571-o573  [ doi:10.1107/S0108270106029532 ]

Tris(1,9-diethyladeninium) triiodide diiodide

E. F. Day, N. S. Dean and A. H. Franz

Formula: 3C₉H₁₄N₅⁺·I₃^-·2I^-

Online 23 August 2006

 

Acta Cryst. (2006). C62, o574-o576  [ doi:10.1107/S0108270106029465 ]

Imino Diels-Alder adducts. XII. Two pyrano[3,2-c]quinolines

K. Ravikumar, B. Sridhar, M. Mahesh and V. V. N. Reddy

Formula: C₁₈H₁₈FNO and C₁₉H₂₁NO

Online 23 August 2006

 

Acta Cryst. (2006). C62, o577-o580  [ doi:10.1107/S0108270106028101 ]

Boc-Pro-Hyp-Gly-OBzl and Boc-Ala-Hyp-Gly-OBzl, two repeating triplets found in collagen

M. Doi, K. Imori, N. Sakaguchi and A. Asano

Formula: C₂₄H₃₃N₃O₇ and C₂₂H₃₁N₃O₇

Online 23 August 2006

 

Acta Cryst. (2006). C62, o581-o582  [ doi:10.1107/S0108270106030502 ]

N-(2-Aminobenzyl)-N,N-bis(quinolin-2-ylmethyl)amine

A. Mitra, P. J. Seaton and K. A. Wheeler

Formula: C₂₇H₂₄N₄

Online 23 August 2006

 

Acta Cryst. (2006). C62, o583-o586  [ doi:10.1107/S0108270106032689 ]

Hydrogen-bonded chains in racemic 2-benzyl-3-(2-bromophenyl)propiononitrile and hydrogen-bonded sheets in methyl 2-benzyl-2-cyano-3-phenylpropionate

G. Calderón, L. M. Jaramillo-Gómez, J. M. de la Torre, J. Cobo, J. N. Low and C. Glidewell

Formula: C₁₆H₁₄BrN and C₁₈H₁₇NO₂

Online 31 August 2006