Acta Crystallographica Section C

Crystal Structure Communications

Volume 63, Part 10 (October 2007)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: Part of the crystal structure of 2,3,10,11-tetrathiatricyclo[10.4.0.04,9]hexadeca-4,6,8,12,14,16-hexaene, showing the formation of a [pi]-stacked sheet. For the sake of clarity, H atoms have been omitted. See Yearley, Lippert, Mitchell & Pinkerton [Acta Cryst. (2007), C63, o576-o577].

inorganic compounds


 

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Acta Cryst. (2007). C63, i83-i85  [ doi:10.1107/S010827010704108X ]

Double complexes [Co(NH3)5(H2O)]2[Zr3F18]·6H2O and [Co(NH3)6]2[Zr3F18]·6H2O

A. I. Gubanov and N. V. Kuratieva

Synopsis: The structures of the title compounds are built from octahedral [Co(NH3)x(H2O)y]3+ cations and [Zr3F18]6- anionic chains. O-H...F hydrogen bonds help to establish the crystal packing.

Formula: [Co(NH3)5(H2O)]2[Zr3F18]·6H2O and [Co(NH3)6]2[Zr3F18]·6H2O

Online 22 September 2007


 

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Acta Cryst. (2007). C63, i86-i88  [ doi:10.1107/S0108270107038772 ]

A new pillared lithium bismuth phosphate, LiBi7.37P3O19, with elliptical channels

N. Arumugam, V. Lynch and H. Steinfink

Synopsis: The structure of a new lithium bismuth phosphate, LiBi7.37P3O19, consists of infinite OBi4 edge-sharing tetrahedral chains in the ac plane, which form Bi2O2 layers parallel to the b axis. They are sandwiched between PO4 tetrahedral and Bi polyhedral layers. The PO4-Bi-PO4 layers are bridged by columns formed by one Bi polyhedron flanked on each side by LiO4 tetrahedra.

Formula: LiBi7.37P3O19

Online 22 September 2007


 

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Acta Cryst. (2007). C63, i89-i90  [ doi:10.1107/S0108270107041169 ]

Isokite, CaMg(PO4)F0.8(OH)0.2, isomorphous with titanite

H. Yang, J. Zwick, R. T. Downs and G. Costin

Synopsis: Isokite, ideally CaMg(PO4)F, is isomorphous with C2/c titanite and consists of PO4, MgO4F2, and CaO6F polyhedra.

Formula: CaMg(PO4)F0.8(OH)0.2

Online 22 September 2007


 

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Acta Cryst. (2007). C63, i91-i92  [ doi:10.1107/S0108270107038036 ]

Kolbeckite, ScPO4·2H2O, isomorphous with metavariscite

H. Yang, C. Li, R. A. Jenkins, R. T. Downs and G. Costin

Synopsis: This study presents the first structural report of kolbeckite, with the ideal formula ScPO4·2H2O (scandium phosphate dihydrate), based on single-crystal X-ray diffraction data. Kolbeckite belongs to the metavariscite mineral group, in which each PO4 tetrahedron shares four vertices with four ScO4(H2O)2 octahedra and vice versa, forming a three-dimensional network of polyhedra.

Formula: ScPO4·2H2O

Online 22 September 2007


 

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Acta Cryst. (2007). C63, i93-i95  [ doi:10.1107/S0108270107042825 ]

Yttrium pyrogermanate, Y2Ge2O7

G. J. Redhammer, G. Roth and G. Amthauer

Synopsis: The structure and absolute configuration of tetragonal Y2Ge2O7 was determined from X-ray diffraction data. A comparison is made with related lanthanide pyrogermanates of the series R2Ge2O7 (R = Eu and Tb-Lu).

Formula: Ge2O7Y2

Online 29 September 2007


 

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Acta Cryst. (2007). C63, i96-i98  [ doi:10.1107/S0108270107041972 ]

SrZn11: a new binary compound with the BaCd11 structure

S. Kal, E. Stoyanov, T. L. Groy and U. Häussermann

Synopsis: A new Sr-Zn compound with the BaCd11 structure type has been synthesized at high pressure. It contains chains of all-face-capped Zn tetrahedra which are interconnected by shared capping atoms.

