################################################################### # tris(acetylacetonato)(1,10-phenanthroline)-erbium(III) # # Gururaj M. Neelgund et al. # # Acta Crystallographica C (2006) # ################################################################### # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title 'tris(acetylacetonato)(1,10-phenanthroline)erbium(III) in P21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 400.56 _exptl_crystal_F_000 1284.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.4660 _cell_length_b 21.0250 _cell_length_c 14.6430 _cell_angle_alpha 90.000 _cell_angle_beta 98.670 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9977.51 10055.13 140.57 o 4 0 0 177.15 196.38 22.29 o 6 0 0 28393.29 29405.98 415.25 o 8 0 0 4341.61 4093.54 126.37 o 10 0 0 3.35 69.51 97.04 o 1 1 0 43601.24 47762.73 492.57 o 2 1 0 24343.22 25390.95 225.17 o 3 1 0 1891.44 2031.30 35.98 o 4 1 0 13720.21 13254.98 141.88 o 5 1 0 1800.46 1772.19 43.27 o 6 1 0 323.77 277.36 24.44 o 7 1 0 6186.96 5927.52 100.12 o 8 1 0 2648.71 2575.92 70.96 o 9 1 0 211.81 269.93 33.44 o 10 1 0 2065.37 2262.15 91.77 o 11 1 0 366.12 593.87 73.61 o 0 2 0 55479.80 62449.72 1537.87 o 1 2 0 8107.50 8897.12 110.83 o 2 2 0 2115.02 2169.90 51.00 o 3 2 0 16556.77 16456.94 162.07 o 4 2 0 837.85 771.67 28.91 o 5 2 0 13381.72 13293.54 152.07 o 6 2 0 2207.85 2097.29 52.36 o 7 2 0 3227.92 3271.73 71.87 o 8 2 0 528.07 474.30 35.01 o 9 2 0 3091.37 3293.59 94.78 o 10 2 0 31.28 -17.08 33.91 o 11 2 0 855.98 950.44 97.54 o 1 3 0 26273.24 27858.39 264.78 o 2 3 0 16.10 15.85 12.89 o 3 3 0 30.06 47.99 11.01 o 4 3 0 5577.66 5617.89 77.43 o 5 3 0 16755.55 16979.60 183.11 o 6 3 0 828.62 817.42 34.20 o 7 3 0 13064.79 12841.06 165.09 o 8 3 0 1552.96 1402.47 52.08 o 9 3 0 533.86 601.67 69.89 o 10 3 0 69.71 116.63 58.26 o 11 3 0 764.03 864.24 87.42 o 0 4 0 18286.14 21164.52 368.48 o 1 4 0 3854.39 3795.60 44.89 o 2 4 0 5658.80 5545.12 213.17 o 3 4 0 10338.40 10102.58 111.80 o 4 4 0 3041.79 3266.41 121.66 o 5 4 0 3990.35 4082.41 64.86 o 6 4 0 13015.19 13049.81 158.00 o 7 4 0 459.74 466.56 38.39 o 8 4 0 2641.03 2478.02 79.37 o 9 4 0 1923.78 2031.19 84.37 o 10 4 0 69.74 122.50 45.83 o 11 4 0 427.06 382.50 74.37 o 1 5 0 29.07 -6.77 8.81 o 2 5 0 30434.05 31038.40 278.06 o 3 5 0 0.11 14.02 12.08 o 4 5 0 31442.51 31831.36 301.30 o 5 5 0 1488.90 1592.38 42.27 o 6 5 0 700.01 699.06 32.87 o 7 5 0 833.31 730.17 43.99 