# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' qa067 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 328.49 _exptl_crystal_F_000 1252.00 _reflns_d_resolution_high 0.8255 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.7162 _cell_length_b 15.0626 _cell_length_c 15.8365 _cell_angle_alpha 76.490 _cell_angle_beta 80.577 _cell_angle_gamma 79.533 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2.27 4.83 8.52 o 2 0 0 3703.45 5498.61 133.96 o 3 0 0 9.47 1.87 35.56 o 4 0 0 5399.21 5924.55 119.13 o 5 0 0 151.87 111.98 44.21 o 6 0 0 5808.66 6370.69 125.96 o 7 0 0 97.30 77.56 41.61 o 8 0 0 289.16 234.25 41.27 o 9 0 0 312.54 415.20 70.90 o 10 0 0 1236.56 1721.93 193.12 o 11 0 0 248.69 264.36 124.04 o 12 0 0 383.04 320.60 138.29 o 13 0 0 87.34 84.98 132.06 o -13 1 0 0.99 -92.74 126.71 o -12 1 0 49.05 74.17 113.35 o -11 1 0 356.50 190.32 113.10 o -10 1 0 516.36 488.20 127.86 o -9 1 0 3572.71 3649.08 215.89 o -8 1 0 579.14 651.80 84.03 o -7 1 0 5601.07 5554.89 123.27 o -6 1 0 688.89 530.90 44.50 o -5 1 0 568.41 474.86 49.06 o -4 1 0 9130.63 9790.83 191.92 o -3 1 0 541.46 660.00 43.91 o -2 1 0 3180.21 3654.77 101.72 o -1 1 0 13294.57 11554.54 140.96 o 0 1 0 78.20 4.45 7.63 o 1 1 0 26564.57 31849.33 620.46 o 2 1 0 17464.81 21046.69 295.50 o 3 1 0 3571.24 4157.74 85.74 o 4 1 0 6030.67 5871.64 123.85 o 5 1 0 5312.76 5037.64 123.59 o 6 1 0 180.84 311.90 39.31 o 7 1 0 5568.42 6152.42 129.35 o 8 1 0 451.80 422.78 84.42 o 9 1 0 12.26 78.32 59.29 o 10 1 0 2.72 -38.68 80.79 o 11 1 0 1018.93 1130.87 176.96 o 12 1 0 37.22 103.18 110.68 o 13 1 0 541.41 794.37 182.69 o -13 2 0 212.76 67.17 135.36 o -12 2 0 1232.58 1305.28 194.39 o -11 2 0 18.92 -2.87 146.05 o -10 2 0 103.38 48.36 57.52 o -9 2 0 844.95 715.73 90.01 o -8 2 0 2722.52 2894.10 129.49 o -7 2 0 1621.77 1642.79 92.32 o -6 2 0 156.80 126.35 41.10 o -5 2 0 4931.87 5007.15 137.24 o -4 2 0 718.30 629.78 50.19 o -3 2 0 9858.74 10145.73 146.08 o -2 2 0 37283.32 37865.95 435.72 o -1 2 0 2395.57 2281.74 44.75 o 0 2 0 4894.23 4126.69 76.23 o 1 2 0 19465.55 20037.27 416.65 o 2 2 0 230.28 177.09 36.89 o 3 2 0 3103.97 3422.06 71.13 o 4 2 0 1109.26 1452.93 111.13 o 5 2 0 7710.90 7918.56 283.51 o 6 2 0 5.47 51.86 49.68 o 7 2 0 5151.81 5216.57 174.29 o 8 2 0 3576.88 3618.23 134.35 o 9 2 0 1430.97 1595.20 105.01 o 10 2 0 50.17 