Crystal Structure Communications

 

Acta Cryst. (2006). C62, i91-i93  [ doi:10.1107/S0108270106028678 ]

Centrosymmetric aliovalent KTP isomorphs KM^III_0.5Nb_0.5OPO₄ (M = Cr and Fe)

A. A. Babaryk, I. V. Zatovsky, V. N. Baumer, N. S. Slobodyanik and O. V. Shishkin

Synopsis: The title isotypic orthorhombic aliovalent KTP isomorphs contain octahedrally coordinated Cr³⁺ or Fe³⁺ and Nb⁵⁺ cations in cis-trans-arranged chains; these are linked by PO₄ anions into a framework containing cavities in which K⁺ cations are located.

Formula: KCr_0.5Nb_0.5OPO₄ and KFe_0.5Nb_0.5OPO₄

Online 31 October 2006

 

Acta Cryst. (2006). C62, i94-i96  [ doi:10.1107/S010827010604176X ]

Ca_7.96Cu_0.04Ge₅O₁₈: a new calcium germanate with GeO₄ and Ge₃O₁₀ units

G. J. Redhammer, G. Roth and G. Amthauer

Synopsis: The crystal structure of a new calcium germanate contains isolated GeO₄ and Ge₃O₁₀ units which are connected by six- and sevenfold coordinated Ca sites.

Formula: Ca_7.96Cu_0.04Ge₅O₁₈

Online 31 October 2006

 

Acta Cryst. (2006). C62, m507-m509  [ doi:10.1107/S0108270106037504 ]

Effects of d-orbital occupancy on the geometry of the trigonal-bipyramidal complexes [M^IICl₃(Hdabco)(dabco)]_n, where M is Mn, Co, Ni or Cu and dabco is 1,4-diazabicyclo[2.2.2]octane

R. G. Pritchard, M. Ali, A. Munim and A. Uddin

Formula: [MnCl₃(C₆H₁₃N₂)(C₆H₁₂N₂)] and [CoCl₃(C₆H₁₃N₂)(C₆H₁₂N₂)]

Online 14 October 2006

 

Acta Cryst. (2006). C62, m510-m512  [ doi:10.1107/S0108270106037310 ]

Bis[bis(2-pyridylcarbonyl)aminato]iron(III) perchlorate acetonitrile disolvate

H. Kooijman, S. Tanase, E. Bouwman, J. Reedijk and A. L. Spek

Formula: [Fe(C₁₂H₈N₃O₂)₂]ClO₄·2C₂H₃N

Online 14 October 2006

 

Acta Cryst. (2006). C62, m513-m515  [ doi:10.1107/S010827010603767X ]

catena-Poly[[[triaquacobalt(II)]--2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carboxylato(2-)] 1.72-hydrate]

O. Sahin, O. Büyükgüngör, D. A. Köse, B. Zümreoglu-Karan and H. Necefoglu

Formula: [Co(C₅H₂N₂O₄)(H₂O)₃]·1.72H₂O

Online 14 October 2006

 

Acta Cryst. (2006). C62, m516-m518  [ doi:10.1107/S0108270106037565 ]

Poly[[-aqua-bis(-2,4-dichlorophenoxyacetato)barium(II)] monohydrate]

C.-S. Gu, X.-M. Hao, S.-X Guan and J.-W. Liu

Formula: [Ba(C₈H₅Cl₂O₃)₂(H₂O)]·H₂O

Online 14 October 2006

 

Acta Cryst. (2006). C62, m519-m521  [ doi:10.1107/S0108270106037747 ]

(Acetonitrile-N){2-[bis(2-pyridylethyl)amino]ethanol-⁴N,N',N'',O}zinc(II) bis(perchlorate) monohydrate

H.-C. Liang, M. M. Hetu, K. A. Wheeler, L. N. Zakharov and A. L. Rheingold

Formula: [Zn(C₂H₃N)(C₁₆H₂₁N₃O)](ClO₄)₂·H₂O

Online 14 October 2006

 