Formula: SrZn11

Online 29 September 2007


metal-organic compounds


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Acta Cryst. (2007). C63, m433-m435  [ doi:10.1107/S0108270107038711 ]

catena-Poly[[bis(nitrato-[kappa]2O,O')copper(II)]-[mu]-propane-1,3-diylbis(diphenylphosphine oxide)-[kappa]2O:O']

A. W. G. Platt and A. M. J. Lees

Formula: [Cu(NO3)2(C27H26O2P2)]

Online 1 September 2007


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Acta Cryst. (2007). C63, m436-m439  [ doi:10.1107/S0108270107039686 ]

2,6-Bis(azaindole)pyridine: reactivity with iron(III) and copper(II) salts

S. N. Collins, S. Taylor, J. A. Krause and W. B. Connick

Formula: C19H13N5, (C19H14N5)[FeCl4] and [Cu(NO3)2(C19H13N5)]

Online 1 September 2007


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Acta Cryst. (2007). C63, m440-m444  [ doi:10.1107/S0108270107040449 ]

Hydrated hexacyanometallate(III) salts of triaqua(18-crown-6)lanthanoid(III) and tetraaqua(18-crown-6)lanthanoid(III) cations containing nine- and ten-coordinate lanthanoids

P. Misra, R. Koner, M. Nayak, S. Mohanta, J. N. Low, G. Ferguson and C. Glidewell

Formula: [Ce(C12H24O6)(H2O)4][Fe(CN)6]·2H2O, [Nd(C12H24O6)(H2O)4][Fe(CN)6]·2H2O, [Sm(C12H24O6)(H2O)3][Fe(CN)6]·2H2O, [Eu(C12H24O6)(H2O)3][Fe(CN)6]·2H2O, [Gd(C12H24O6)(H2O)3][Cr(CN)6]·2H2O and [Gd(C12H24O6)(H2O)3][Co(CN)6]·2H2O

Online 1 September 2007


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Acta Cryst. (2007). C63, m445-m447  [ doi:10.1107/S0108270107040498 ]

Bis([mu]-4-carboxy-2-sulfonatobenzoato)bis[aqua(2,2'-bipyridyl)manganese(II)]

Z.-X. Lian, J.-M. Zhang, M.-L. Xu, G.-R. Xu and T.-J. Lou

Formula: [Mn2(C8H4O7S)2(C10H8N2)2(H2O)2]

Online 22 September 2007


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Acta Cryst. (2007). C63, m448-m450  [ doi:10.1107/S0108270107040437 ]

Hydrogen bonding in diaquatetrakis(urea-[kappa]O)MII dinitrates, with M = Ni and Co

A. Krawczuk and K. Stadnicka

Formula: [Ni(CH4N2O)4(H2O)2](NO3)2 and [Co(CH4N2O)4(H2O)2](NO3)2

Online 22 September 2007


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Acta Cryst. (2007). C63, m451-m453  [ doi:10.1107/S0108270107039856 ]

A novel framework of N-H...Br hydrogen bonds forming Br(4,4'-bipyridinium)4 supramolecular synthons: bis(4,4'-bipyridinium) tris[tetrabromidoferrate(III)] bromide

B. F. Ali and R. Al-Far

Formula: (C10H10N2)2[FeBr4]3Br

Online 22 September 2007


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Acta Cryst. (2007). C63, m454-m455  [ doi:10.1107/S0108270107043454 ]

catena-Poly[[dinitratocadmium(II)]bis[[mu]-bis(2-methyl-1H-imidazol-1-yl)methane-[kappa]2N3:N3']]

C.-M. Jin, C.-Y. Chen, W.-D. Wang and L.-Y. Wu

Formula: [Cd(NO3)2(C9H12N4)2]

Online 22 September 2007


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Acta Cryst. (2007). C63, m456-m458  [ doi:10.1107/S0108270107044009 ]

