Acta Crystallographica Section C

Crystal Structure Communications

Volume 63, Part 1 (January 2007)


organic compounds



gg3058 scheme

Acta Cryst. (2007). C63, o68-o72    [ doi:10.1107/S0108270106052486 ]

2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions

M. A. Peralta, M. N. V. de Souza, S. M. S. V. Wardell, J. L. Wardell, J. N. Low and C. Glidewell

Abstract: In 2,3-dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, C15H15N3O3·CHCl3, the hydrazone molecules are linked by a combination of N-H...N and C-H...N hydrogen bonds into chains from which the chloroform molecules are pendent. 3,4,5-Trimethoxybenzaldehyde isonicotinoylhydrazone forms two stoichiometric hydrates. In the monohydrate, C16H17N3O4·H2O, the components are linked into sheets by a combination of O-H...O, O-H...N and N-H...N hydrogen bonds, and in the dihydrate, C16H17N3O4·2H2O, a combination of O-H...O, O-H...N and N-H...O hydrogen bonds links the components into a three-dimensional framework structure.

Formula: C15H15N3O3·CHCl3, C16H17N3O4·H2O and C16H17N3O4·2H2O


hkldisplay filedownload file

Structure factor file (CIF format) (202.3 kbytes)
[ doi:10.1107/S0108270106052486/gg3058Isup2.hkl ]
Contains datablock I


hkldisplay filedownload file

Structure factor file (CIF format) (180.8 kbytes)
[ doi:10.1107/S0108270106052486/gg3058IIsup3.hkl ]
Contains datablock II


hkldisplay filedownload file

Structure factor file (CIF format) (190.7 kbytes)
[ doi:10.1107/S0108270106052486/gg3058IIIsup4.hkl ]
Contains datablock III


Notes:

To open or display or play some files, you may need to set your browser up to use the appropriate software. See the full list of file types for an explanation of the different file types and their related mime types and, where available links to sites from where the appropriate software may be obtained.

The download button will force most browsers to prompt for a file name to store the data on your hard disk.

Where possible, images are represented by thumbnails.

 bibliographic record in  format

  Find reference:   Volume   Page   
  Search:     From   to      Advanced search

Copyright © International Union of Crystallography
IUCr Webmaster