Acta Cryst. (2006). C62, m522-m524  [ doi:10.1107/S0108270106038844 ]

catena-Poly[[[tetraaquazinc(II)]--4,4'-bipyridine] bis(4-hydroxybenzenesulfonate) trihydrate]

Y.-L. Wang

Formula: [Zn(C₁₀H₈N₂)(H₂O)₄](C₆H₅O₄S)₂·3H₂O

Online 14 October 2006

 

Acta Cryst. (2006). C62, m525-m526  [ doi:10.1107/S0108270106038108 ]

catena-Poly[4,4'-bipyridinium [[cis-dichloromanganese(II)]-di--chloro]], a novel manganese(II) coordination polymer with 4,4'-bipyridinium

M.-X. Li and S.-Z. Li

Formula: (C₁₀H₁₀N₂)[MnCl₄]

Online 19 October 2006

 

Acta Cryst. (2006). C62, m527-m530  [ doi:10.1107/S0108270106039072 ]

Bis[bis(3,5-dimethylpyrazol-1-yl)methane]bis(isothiocyanato)cadmium(II) and catena-poly[[di--dicyanamidato-bis{[bis(3,5-dimethylpyrazol-1yl)methane]cadmium(II)}]-di--dicyanamidato]

Q.-Y. Li, H.-X. Li, X.-Y. Tang, Z. Yong and J.-P. Lang

Formula: [Cd(NCS)₂(C₁₁H₁₆N₄)₂] and [Cd₂(C₂N₃)₄(C₁₁H₁₆N₄)₂]

Online 31 October 2006

 

Acta Cryst. (2006). C62, m531-m534  [ doi:10.1107/S0108270106038662 ]

The effect of counter-ions on the supramolecular arrangement of (benzonitrile)[1,2-bis(diphenylphosphino)ethane](⁵-cyclopentadienyl)iron(II) cations

M. T. Duarte, M. F. M. Piedade, M. P. Robalo, C. Jacob and M. H. Garcia

Formula: [Fe(C₅H₅)(C₇H₄N₂O₂)(C₂₆H₄P₂)]I

Online 31 October 2006

 

Acta Cryst. (2006). C62, m535-m537  [ doi:10.1107/S0108270106039527 ]

trans-Bis[1-benzyl-3-(2,3,4,5,6-pentafluorobenzyl)benzimidazol-2-ylidene]dibromopalladium(II)

A. G. Gökçe, S. Gülcemal, M. Aygün, B. Çetinkaya and O. Büyükgüngör

Formula: [PdBr₂(C₂₁H₁₃F₅N₂)₂]

Online 31 October 2006

 

Acta Cryst. (2006). C62, m538-m540  [ doi:10.1107/S0108270106038996 ]

Hydrogen-bonded supramolecular arrays of aqua[20-(4-carboxyphenyl)-5,10,15-triphenylporphyrinato]zinc(II) in crystals of its nitrobenzene disolvate

S. Lipstman, S. Muniappan and I. Goldberg

Formula: [Zn(C₄₅H₂₈N₄O₂)(H₂O)]·2C₆H₅NO₂

Online 31 October 2006

 

Acta Cryst. (2006). C62, m541-m544  [ doi:10.1107/S0108270106041746 ]

The first compound with an unusual type of anion, [Li(SR)₂]^-: bis(₂-aqua-d₂)tetrakis(aqua-d₂)dilithium(I) bis[bis(tri-tert-butoxysilanethiolato-²O,S)lithate(I)] dihydrate-d₂

M. Kloskowska, J. Chojnacki, W. Wojnowski and B. Becker

Formula: [Li₂(D₂O)₆][Li(C₁₂H₂₇O₃SSi)₂]₂·2D₂O

Online 31 October 2006

 

Acta Cryst. (2006). C62, m545-m547  [ doi:10.1107/S0108270106040972 ]

catena-Poly[[[tetrakis(-acetato-²O:O')dirhodium(II)]--[1,3-bis(dimethylamino)propan-2-ol-²N:N']] tetrahydrofuran hemisolvate]