o 8 5 0 6258.62 5986.84 139.73 o 9 5 0 5.06 -4.72 45.01 o 10 5 0 2422.38 2501.49 99.22 o 11 5 0 53.33 206.66 87.88 o 0 6 0 10563.23 10566.71 169.01 o 1 6 0 1594.41 1599.11 28.66 o 2 6 0 16551.96 16908.49 163.51 o 3 6 0 2451.16 2223.51 41.84 o 4 6 0 13233.64 13754.16 152.30 o 5 6 0 628.95 523.73 27.78 o 6 6 0 8099.43 7904.51 116.67 o 7 6 0 796.11 701.54 56.22 o 8 6 0 4752.10 4692.27 122.74 o 9 6 0 1139.77 1080.53 67.40 o 10 6 0 226.39 237.68 46.99 o 11 6 0 227.94 276.47 72.07 o 1 7 0 19230.15 19800.79 186.73 o 2 7 0 3089.88 3277.55 68.91 o 3 7 0 74.49 117.73 15.09 o 4 7 0 15637.40 16185.96 173.23 o 5 7 0 9046.66 8129.71 111.11 o 6 7 0 200.17 189.21 29.55 o 7 7 0 5518.65 5404.76 125.71 o 8 7 0 99.23 91.00 37.06 o 9 7 0 186.98 301.69 46.95 o 10 7 0 615.66 582.66 74.59 o 11 7 0 597.06 582.23 84.16 o 0 8 0 3964.81 4238.76 105.08 o 1 8 0 5599.17 5202.08 67.01 o 2 8 0 579.06 1171.12 175.48 o 3 8 0 42200.58 43574.11 392.86 o 4 8 0 5.07 41.54 23.68 o 5 8 0 4417.64 4329.62 107.40 o 6 8 0 2044.58 1851.40 67.79 o 7 8 0 894.60 1002.79 56.57 o 8 8 0 46.09 11.11 33.65 o 9 8 0 3779.78 3944.69 121.72 o 10 8 0 31.37 -41.07 52.72 o 1 9 0 14173.67 14005.64 145.28 o 2 9 0 6652.60 5948.38 77.07 o 3 9 0 1052.80 954.83 27.21 o 4 9 0 8123.07 7989.88 102.28 o 5 9 0 3535.14 3645.87 76.71 o 6 9 0 260.38 249.65 43.22 o 7 9 0 2130.34 2135.90 79.76 o 8 9 0 1960.52 1905.99 81.27 o 9 9 0 51.14 59.75 47.43 o 10 9 0 1062.15 876.55 85.13 o 0 10 0 42878.57 47212.05 594.45 o 1 10 0 114.75 127.80 14.35 o 2 10 0 15196.45 15521.83 162.72 o 3 10 0 3614.47 3434.11 56.12 o 4 10 0 5685.35 5749.14 98.76 o 5 10 0 173.19 201.18 29.82 o 6 10 0 7336.86 6920.06 142.60 o 7 10 0 56.50 90.12 32.29 o 8 10 0 2112.54 2088.56 85.69 o 9 10 0 322.93 390.97 64.55 o 10 10 0 51.70 139.94 58.87 o 1 11 0 3558.64 3522.64 58.48 o 2 11 0 10820.06 10300.44 120.91 o 3 11 0 1370.44 1382.58 34.55 o 4 11 0 14598.98 14056.71 180.54 o 5 11 0 1028.55 948.40 50.06 o 6 11 0 48.83 85.47 38.19 o 7 11 0 403.64 401.93 43.98 o 8 11 0 1953.79 1927.28 83.94 o 9 11 0 258.05 320.91 62.69 o 10 11 0 2014.20 2105.77 120.72 o 0 12 0 5619.88 5970.96 119.18 o 1 12 0 6325.27 6547.30 89.54 o 2 12 0 1514.46 1926.21 182.08 o 3 12 0 12947.35 12675.34 166.04 o 4 12 0 2315.84 2292.23 74.12 o 5 12 0 3114.78 3136.65 91.45 o 6 12 0 1332.21 1324.64 81.46 o 7 12 0 601.84 529.34 50.35 o 8 12 0 815.60 871.77 76.97 o 9 12 0 2146.27 2324.23 120.14 o 10 12 0 51.93 59.09 57.56 o 