34.22 90.33 o 11 2 0 445.80 849.96 159.79 o 12 2 0 43.14 68.32 106.36 o 13 2 0 208.89 173.15 128.11 o -12 3 0 97.34 187.27 130.53 o -11 3 0 37.87 12.89 58.23 o -10 3 0 1390.74 1532.49 216.28 o -9 3 0 402.30 550.32 82.90 o -8 3 0 3043.71 2996.44 135.91 o -7 3 0 1785.88 1891.02 103.83 o -6 3 0 4370.56 4682.00 156.29 o -5 3 0 750.15 915.22 65.54 o -4 3 0 913.20 883.06 43.25 o -3 3 0 5242.43 5307.54 96.34 o -2 3 0 7383.94 7725.89 118.87 o -1 3 0 7095.73 8151.78 118.38 o 0 3 0 28843.97 31976.67 449.81 o 1 3 0 1658.43 1439.15 45.10 o 2 3 0 57.60 34.60 42.36 o 3 3 0 122.27 51.65 42.75 o 4 3 0 14939.37 16768.15 255.00 o 5 3 0 1312.04 1701.85 98.15 o 6 3 0 1200.50 1318.58 58.05 o 7 3 0 900.35 1215.64 143.06 o 8 3 0 209.29 127.35 67.30 o 9 3 0 338.54 323.90 68.50 o 10 3 0 1655.91 1441.41 111.14 o 11 3 0 39.48 59.54 91.22 o 12 3 0 11.09 50.38 108.01 o 13 3 0 30.88 46.05 95.54 o -12 4 0 89.76 184.72 107.88 o -11 4 0 920.37 833.43 108.24 o -10 4 0 1536.54 1478.17 121.12 o -9 4 0 435.25 361.10 77.06 o -8 4 0 785.60 653.37 80.41 o -7 4 0 104.36 80.09 49.74 o -6 4 0 375.71 611.59 66.29 o -5 4 0 9233.72 8245.14 147.12 o -4 4 0 2738.07 2546.58 74.19 o -3 4 0 6428.78 6125.52 110.63 o -2 4 0 379.72 383.82 54.21 o -1 4 0 161.31 151.08 31.55 o 0 4 0 22.18 38.16 27.75 o 1 4 0 579.62 580.88 38.40 o 2 4 0 8700.11 9436.73 264.36 o 3 4 0 1599.21 1644.58 104.83 o 4 4 0 78.65 106.23 50.76 o 5 4 0 6978.70 6967.12 237.78 o 6 4 0 5.99 -3.31 44.53 o 7 4 0 2506.72 2478.90 151.39 o 8 4 0 536.24 546.92 95.54 o 9 4 0 4.91 -29.90 67.05 o 10 4 0 71.46 65.18 61.22 o 11 4 0 325.28 171.75 117.04 o 12 4 0 69.38 97.71 104.07 o 13 4 0 739.70 852.00 186.76 o -12 5 0 49.43 53.81 97.83 o -11 5 0 6.09 -61.70 71.75 o -10 5 0 1220.70 1333.91 164.50 o -9 5 0 768.81 659.71 92.11 o -8 5 0 403.69 381.41 72.13 o -7 5 0 1221.22 1139.22 116.47 o -6 5 0 2641.54 2311.57 78.11 o -5 5 0 1580.24 1440.02 61.51 o -4 5 0 10567.35 10393.18 171.04 o -3 5 0 8610.57 8872.23 188.98 o -2 5 0 3588.45 3186.38 76.11 o -1 5 0 1477.40 1348.88 75.76 o 0 5 0 4044.89 3823.74 101.40 o 1 5 0 290.75 267.26 56.61 o 2 5 0 1803.84 1350.74 52.57 o 3 5 0 3461.86 3844.05 81.60 o 4 5 0 678.37 508.88 79.00 o 5 5 0 1941.51 1314.44 112.72 o 6 5 0 383.63 336.12 77.35 o 7 5 0 1382.08 1625.37 140.83 o 8 5 0 5254.49 5464.13 247.44 o 9 5 0 2761.14 2627.62 184.47 o 10 