Acta Crystallographica Section C

Crystal Structure Communications

Volume 63, Part 11 (November 2007)


organic compounds



gd3147 scheme

Acta Cryst. (2007). C63, o617-o619    [ doi:10.1107/S010827010704468X ]

Tetrakis(1-naphthylamino)silane and its tetrahydrofuran trisolvate

M. S. Balakrishna, T. Chivers and M. Parvez

Abstract: In both title structures, C40H32N4Si and C40H32N4Si·3C4H8O, the angles around the Si atom deviate significantly from the tetrahedral value [104.34 (7)-116.63 (7)° in the nonsolvate and 99.91 (15)-116.85 (15)° in the solvate]. The amino H atoms in the solvated structure are involved in hydrogen bonding with two of the tetrahydrofuran solvent molecules.

Formula: C40H32N4Si and C40H32N4Si·3C4H8O


hkldisplay filedownload file

Structure factor file (CIF format) (337.3 kbytes)
[ doi:10.1107/S010827010704468X/gd3147Isup2.hkl ]
Contains datablock I


hkldisplay filedownload file

Structure factor file (CIF format) (478.0 kbytes)
[ doi:10.1107/S010827010704468X/gd3147IIsup3.hkl ]
Contains datablock II


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