1 13 0 17917.03 18037.95 192.20 o 2 13 0 80.87 185.99 34.03 o 3 13 0 10.66 15.81 17.94 o 4 13 0 548.18 515.66 40.49 o 5 13 0 5782.84 5755.34 130.78 o 6 13 0 92.92 133.28 35.79 o 7 13 0 4956.28 4933.08 131.05 o 8 13 0 1.71 -23.59 45.59 o 9 13 0 246.26 226.42 61.62 o 0 14 0 7622.82 7735.26 149.83 o 1 14 0 2731.91 2799.38 58.42 o 2 14 0 3713.29 3977.15 92.89 o 3 14 0 4973.37 4840.03 126.05 o 4 14 0 1341.21 1403.74 66.31 o 5 14 0 2052.54 1984.92 77.90 o 6 14 0 2588.41 2472.28 109.42 o 7 14 0 507.06 615.20 66.04 o 8 14 0 1422.42 1391.92 93.81 o 9 14 0 1575.89 1636.64 108.20 o 1 15 0 104.07 96.99 19.21 o 2 15 0 8221.61 7793.43 124.65 o 3 15 0 7.01 57.54 31.35 o 4 15 0 10017.24 10072.20 184.70 o 5 15 0 228.10 237.41 52.38 o 6 15 0 184.31 211.91 65.78 o 7 15 0 184.44 262.64 53.46 o 8 15 0 1559.84 1391.11 93.78 o 9 15 0 5.39 24.37 57.22 o 0 16 0 7114.45 6859.27 223.04 o 1 16 0 22.58 47.00 21.18 o 2 16 0 2884.04 2850.23 123.24 o 3 16 0 2955.90 3084.73 121.83 o 4 16 0 1620.21 1754.55 107.80 o 5 16 0 11.91 6.90 34.94 o 6 16 0 4225.81 3929.77 216.97 o 7 16 0 3.41 17.32 44.64 o 8 16 0 952.14 791.26 80.50 o 9 16 0 295.30 254.35 63.05 o 1 17 0 5556.05 5490.50 104.45 o 2 17 0 3589.01 3410.58 96.49 o 3 17 0 19.47 3.45 32.41 o 4 17 0 3287.67 3094.35 152.78 o 5 17 0 2456.67 2386.00 91.29 o 6 17 0 184.05 261.31 61.81 o 7 17 0 1795.03 1990.47 109.24 o 8 17 0 286.22 329.65 61.33 o 0 18 0 459.59 545.37 62.86 o 1 18 0 2311.63 2467.84 81.27 o 2 18 0 310.86 859.65 128.54 o 3 18 0 9780.95 9670.37 186.20 o 4 18 0 48.02 44.51 35.47 o 5 18 0 1751.57 1777.43 98.21 o 6 18 0 170.41 270.26 65.25 o 7 18 0 168.03 163.19 66.77 o 8 18 0 53.23 9.12 56.83 o 1 19 0 5233.73 5486.08 149.03 o 2 19 0 539.75 508.65 48.29 o 3 19 0 89.08 85.70 37.80 o 4 19 0 1436.86 1397.50 73.02 o 5 19 0 1518.64 1474.57 132.72 o 6 19 0 44.67 144.72 51.58 o 7 19 0 1381.62 1651.69 144.29 o 0 20 0 8010.13 8705.40 349.22 o 1 20 0 380.44 399.97 54.96 o 2 20 0 2310.33 2256.71 85.97 o 3 20 0 699.24 717.08 56.15 o 4 20 0 301.81 417.79 66.82 o 5 20 0 201.76 214.01 54.97 o 6 20 0 1999.17 1825.71 139.84 o 7 20 0 1.17 101.45 54.64 o 1 21 0 324.65 569.85 82.70 o 2 21 0 2631.42 3001.32 118.28 o 3 21 0 0.08 -20.09 37.08 o 4 21 0 3063.13 3321.13 132.29 o 5 21 0 37.40 42.40 50.40 o 6 21 0 139.59 137.88 58.01 o 0 22 0 1514.41 1645.36 167.15 o 1 22 0 976.76 1086.04 153.30 o 2 22 0 474.76 623.87 67.68 o 3 22 0 1726.62 1854.51 100.11 o 4 22 0 86.66 68.10 