Acta Crystallographica Section C

Crystal Structure Communications

Volume 62, Part 10 (October 2006)


organic compounds



gg3041 scheme

Acta Cryst. (2006). C62, o618-o624    [ doi:10.1107/S0108270106034974 ]

Four substituted benzohydrazides: hydrogen-bonded structures in one, two and three dimensions

S. M. S. V. Wardell, T. R. A. Vasconcelos, M. V. N. de Souza, J. L. Wardell, J. N. Low and C. Glidewell

Abstract: The molecules of 2,6-dichlorobenzohydrazide, C7H6Cl2N2O, are linked into simple chains by a single N-H...O hydrogen bond, while in the isomeric compound 2,4-dichlorobenzohydrazide, the molecules are linked by N-H...N and N-H...O hydrogen bonds into complex sheets comprising an inner polar layer sandwiched between two non-polar layers. In 4-amino-2-chlorobenzohydrazide monohydrate, C7H8ClN3O·H2O, the components are linked into a three-dimensional framework by a combination of O-H...O, O-H...N, N-H...N and N-H...O hydrogen bonds, and in 2-nitrobenzohydrazide, C7H7N3O3, a three-dimensional framework is formed by a combination of N-H...N and N-H...O hydrogen bonds

Formula: C7H6Cl2N2O, C7H8ClN3O·H2O and C7H7N3O3


hkldisplay filedownload file

Structure factor file (CIF format) (96.0 kbytes)
[ doi:10.1107/S0108270106034974/gg3041Isup2.hkl ]
Contains datablock I


hkldisplay filedownload file

Structure factor file (CIF format) (89.3 kbytes)
[ doi:10.1107/S0108270106034974/gg3041IIsup3.hkl ]
Contains datablock II


hkldisplay filedownload file

Structure factor file (CIF format) (103.9 kbytes)
[ doi:10.1107/S0108270106034974/gg3041IIIsup4.hkl ]
Contains datablock III


hkldisplay filedownload file

Structure factor file (CIF format) (54.1 kbytes)
[ doi:10.1107/S0108270106034974/gg3041IVsup5.hkl ]
Contains datablock IV


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