5 0 174.14 29.01 86.38 o 11 5 0 86.46 102.66 73.53 o 12 5 0 291.77 328.74 120.99 o 13 5 0 482.27 490.31 148.47 o -12 6 0 1444.49 1398.03 196.68 o -11 6 0 73.26 -60.94 90.71 o -10 6 0 88.76 88.04 88.04 o -9 6 0 26.82 90.45 79.00 o -8 6 0 340.20 435.87 201.52 o -7 6 0 516.21 456.73 74.66 o -6 6 0 2520.86 2741.17 123.87 o -5 6 0 204.53 193.92 37.45 o -4 6 0 1900.33 1863.39 69.33 o -3 6 0 41.95 62.43 26.82 o -2 6 0 7490.44 7503.88 236.06 o -1 6 0 945.58 942.41 59.90 o 0 6 0 1687.02 1557.11 69.86 o 1 6 0 275.90 219.23 35.58 o 2 6 0 7.46 -6.91 21.81 o 3 6 0 4414.53 3901.86 178.11 o 4 6 0 12946.06 12344.23 364.87 o 5 6 0 88.97 179.64 68.95 o 6 6 0 978.96 742.46 105.85 o 7 6 0 1.80 -58.27 58.27 o 8 6 0 13.71 26.33 76.71 o 9 6 0 335.20 411.56 114.50 o 10 6 0 1990.25 1932.36 173.66 o 11 6 0 235.54 123.79 94.27 o 12 6 0 107.33 41.47 91.98 o 13 6 0 24.99 114.88 106.74 o -11 7 0 1432.36 1091.05 186.63 o -10 7 0 97.83 26.21 103.81 o -9 7 0 13.12 106.74 90.33 o -8 7 0 131.55 209.15 93.38 o -7 7 0 459.16 273.02 93.76 o -6 7 0 1852.34 1917.50 164.50 o -5 7 0 2144.57 2130.69 80.92 o -4 7 0 935.56 897.26 55.99 o -3 7 0 113.77 74.31 38.85 o -2 7 0 298.71 301.74 48.07 o -1 7 0 6997.72 6493.85 177.73 o 0 7 0 1397.69 1392.06 72.89 o 1 7 0 10.45 3.59 27.20 o 2 7 0 243.67 262.79 37.24 o 3 7 0 137.94 98.34 42.05 o 4 7 0 233.60 212.41 26.14 o 5 7 0 16395.75 15444.85 453.92 o 6 7 0 300.92 337.13 91.34 o 7 7 0 4110.48 3657.85 208.90 o 8 7 0 405.38 370.72 103.94 o 9 7 0 228.99 202.79 95.67 o 10 7 0 401.57 179.25 99.87 o 11 7 0 922.09 668.80 139.43 o 12 7 0 353.98 652.90 174.93 o 13 7 0 29.03 50.38 106.61 o -11 8 0 106.36 65.14 105.97 o -10 8 0 979.04 1142.06 182.18 o -9 8 0 94.42 68.19 91.47 o -8 8 0 544.69 662.82 134.60 o -7 8 0 582.32 565.62 119.46 o -6 8 0 1402.40 1170.30 152.28 o -5 8 0 295.86 279.63 86.51 o -4 8 0 3747.90 3514.93 101.00 o -3 8 0 191.95 180.96 44.28 o -2 8 0 2055.37 1970.72 96.48 o -1 8 0 1817.14 1854.12 101.39 o 0 8 0 2511.53 2651.20 117.81 o 1 8 0 1684.79 1465.59 76.13 o 2 8 0 723.25 812.11 58.98 o 3 8 0 732.51 582.79 46.94 o 4 8 0 155.61 174.67 79.64 o 5 8 0 43.48 96.69 76.46 o 6 8 0 1042.81 1096.13 135.87 o 7 8 0 126.32 82.06 86.76 o 8 8 0 1518.35 1372.71 158.64 o 9 8 0 158.62 206.10 107.25 o 10 8 0 333.90 220.60 110.94 o 11 8 0 1.77 -75.82 75.82 o 12 8 0 90.75 136.71 77.29 