53.41 o 5 22 0 770.29 874.86 89.71 o 6 22 0 966.12 1192.46 92.60 o 1 23 0 1931.84 1987.67 132.35 o 2 23 0 94.65 143.34 72.27 o 3 23 0 1.12 48.09 67.43 o 4 23 0 15.00 18.04 51.56 o 5 23 0 1111.89 1049.19 103.72 o 0 24 0 645.84 878.17 146.04 o 1 24 0 713.44 625.40 93.76 o 2 24 0 33.19 221.58 124.35 o 3 24 0 1962.23 1559.56 185.36 o 4 24 0 40.34 46.42 70.51 o 1 25 0 282.74 407.85 86.71 o 2 25 0 1243.92 1025.95 163.28 o 3 25 0 0.40 -109.82 109.82 o -11 0 1 2459.10 2000.00 200.66 o -9 0 1 1782.15 1830.03 90.06 o -7 0 1 87.94 59.25 36.57 o -5 0 1 23311.59 24452.02 341.72 o -3 0 1 8947.93 9023.75 137.12 o -1 0 1 69.75 -0.89 12.12 o 1 0 1 117295.66 128703.48 2207.30 o 3 0 1 15190.81 14813.67 213.79 o 5 0 1 3133.41 3369.92 91.00 o 7 0 1 11460.91 11382.98 221.74 o 9 0 1 4586.10 4777.46 148.54 o 11 0 1 66.77 177.61 83.67 o -11 1 1 10.83 97.97 63.52 o -10 1 1 652.75 619.55 53.65 o -9 1 1 1434.76 1521.23 58.82 o -8 1 1 831.63 701.99 38.82 o -7 1 1 10096.00 9972.69 134.57 o -6 1 1 6140.57 5994.58 91.14 o -5 1 1 17.09 21.19 12.15 o -4 1 1 8280.01 8681.21 113.25 o -3 1 1 6853.52 6740.34 77.65 o -2 1 1 11243.42 11695.43 111.62 o -1 1 1 58796.17 64085.41 662.19 o 1 1 1 20817.23 22951.54 200.76 o 2 1 1 23379.78 24718.29 223.11 o 3 1 1 2555.19 2366.29 41.62 o 4 1 1 10811.56 11728.19 132.49 o 5 1 1 18829.88 19331.55 205.53 o 6 1 1 935.71 929.98 38.18 o 7 1 1 2268.17 2188.98 61.29 o 8 1 1 3769.93 3602.87 85.71 o 9 1 1 12.20 -0.49 30.52 o 10 1 1 377.86 445.67 80.07 o 11 1 1 1164.25 1218.40 98.65 o -11 2 1 297.86 336.85 80.47 o -10 2 1 522.43 553.25 55.47 o -9 2 1 256.02 256.99 35.24 o -8 2 1 8147.70 8173.65 128.23 o -7 2 1 94.98 107.65 22.16 o -6 2 1 10424.18 10353.27 132.22 o -5 2 1 3986.32 3919.91 64.35 o -4 2 1 10908.02 11875.87 128.67 o -3 2 1 680.20 600.28 19.18 o -2 2 1 39020.54 40995.88 353.43 o -1 2 1 3896.58 3873.61 55.68 o 0 2 1 107234.86 125555.64 2064.70 o 1 2 1 17501.85 18863.61 184.60 o 2 2 1 4076.72 4365.99 54.80 o 3 2 1 131.91 118.16 13.04 o 4 2 1 15328.76 15370.13 163.63 o 5 2 1 1.97 0.58 15.53 o 6 2 1 21657.86 21587.69 233.37 o 7 2 1 3934.28 3705.82 78.84 o 8 2 1 821.83 774.88 44.58 o 9 2 1 574.51 612.58 49.08 o 10 2 1 1086.11 1124.48 70.30 o 11 2 1 38.94 116.26 52.27 o -11 3 1 8.87 266.00 78.04 o -10 3 1 1979.30 1927.23 104.63 o -9 3 1 107.35 87.64 36.16 o -8 3 1 202.77 231.49 31.24 o -7 3 1 1610.27 1541.51 50.27 o -6 3 1 6812.82 6427.25 98.92 o -5 3 1 1.91 -0.40 17.05 o -4 3 1 32258.80 32210.52 299.98 o -3 3 1 8.42 17.87 10.47 o -2 3 1 14394.32 14592.85 139.30 o -1 3 1 20153.82 20313.87 199.31 o 0 3 1 24421.06 28818.43 314.92 o 1 3 1 1530.04 1640.96 30.11 o 2 3 1 37312.04 38636.32 338.01 o 3 3 1 2651.19 2664.35 44.63 o 4 3 1 7171.14 7027.02 91.94 o 5 3 1 2233.18 2107.13 48.49 o 6 3 1 2634.59 2615.42 69.32 o 7 3 1 368.52 387.02 32.66 o 8 3 1 11616.34 11444.81 183.90 o 9 3 1 18.25 35.91 30.87 o 10 3 1 1754.99 1870.03 99.58 o 11 3 1 56.86 88.88 51.51 o -11 4 1 846.13 1046.07 92.53 o -10 4 1 189.50 183.23 43.58 o -9 4 1 1360.55 1441.89 72.44 o -8 4 1 4048.87 4144.84 110.75 o -7 4 1 102.12 99.99 23.92 o -6 4 1 4163.79 3859.34 72.94 o -5 4 1 9162.83 8705.27 124.88 o -4 4 1 1705.50 1670.25 39.82 o -3 4 1 15231.10 15010.11 151.82 o -2 4 1 30872.33 31300.75 277.39 o -1 4 1 293.87 373.77 17.06 o 0 4 1 1615.96 1522.95 36.73 o 1 4 1 205.94 241.76 14.53 o 3 4 1 9979.01 9600.53 106.78 o 4 4 1 15867.71 16560.37 173.69 o 5 4 1 6.46 16.12 14.00 o 6 4 1 5777.92 5615.06 91.56 o 7 4 1 2102.67 1960.04 64.21 o 8 4 1 239.30 279.95 37.64 o 9 4 1 1801.36 1827.92 81.27 o 10 4 1 572.22 508.28 105.62 o 11 4 1 41.56 221.07 50.54 o -11 5 1 76.45 97.83 100.53 o -10 5 1 73.16 45.38 51.09 o -9 5 1 3336.50 3482.81 108.65 o -8 5 1 845.54 836.91 55.39 o -7 5 1 11297.86 11101.95 153.02 o -6 5 1 6.58 30.07 19.80 o -5 5 1 2293.08 2110.98 49.83 o -4 5 1 5527.01 5918.73 82.35 o -3 5 1 10725.12 10248.22 118.32 o -1 5 1 37132.88 40014.02 345.76 o 0 5 1 6866.65 8055.81 119.94 o 1 5 1 26388.66 27537.97 270.48 o 2 5 1 1079.53 807.97 38.71 o 3 5 1 23509.67 24391.45 233.06 o 4 5 1 165.71 171.56 20.68 o 5 5 1 23716.64 23580.52 240.51 o 6 5 1 4.74 -22.37 22.37 o 7 5 1 2257.09 2281.63 64.70 o 8 5 1 474.59 470.74 44.63 o 9 5 1 373.69 409.71 49.10 o 10 5 1 57.16 11.88 62.29 o 11 5 1 1464.17 1636.68 92.36 o -11 6 1 1341.90 1490.91 109.31 o -10 6 1 63.51 140.74 52.58 o -9 6 1 2006.63 2164.30 94.44 o -8 6 1 4118.35 3839.63 128.12 o -7 6 1 1462.39 1455.22 75.64 o -6 6 1 3457.69 3434.18 80.53 o -5 6 1 10052.20 9529.82 122.65 o -4 6 1 1523.94 1672.05 40.24 o -3 6 1 47445.86 48825.54 464.57 o -2 6 1 9989.98 10382.42 153.06 o -1 6 1 1350.64 1220.77 24.89 o 0 6 1 19446.91 20837.83 245.07 o 1 6 1 16946.17 17466.83 166.16 o 3 6 1 22622.08 23410.38 234.61 o 4 6 1 5001.79 5267.47 192.00 o 5 6 1 300.50 328.20 27.55 o 6 6 1 5968.87 5977.64 111.25 o 7 6 1 4855.19 4662.63 103.49 o 8 6 1 96.38 89.86 36.88 