[2,6-Bis(5-methyl-2-pyridyl)phenyl-[kappa]3N,C1,N']chloridoplatinum(II)

T. Abe, K. Shinozaki, N. Ikeda and T. Suzuki

Formula: [PtCl(C18H15N2)]

Online 29 September 2007


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Acta Cryst. (2007). C63, m459-m461  [ doi:10.1107/S0108270107044010 ]

Tetraaquabis(2-methoxybenzaldehyde isonicotinoylhydrazone)cadmium(II) dinitrate

Z. Fu, S. Gao and S. Liu

Formula: [Cd(C14H13N3O2)2(H2O)4](NO3)2

Online 29 September 2007


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Acta Cryst. (2007). C63, m462-m464  [ doi:10.1107/S0108270107042643 ]

Aqua-2[kappa]O-[mu]-{N,N'-bis[2-(dimethylamino)ethyl]oxamidato(2-)}-1[kappa]2O,O':2[kappa]4N,N',N'',N'''-bis(4,4'-dimethyl-2,2'-bipyridine-1[kappa]2N,N')copper(II)nickel(II) bis(perchlorate) methanol hemisolvate

W. Sun, Y.-T. Li, Z.-Y. Wu and J.-L. Liu

Formula: [CuNi(C10H20N4O2)(C12H8N2)2(H2O)](ClO4)2·0.5CH4O

Online 29 September 2007


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Acta Cryst. (2007). C63, m465-m468  [ doi:10.1107/S0108270107040504 ]

cis-Bis(dimethyl sulfide)dinitratoplatinum(II) at 295 and 150 K

C. Hansson and Å. Oskarsson

Formula: [Pt(NO3)2(C2H6S)2]

Online 29 September 2007


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Acta Cryst. (2007). C63, m469-m472  [ doi:10.1107/S0108270107044976 ]

Aqua(dipicolinato-[kappa]3O,N,O')(1H-imidazole-[kappa]N3)(1,10-phenanthroline-N,N')manganese(II)

C.-B. Ma, C.-N. Chen and Q.-T. Liu

Formula: [Mn(C7H3NO4)(C3H4N2)(C12H8N2)(H2O)]

Online 29 September 2007


organic compounds


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Acta Cryst. (2007). C63, o565-o567  [ doi:10.1107/S0108270107038632 ]

Two substituted 2-pyrrolin-5-ones: chains built from a single N-H...O hydrogen bond

Z.-F. Zhang, J.-G. Wang, S.-Q. Wang and G.-R. Qu

Formula: C7H9NO3 and C7H9NO2

Online 1 September 2007


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Acta Cryst. (2007). C63, o568-o571  [ doi:10.1107/S0108270107039194 ]

[pi]-Stacked dimers in 6-methoxy-3,3-dimethyl-3H-benzo[f]chromene, and centrosymmetric dimers containing C-H...[pi](arene) hydrogen bonds in racemic 3-bromo-2,2,6,6-tetramethyl-3,4-dihydro-2H,6H-1,5-dioxatriphenylene

F. de C. da Silva, J. L. Wardell, S. M. S. V. Wardell, V. F. Ferreira, J. N. Low and C. Glidewell

Formula: C16H16O2 and C20H21BrO2

Online 1 September 2007


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Acta Cryst. (2007). C63, o572-o575  [ doi:10.1107/S0108270107038413 ]

N-Acetyl-L-tyrosine methyl ester monohydrate at 293 and 123 K

A. Janik, A. Chyra and K. Stadnicka

Formula: C12H15NO4·H2O

Online 1 September 2007


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Acta Cryst. (2007). C63, o576-o577  [ doi:10.1107/S0108270107040358 ]

2,3,10,11-Tetrathiatricyclo[10.4.0.04,9]hexadeca-4,6,8,12,14,16-hexaene (precession camera versus CCD)