A. Pevec, A. Demsar, K. Aoki and I. Turel

Formula: [Rh₂(C₂H₃O₂)₄(C₇H₁₈N₂O)]·0.5C₄H₈O

Online 31 October 2006

 

Acta Cryst. (2006). C62, m548-m549  [ doi:10.1107/S0108270106039965 ]

catena-Poly[[diiodozinc(II)]--4,4'-bipyridine-²N:N']

L.-Q. Fan and J.-H. Wu

Formula: [ZnI₂(C₁₀H₈N₂)]

Online 31 October 2006

 

Acta Cryst. (2006). C62, m550-m552  [ doi:10.1107/S0108270106040935 ]

A dimeric cobalt(II)-suberate complex with 3-aminopyridine

N. Lah and I. Leban

Formula: [Co₂(C₈H₁₂O₄)Cl₂(C₅H₆N₂)₄(CH₄O)₂]

Online 31 October 2006

 

Acta Cryst. (2006). C62, m553-m555  [ doi:10.1107/S0108270106040765 ]

Dichloro(4,10-dimethyl-1,4,7,10-tetraazabicyclo[5.5.2]tetradecane)iron(III) hexafluorophosphate

J. M. McClain II, D. L. Maples, R. D. Maples, D. L. Matz, S. M. Harris, A. D. L. Nelson, J. D. Silversides, S. J. Archibald and T. J. Hubin

Formula: [FeCl₂(C₁₂H₂₆N₄)]PF₆

Online 31 October 2006

 

Acta Cryst. (2006). C62, m556-m558  [ doi:10.1107/S0108270106040121 ]

A zigzag chain structure in catena-poly[[[tetra--acetamidato-⁴N:O;⁴O:N-dirhodium(II,III)]--chloro] methanol solvate]

M. Ebihara and Y. Fuma

Formula: [Rh₂(C₂H₄NO)₄Cl]·CH₄O

Online 31 October 2006

 

Acta Cryst. (2006). C62, m559-m562  [ doi:10.1107/S0108270106041345 ]

N,N'-Bis(2-pyridylmethyl)ferrocene-1,1'-diyldicarboxamide and N,N'-bis(3-pyridylmethyl)ferrocene-1,1'-diyldicarboxamide

Y.-C. Shi, B.-B. Zhu and X.-B. Jing

Formula: [Fe(C₁₂H₁₁N₂O)₂]

Online 31 October 2006

 

Acta Cryst. (2006). C62, m563-m565  [ doi:10.1107/S0108270106041692 ]

Poly[aqua-₃-2,2-dimethylmalonato-zinc(II)]

M.-L. Guo and Y.-N. Zhao

Formula: [Zn(C₅H₆O₄)(H₂O)]

Online 31 October 2006

 

Acta Cryst. (2006). C62, m566-m568  [ doi:10.1107/S0108270106040777 ]

A second polymorph of [H₃N(CH₂)₃NH₃][V₄O₁₀]

N. F. Stephens and P. Lightfoot

Formula: (C₃H₁₂N₂)[V₄O₁₀]

Online 31 October 2006

 

Acta Cryst. (2006). C62, o633-o635  [ doi:10.1107/S0108270106037358 ]

Invariom-model refinement of L-valinol

B. Dittrich, P. Munshi and M. A. Spackman

Formula: C₅H₁₃NO

Online 14 October 2006

 

Acta Cryst. (2006). C62, o636-o638  [ doi:10.1107/S0108270106037127 ]

rac-(Z)-Ethyl 2-bromo-2-[(3R,5R)-3-bromo-5-methyltetrahydrofuran-2-ylidene]acetate

F. Loiseau, R. Neier, G. Labat and H. Stoeckli-Evans

Formula: C₉H₁₂Br₂O₃

Online 14 October 2006

 

Acta Cryst. (2006). C62, o639-o642  [ doi:10.1107/S0108270106037930 ]