o 9 6 1 2857.88 2908.41 103.44 o 10 6 1 174.84 257.86 50.40 o 11 6 1 23.09 135.87 71.44 o -11 7 1 119.79 279.36 65.81 o -10 7 1 2274.98 2329.10 118.18 o -9 7 1 259.81 239.51 55.87 o -8 7 1 378.05 432.55 47.66 o -7 7 1 2019.91 1974.76 73.71 o -6 7 1 4646.94 4523.41 92.54 o -5 7 1 153.93 142.43 19.36 o -4 7 1 19381.22 19434.49 198.53 o -3 7 1 4965.79 5307.97 70.65 o -2 7 1 7170.10 7563.50 86.31 o -1 7 1 5991.64 5858.43 70.11 o 0 7 1 10787.70 11158.62 114.70 o 1 7 1 4815.27 4843.98 62.02 o 2 7 1 25222.70 24274.98 253.76 o 3 7 1 5996.46 6274.20 94.80 o 4 7 1 6250.23 6051.32 85.77 o 5 7 1 4427.12 4395.33 86.83 o 6 7 1 1881.26 1896.55 93.78 o 7 7 1 32.66 58.76 35.18 o 8 7 1 6771.86 6578.32 151.86 o 9 7 1 166.06 231.57 45.05 o 10 7 1 935.02 1061.13 71.81 o -11 8 1 45.17 11.61 67.70 o -10 8 1 313.44 365.30 63.46 o -9 8 1 63.20 64.46 47.92 o -8 8 1 8339.04 8054.65 224.74 o -7 8 1 29.28 65.99 33.07 o -6 8 1 5016.85 4952.27 111.89 o -5 8 1 430.99 354.85 34.26 o -4 8 1 1725.32 1761.99 40.70 o -3 8 1 255.13 213.76 15.93 o -2 8 1 36677.53 36528.34 328.96 o -1 8 1 674.84 723.43 22.18 o 0 8 1 18073.92 18855.17 181.48 o 1 8 1 1184.09 1095.31 26.68 o 2 8 1 3496.51 3430.45 79.90 o 3 8 1 4396.65 4629.77 79.43 o 4 8 1 24047.25 24538.68 514.51 o 5 8 1 91.50 119.77 36.32 o 6 8 1 7898.46 7437.16 149.00 o 7 8 1 664.45 653.42 50.05 o 8 8 1 375.39 459.39 48.48 o 9 8 1 113.03 75.13 39.02 o 10 8 1 1241.28 1216.46 79.26 o -10 9 1 1310.13 1402.60 97.45 o -9 9 1 1384.96 1531.27 95.55 o -8 9 1 47.34 100.45 47.54 o -7 9 1 3359.70 3122.09 93.90 o -6 9 1 1254.34 1259.09 56.60 o -5 9 1 1680.74 1684.13 59.83 o -4 9 1 13134.85 12867.99 144.05 o -3 9 1 5566.83 5612.75 75.78 o -2 9 1 511.48 623.50 81.24 o -1 9 1 20305.51 20599.90 199.59 o 0 9 1 1532.07 1511.13 33.22 o 1 9 1 9274.79 9260.79 105.75 o 2 9 1 21696.26 21607.62 236.76 o 3 9 1 410.80 316.71 23.32 o 4 9 1 7691.78 7498.43 116.23 o 5 9 1 6551.55 6201.84 108.84 o 6 9 1 216.69 181.93 30.48 o 7 9 1 1450.83 1441.28 68.19 o 8 9 1 1959.56 1938.61 108.19 o 9 9 1 70.54 37.48 38.82 o 10 9 1 514.47 479.25 71.47 o -10 10 1 8.41 13.09 52.39 o -9 10 1 1249.64 1351.64 94.57 o -8 10 1 312.17 374.49 56.93 o -7 10 1 7.79 14.87 29.91 o -6 10 1 207.58 221.89 34.02 o -5 10 1 11274.21 11395.50 185.24 o -4 10 1 13.69 0.87 31.10 o -3 10 1 15372.81 15583.82 165.20 o -2 10 1 218.24 568.27 46.68 o -1 10 1 1287.64 1373.60 33.37 o 0 10 1 1302.92 1551.40 55.84 o 1 10 1 15385.03 