o 13 8 0 19.65 40.20 110.05 o -10 9 0 201.01 230.40 121.50 o -9 9 0 521.34 351.26 120.10 o -8 9 0 1173.14 811.16 152.92 o -7 9 0 232.66 322.38 97.83 o -6 9 0 911.50 717.91 131.42 o -5 9 0 41.46 29.77 72.52 o -4 9 0 1848.41 1907.49 107.34 o -3 9 0 1765.83 1799.97 99.92 o -2 9 0 6290.49 6227.54 253.42 o -1 9 0 246.66 321.17 90.07 o 0 9 0 1671.14 1592.51 86.78 o 1 9 0 133.49 127.67 42.07 o 2 9 0 1544.31 1612.43 81.89 o 3 9 0 4255.21 3892.95 168.19 o 4 9 0 2328.57 2423.43 180.65 o 5 9 0 8.77 24.81 89.56 o 6 9 0 450.75 414.10 115.13 o 7 9 0 3.63 -80.79 80.79 o 8 9 0 233.49 150.25 106.87 o 9 9 0 727.40 543.36 129.89 o 10 9 0 614.03 669.18 139.69 o 11 9 0 32.76 168.44 105.97 o 12 9 0 4.73 -85.87 85.87 o -10 10 0 5.17 -0.64 100.63 o -9 10 0 0.16 -1.53 90.07 o -8 10 0 79.23 107.88 98.34 o -7 10 0 398.58 470.21 125.69 o -6 10 0 35.39 -55.60 55.60 o -5 10 0 22.07 90.96 76.08 o -4 10 0 598.80 642.55 132.56 o -3 10 0 1862.18 1607.79 115.52 o -2 10 0 2881.11 2826.72 415.57 o -1 10 0 2770.70 2327.20 113.21 o 0 10 0 2327.44 2439.47 115.39 o 1 10 0 41.17 123.24 45.28 o 2 10 0 49.75 52.92 58.52 o 3 10 0 1421.69 1233.28 99.74 o 4 10 0 1626.94 1569.65 167.68 o 5 10 0 1490.00 1520.42 172.13 o 6 10 0 220.17 221.75 106.48 o 7 10 0 0.96 60.30 100.38 o 8 10 0 81.23 137.27 104.70 o 9 10 0 990.60 1055.68 163.10 o 10 10 0 76.01 21.75 85.87 o 11 10 0 570.69 572.11 149.99 o 12 10 0 3.98 -97.96 105.34 o -9 11 0 1.05 103.05 114.37 o -8 11 0 8.40 -19.46 91.47 o -7 11 0 134.42 129.89 81.93 o -6 11 0 582.67 685.08 132.82 o -5 11 0 1090.57 1151.60 153.81 o -4 11 0 4418.98 4669.13 258.00 o -3 11 0 172.10 160.39 62.12 o -2 11 0 37.15 50.68 55.57 o -1 11 0 1158.96 1071.55 92.31 o 0 11 0 1960.97 1884.85 155.91 o 1 11 0 1583.59 1568.77 96.62 o 2 11 0 3107.22 3247.77 169.33 o 3 11 0 251.36 358.76 124.80 o 4 11 0 301.63 351.51 113.99 o 5 11 0 228.55 91.47 113.23 o 6 11 0 328.90 471.35 129.89 o 7 11 0 87.50 3.31 92.49 o 8 11 0 3.91 -26.46 86.51 o 9 11 0 15.10 131.67 106.48 o 10 11 0 428.19 481.53 151.52 o 11 11 0 124.96 135.49 109.92 o 12 11 0 205.83 336.12 142.74 o -8 12 0 744.07 905.30 174.93 o -7 12 0 11.85 18.96 81.80 o -6 12 0 26.12 170.86 88.29 o -5 12 0 122.67 95.80 76.46 o -4 12 0 41.90 -10.30 63.99 o -3 12 0 1335.99 1418.98 108.68 o -2 12 0 102.08 79.82 56.40 o -1 12 0 363.24 316.69 68.39 o 0 12 0 