N-Cyclohexyl-2-[5-(4-pyridyl)-4-(p-tolyl)-4H-1,2,4-triazol-3-ylsulfanyl]acetamide dihydrate

M. Dinçer, N. Özdemir, A. Çetin, T. Keser and O. Büyükgüngör

Formula: C₂₂H₂₅N₅OS·2H₂O

Online 14 October 2006

 

Acta Cryst. (2006). C62, o643-o646  [ doi:10.1107/S0108270106037668 ]

N-HN and C-H interactions in 4-amino-3-methyl-5-(p-tolyl)-4H-1,2,4-triazole and 4-amino-3-methyl-5-phenyl-4H-1,2,4-triazole

O. Sahin, O. Büyükgüngör, S. Sasmaz, N. Gümrükçüoglu and C. Kantar

Formula: C₁₀H₁₂N₄ and C₉H₁₀N₄

Online 14 October 2006

 

Acta Cryst. (2006). C62, o647-o649  [ doi:10.1107/S0108270106039205 ]

3-Nitrophenylacetic acid: a three-dimensional hydrogen-bonded framework structure containing substructures in zero, one and two dimensions

S. M. S. V. Wardell, J. L. Wardell, J. N. Low and C. Glidewell

Formula: C₈H₇NO₄

Online 19 October 2006

 

Acta Cryst. (2006). C62, o650-o652  [ doi:10.1107/S0108270106038522 ]

3-Diphenylphosphino-1,2:5,6-di-O-isopropylidene-4-O-methyl-1D-chiro-inositol

G. J. Gainsford, C. Lensink and A. Falshaw

Formula: C₂₅H₃₁O₆P

Online 19 October 2006

 

Acta Cryst. (2006). C62, o653-o655  [ doi:10.1107/S0108270106038583 ]

1:1 Adduct of (S,S)-4-amino-3,5-bis(1-hydroxyethyl)-1,2,4-triazole with (S,S)-1,2-bis(2-hydroxypropionyl)hydrazine stabilized by eight hydrogen bonds

U. Beckmann and S. Brooker

Formula: C₆H₁₂N₄O₂·C₆H₁₂N₂O₄

Online 19 October 2006

 

Acta Cryst. (2006). C62, o656-o658  [ doi:10.1107/S0108270106039825 ]

Solvent-free synthesis and crystal structure of (Ph₃PI)I₅, the third member in the series Ph₃P(I₂)_n (n = 1, 2 and 3)

R. G. Pritchard and L. Moreland

Formula: C₁₈H₁₅IP⁺·I₅^-

Online 19 October 2006

 

Acta Cryst. (2006). C62, o659-o660  [ doi:10.1107/S0108270106037759 ]

9-(1,3-Anhydro--D-psicofuranosyl)adenine

J. Roivainen, I. Mikhailopulo, H. Reuter and H. Eickmeier

Formula: C₁₁H₁₃N₅O₄

Online 19 October 2006

 

Acta Cryst. (2006). C62, o661-o662  [ doi:10.1107/S0108270106041230 ]

[(4,4-Dimethyl-2-oxo-1,3-oxazolidin-3-yl)methyl]phosphonic acid

P. Todorov, E. Naydenova, R. Petrova, B. Shivachev and K. Troev

Formula: C₆H₁₂NO₅P

Online 31 October 2006

 

Acta Cryst. (2006). C62, o663-o665  [ doi:10.1107/S0108270106040753 ]

1,1'-(Ethenylidene)bis(4-chlorobenzene)

M. A. Jabbar, I. Aritome, H. Shimakoshi and Y. Hisaeda

Formula: C₁₄H₁₀Cl₂

Online 31 October 2006

 

Acta Cryst. (2006). C62, o666-o668  [ doi:10.1107/S0108270106041151 ]

1-(4,6-Diethoxypyrimidin-2-yl)-2-thioxo-2,3-dihydropyrido[2,3-d]pyrimidin-4(1H)-one

S.-J. Xue, Q.-D. Wang and J.-Z. Li

Formula: C₁₅H₁₅N₅O₃S

Online 31 October 2006