E. J. Yearley, E. L. Lippert, D. J. Mitchell and A. A. Pinkerton

Formula: C12H8S4

Online 1 September 2007


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Acta Cryst. (2007). C63, o578-o581  [ doi:10.1107/S0108270107038553 ]

3-Deoxy-[beta]-D-ribo-hexopyranose (3-deoxy-[beta]-D-glucopyranose)

W. Zhang, B. C. Noll and A. S. Serianni

Formula: C6H12O5

Online 1 September 2007


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Acta Cryst. (2007). C63, o582-o584  [ doi:10.1107/S0108270107041236 ]

8-tert-Butyl-7-(4-chlorophenyl)-10-phenyl-5,6-dihydro-10H-benzo[h]pyrazolo[3,4-b]quinoline

J. Portilla, J. Quiroga, J. Cobo, J. N. Low and C. Glidewell

Formula: C30H26ClN3

Online 1 September 2007


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Acta Cryst. (2007). C63, o585-o587  [ doi:10.1107/S0108270107040450 ]

Hydrogen-bonded sheets in benzylmethylammonium hydrogen maleate

L. Santacruz, R. Abonia, J. Cobo, J. N. Low and C. Glidewell

Formula: C8H12N+·C4H3O4-

Online 1 September 2007


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Acta Cryst. (2007). C63, o588-o590  [ doi:10.1107/S0108270107041352 ]

A new polymorph of tetraphenyldiboroxane

L. Kaufmann, H.-W. Lerner and M. Bolte

Formula: C24H20B2O

Online 22 September 2007


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Acta Cryst. (2007). C63, o591-o593  [ doi:10.1107/S0108270107040048 ]

Hexagonal packing of cis,cis-cyclohexane-1,3,5-tricarboxamide

B. K. Saha

Formula: C9H15N3O3

Online 22 September 2007


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Acta Cryst. (2007). C63, o594-o596  [ doi:10.1107/S010827010703805X ]

A new conformer of 1,4,7-tris(p-tolylsulfonyl)-1,4,7-triazacyclononane

V. André, S. Barroso, A. M. Martins and M. T. Duarte

Formula: C27H33N3O6S3

Online 22 September 2007


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Acta Cryst. (2007). C63, o597-o599  [ doi:10.1107/S010827010704156X ]

Acyclic Schiff base salts derived from 1,3-diaminopropane and 1,3-diamino-2-hydroxypropane

C. Rodríguez de Barbarín, S. Bernès, B. Nájera and P. Elizondo

Formula: C17H22N4O42+·2Cl-·H2O and C17H22N4O52+·2Cl-

Online 22 September 2007


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Acta Cryst. (2007). C63, o600-o602  [ doi:10.1107/S0108270107027138 ]

The 7-bromo derivative of 2-amino-2'-deoxytubercidin fluorinated at the sugar moiety

F. Seela, P. Ding, X. Peng, H. Eickmeier and H. Reuter

Formula: C11H13BrFN5O3

Online 22 September 2007


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Acta Cryst. (2007). C63, o603-o605  [ doi:10.1107/S010827010703569X ]

2,3,5,6-Tetrakis[3,5-bis(trifluoromethyl)phenoxy]-2,5-bis(dimethylamino)2,3,5,6-tetrabora-1,4-dioxane diethyl ether 0.667-solvate

W. Clegg, T. B. Marder, S. Nlate and A. J. Scott

Formula: C36H26B4F24N2O6·0.667C4H10O

Online 22 September 2007


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Acta Cryst. (2007). C63, o606-o608  [ doi:10.1107/S010827010704142X ]

5-(5-Nitropyridin-2-yldithio)-1-phenyl-1H-tetrazole

I. Brito, A. Mundaca, A. Cárdenas and M. López-Rodríguez

Formula: C12H8N6O2S2

Online 22 September 2007


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Acta Cryst. (2007). C63, o609-o612  [ doi:10.1107/S0108270107044241 ]

Ammonium violurate: a compact structure with extensive hydrogen bonding in three dimensions

G. S. Nichol and W. Clegg

Formula: NH4+·C4H2N3O4-

Online 29 September 2007


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