15033.53 157.71 o 2 10 1 21.07 2759.63 139.07 o 3 10 1 15314.55 14799.91 183.08 o 4 10 1 2193.82 2236.55 58.59 o 5 10 1 180.82 211.59 26.57 o 6 10 1 3.99 6.38 30.58 o 7 10 1 2225.00 2157.00 82.20 o 8 10 1 134.35 128.72 40.84 o 9 10 1 3168.73 3192.24 115.04 o 10 10 1 116.28 72.67 63.69 o -10 11 1 110.62 72.78 57.36 o -9 11 1 2007.81 2123.34 113.95 o -8 11 1 113.00 135.93 51.60 o -7 11 1 6049.82 6038.27 159.55 o -6 11 1 904.36 898.80 51.57 o -5 11 1 2946.51 3026.29 85.67 o -4 11 1 3161.53 3155.46 82.86 o -3 11 1 4765.34 4585.89 69.37 o -2 11 1 242.05 337.02 31.75 o -1 11 1 23444.97 23533.78 230.91 o 0 11 1 3996.61 4159.39 64.60 o 1 11 1 9994.40 9888.80 117.16 o 2 11 1 5482.61 4972.04 84.11 o 3 11 1 4963.89 5184.30 91.36 o 4 11 1 1075.87 1105.26 42.87 o 5 11 1 7188.73 6839.16 139.92 o 6 11 1 335.24 407.66 41.81 o 7 11 1 2231.26 2135.85 84.51 o 8 11 1 393.13 325.18 45.80 o 9 11 1 327.28 359.62 64.71 o 10 11 1 172.40 178.55 62.56 o -10 12 1 216.71 129.64 60.27 o -9 12 1 948.01 970.95 85.52 o -8 12 1 3029.79 2813.74 122.77 o -7 12 1 1.46 116.75 45.48 o -6 12 1 3501.75 3416.54 98.23 o -5 12 1 2383.47 2183.96 74.59 o -4 12 1 329.61 322.16 32.49 o -3 12 1 8415.68 8147.04 120.93 o -2 12 1 15321.31 14423.54 159.05 o -1 12 1 20.22 35.49 17.87 o 0 12 1 18375.19 19111.84 197.28 o 1 12 1 5197.06 4982.92 75.37 o 2 12 1 824.89 1050.95 107.58 o 3 12 1 2286.05 2227.48 58.43 o 4 12 1 7007.33 6998.00 116.93 o 5 12 1 5.62 31.34 45.09 o 6 12 1 5070.95 4932.95 124.83 o 7 12 1 1732.28 1747.19 78.65 o 8 12 1 322.83 410.11 49.85 o 9 12 1 710.49 774.53 78.69 o 10 12 1 603.10 555.01 76.78 o -10 13 1 1528.50 1605.99 154.57 o -9 13 1 7.77 22.11 51.44 o -8 13 1 116.55 168.62 62.16 o -7 13 1 1.56 -38.78 38.78 o -6 13 1 2940.35 3043.72 94.61 o -5 13 1 0.07 0.66 37.52 o -4 13 1 15995.49 16039.71 240.38 o -3 13 1 33.35 34.44 28.07 o -2 13 1 2008.65 1996.86 46.05 o -1 13 1 343.78 339.85 22.60 o 0 13 1 5601.95 5829.05 104.45 o 1 13 1 0.34 -14.45 14.45 o 2 13 1 21665.47 21231.94 247.74 o 3 13 1 9.38 13.07 18.65 o 4 13 1 3588.14 3350.18 93.90 o 5 13 1 708.01 731.92 50.50 o 6 13 1 1241.29 1189.16 64.90 o 7 13 1 29.75 -14.56 31.77 o 8 13 1 4127.77 3887.14 191.83 o 9 13 1 9.69 24.87 54.92 o -9 14 1 287.92 405.96 68.88 o -8 14 1 1940.93 1765.37 104.23 o -7 14 1 190.01 236.84 53.97 o -6 14 1 2415.26 2493.39 108.01 o -5 14 1 4931.36 4900.23 120.94 o -4 14 1 343.97 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