403.74 454.06 92.17 o 1 12 0 549.60 523.25 74.47 o 2 12 0 1439.84 1348.54 171.24 o 3 12 0 3543.35 3788.51 260.17 o 4 12 0 287.12 284.85 128.87 o 5 12 0 942.26 965.99 159.53 o 6 12 0 95.46 54.70 100.63 o 7 12 0 888.93 744.24 158.77 o 8 12 0 309.07 247.83 121.88 o 9 12 0 79.77 164.37 115.77 o 10 12 0 85.54 7.25 110.17 o 11 12 0 17.66 32.06 118.57 o -7 13 0 1811.21 1921.16 224.54 o -6 13 0 182.36 282.94 116.03 o -5 13 0 8.51 -33.08 71.12 o -4 13 0 7.24 -2.93 73.41 o -3 13 0 268.02 414.99 105.47 o -2 13 0 257.52 218.05 119.27 o -1 13 0 2480.24 2335.04 134.22 o 0 13 0 642.27 670.39 85.16 o 1 13 0 49.97 -45.80 45.80 o 2 13 0 240.88 267.93 117.55 o 3 13 0 1958.87 1834.65 203.04 o 4 13 0 10.60 133.71 108.14 o 5 13 0 842.10 796.91 170.86 o 6 13 0 198.58 395.66 130.66 o 7 13 0 134.06 80.02 111.95 o 8 13 0 381.67 339.42 127.09 o 9 13 0 521.90 280.65 140.20 o 10 13 0 0.10 3.94 116.79 o -6 14 0 711.69 817.65 157.88 o -5 14 0 0.05 82.06 95.29 o -4 14 0 162.50 155.21 95.42 o -3 14 0 91.86 181.67 82.95 o -2 14 0 13.04 10.27 52.36 o -1 14 0 0.95 56.21 56.97 o 0 14 0 437.24 454.62 78.28 o 1 14 0 249.82 447.82 139.69 o 2 14 0 30.51 95.42 106.74 o 3 14 0 135.95 54.96 112.72 o 4 14 0 1226.13 1449.68 202.28 o 5 14 0 380.83 419.07 145.29 o 6 14 0 804.09 606.59 168.57 o 7 14 0 190.82 274.92 136.38 o 8 14 0 45.08 67.81 108.01 o 9 14 0 6.08 -92.74 102.29 o 10 14 0 319.13 514.99 169.20 o -5 15 0 172.87 296.17 125.95 o -4 15 0 55.08 57.12 86.89 o -3 15 0 183.26 111.95 82.44 o -2 15 0 319.09 344.51 102.16 o -1 15 0 133.34 125.88 62.11 o 0 15 0 45.47 148.47 111.83 o 1 15 0 1145.32 1284.04 188.41 o 2 15 0 1.84 168.69 119.71 o 3 15 0 62.86 113.99 113.74 o 4 15 0 19.63 -25.83 120.35 o 5 15 0 9.14 -17.81 114.63 o 6 15 0 267.82 79.77 133.45 o 7 15 0 320.70 556.72 154.19 o 8 15 0 114.51 398.84 157.37 o 9 15 0 0.19 -83.33 109.79 o -4 16 0 16.70 -40.33 92.36 o -3 16 0 180.68 -11.07 86.89 o -2 16 0 6.27 -25.32 72.90 o -1 16 0 381.24 460.10 87.30 o 0 16 0 0.01 79.00 103.68 o 1 16 0 2.09 -22.26 111.70 o 2 16 0 360.06 243.12 145.41 o 3 16 0 409.56 616.51 172.64 o 4 16 0 18.68 75.44 128.87 o 5 16 0 1.11 17.94 122.26 o 6 16 0 56.60 30.79 129.38 o 7 16 0 43.72 -81.29 123.79 o 0 17 0 28.35 180.14 134.85 o 1 17 0 34.09 80.66 124.80 o 2 17 0 42.16 220.35 138.67 o 3 17 0 21.03 -83.84 123.91 o 4 17 0 122.05 -82.44 113.74 o 5 17 0 0.57 78.50 128.62 o -5 -17 1 0.64 -28.62 124.80 o -4 -17 1 163.80 232.94 152.41 o -3 -17 1 222.23 120.22 136.64 o -2 -17 1 89.51 186.00 140.32 o -1 -17 1 22.81 -29.90 115.13 o 0 -17 1 1.02 98.47 123.15 o -7 -16 1 34.91 4.83 120.61 o -6 -16 1 688.92 576.69 194.27 o -5 -16 1 11.79 -7.00 117.17 o -4 -16 1 30.49 -50.12 118.82 o -3 -16 1 44.59 -9.92 133.33 o -2 -16 1 497.74 562.95 164.62 o -1 -16 1 37.77 -28.12 100.38 o 0 -16 1 444.11 545.52 155.85 o 1 -16 1 27.97 33.33 119.84 o 2 -16 1 267.55 121.88 94.14 o 3 -16 1 0.15 -29.26 73.92 o -8 -15 1 29.37 128.11 124.29 o -7 -15 1 141.67 69.72 127.48 o -6 -15 1 262.06 151.90 151.14 o -5 -15 1 256.73 267.80 146.81 o -4 -15 1 19.11 -27.48 104.58 o -3 -15 1 7.45 -63.48 123.79 o -2 -15 1 53.60 52.92 108.01 o -1 -15 1 758.20 728.34 165.26 o 0 -15 1 287.35 148.21 115.39 o 1 -15 1 1492.51 1435.74 124.13 o 2 -15 1 2.52 57.25 80.47 o 3 -15 1 0.23 128.37 82.06 o 4 -15 1 18.18 51.02 88.16 o 5 -15 1 33.50 106.87 91.98 o -9 -14 1 121.00 527.46 170.60 o -8 -14 1 112.99 83.20 121.88 o -7 -14 1 646.66 882.15 181.80 o -6 -14 1 4.21 33.59 121.37 o -5 -14 1 4.28 208.77 121.11 o -4 -14 1 549.69 525.42 152.92 o -3 -14 1 13.75 71.37 119.08 o -2 -14 1 285.42 248.08 131.80 o -1 -14 1 62.13 40.97 91.34 o 0 -14 1 206.98 160.66 97.01 o 1 -14 1 990.83 1026.51 106.44 o 2 -14 1 939.54 941.69 105.82 o 3 -14 1 317.43 421.23 111.19 o 4 -14 1 37.25 163.61 93.25 o 5 -14 1 10.28 -0.89 77.48 o 6 -14 1 17.21 231.54 102.67 o -10 -13 1 4.73 176.71 125.69 o -9 -13 1 61.26 -33.33 113.99 o -8 -13 1 677.76 656.84 164.11 o -7 -13 1 8.98 -88.80 94.78 o -6 -13 1 909.06 769.30 163.86 o -5 -13 1 4.17 -102.16 102.16 o -4 -13 1 295.51 228.49 119.08 o -3 -13 1 2.41 40.97 100.63 o -2 -13 1 2884.03 2567.57 230.91 o -1 -13 1 973.15 964.84 158.01 o 0 -13 1 539.67 523.43 82.18 o 1 -13 1 969.65 1017.34 101.33 o 2 -13 1 1183.80 1083.74 105.66 o 3 -13 1 19.40 153.88 73.28 o 4 -13 1 941.32 684.83 131.42 o 5 -13 1 3.27 -16.92 70.23 o 6 -13 1 150.57 203.93 93.76 o 7 -13 1 8.36 -44.91 69.08 o -11 -12 1 261.84 109.54 131.80 o -10 -12 1 19.22 -68.83 104.45 o -9 -12 1 241.04 180.14 126.46 o -8 -12 1 99.69 252.02 120.86 o -7 -12 1 220.10 324.29 128.11 o -6 -12 1 268.28 200.88 115.13 o -5 -12 1 1286.31 1055.30 171.11 o -4 -12 1 71.47 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