Acta Crystallographica Section C

Crystal Structure Communications

Volume 63, Part 12 (December 2007)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The one-dimensional hydrogen-bonding motifs in 5-butyl-5-ethylbarbituric acid, viz. tape and ladder. See Gelbrich, Zencirci & Griesser [Acta Cryst. (2007), C63, o751-o753].

inorganic compounds


 

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Acta Cryst. (2007). C63, i109-i111  [ doi:10.1107/S0108270107049025 ]

Bi5O7Br and its structural relation to [alpha]-Bi5O7I

E. Keller and V. Krämer

Synopsis: The crystal structure and synthesis of Bi5O7Br are described. The structure is compared with that of closely related (but non-isotypic) [alpha]-Bi5O7I.

Formula: Bi5O7Br

Online 24 November 2007


 

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Acta Cryst. (2007). C63, i112-i114  [ doi:10.1107/S0108270107054078 ]

Rb3Y2(BO3)3 with a noncentrosymmetric structure

J. H. Gao and R. K. Li

Synopsis: The title compound contains zigzag-like chains of corner-sharing [Y2O10] dimers and BO3 triangles, which complete a three-dimensional framework. The Rb+ ions are located in the channels.

Formula: Rb3Y2(BO3)3

Online 24 November 2007


 

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Acta Cryst. (2007). C63, i115-i118  [ doi:10.1107/S0108270107050640 ]

Monoclinic PZN-8%PT [Pb(Zn0.3066Nb0.6133Ti0.08)O3] at 4 K

J. S. Forrester and E. H. Kisi

Synopsis: Rietveld refinements from very high resolution neutron powder diffraction data on the relaxor ferroelectric [Pb(Zn0.3066Nb0.6133Ti0.08)O3] (PZN-8%PT) show that it is monoclinic in the space group Cm at 4 K. Atomic coordinates show strong electric polarization at this temperature.

Formula: Pb(Zn0.3066Nb0.6133Ti0.08)O3

Online 30 November 2007


 

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Acta Cryst. (2007). C63, i119-i121  [ doi:10.1107/S0108270107053462 ]

FeII2(PO4)(OH), a synthetic analogue of wolfeite

F. Hatert

Synopsis: The title compound, diiron(II) phosphate hydroxide, Fe2(PO4)(OH), has been synthesized hydrothermally and is the synthetic analogue of the mineral wolfeite. The crystal structure contains edge- and corner-sharing FeO4(OH) and FeO4(OH)2 polyhedra, linked via corner-sharing to the PO4 tetrahedra.

Formula: Fe2(PO4)(OH)

Online 30 November 2007


 

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Acta Cryst. (2007). C63, i122-i124  [ doi:10.1107/S0108270107053449 ]

Iranite, CuPb10(CrO4)6(SiO4)2(OH)2, isomorphous with hemihedrite

H. Yang, J. L. Sano, C. Eichler, R. T. Downs and G. Costin

Synopsis: Iranite is isomorphous with hemihedrite, ZnPb10(CrO4)6(SiO4)2F2. The SiO4 and CrO4 tetrahedra and CuO4(OH)2 octahedra form layers parallel to (120) that are held together by Pb2+ cations.

Formula: CuPb10(CrO4)6(SiO4)2(OH)2

Online 30 November 2007


metal-organic compounds


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Acta Cryst. (2007). C63, m541-m547  [ doi:10.1107/S0108270107045453 ]

Luminescent properties of three structures built from 3-cyano-4-dicyanomethylene-5-oxo-4,5-dihydro-1H-pyrrol-2-olate and cadmium

V. A. Tafeenko, G. N. Panin, A. N. Baranov, I. N. Bardasov and L. A. Aslanov

Formula: [Cd(C8HN4O2)2(H2O)4]·2H2O, [Cd(C8HN4O2)2(H2O)4]·C4H8O2 and[Cd3(C8HN4O2)2(C8N4O2)2(H2O)10]·0.5H2O

Online 14 November 2007


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Acta Cryst. (2007). C63, m548-m549  [ doi:10.1107/S0108270107049943 ]

1,1,1,1,4,4,4,4-Octacarbonyl-2,2,3,3,5,5,6,6-octamethyl-cyclo-2,3,5,6-tetraantimony-1,4-dichromium

H. J. Breunig, E. Lork, O. Moldovan and C. I. Rat

Formula: [Cr2Sb4(CH3)8(CO)8]

Online 14 November 2007


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Acta Cryst. (2007). C63, m550-m552  [ doi:10.1107/S0108270107048706 ]

In search of conformationally chiral square-planar complexes: dichloridobis(2-methoxypyridine-[kappa]N)copper(II)

A. Lennartson, T. Wiklund and M. Håkansson

Formula: [CuCl2(C6H7NO)2]

Online 14 November 2007


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Acta Cryst. (2007). C63, m553-m556  [ doi:10.1107/S0108270107048937 ]

Two new oximate-bridged square-planar dinuclear nickel(II) complexes

M. Bera and B. C. Noll

Formula: [Ni2(C8H16N3O)2](ClO4)2·C2H3N and [Ni2(C13H18N3O)2](ClO4)2

Online 14 November 2007


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Acta Cryst. (2007). C63, m557-m559  [ doi:10.1107/S0108270107051566 ]

(Nitrato-[kappa]O)bis(pyridine-2-carboxamide-[kappa]2N1,O)mercury(II) nitrate

M. Đakovic and Z. Popovic

Formula: [Hg(NO3)(C6H6N2O)2]NO3

Online 14 November 2007


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Acta Cryst. (2007). C63, m560-m562  [ doi:10.1107/S0108270107051293 ]

Poly[[mu]2-(N-hydroxypyridine-2-carboxamidine)-[mu]2-nitrato-silver(I)]

A.-L. Cui, P. Han, H.-J. Yang, R.-J. Wang and H.-Z. Kou

Formula: [Ag(NO3)(C6H7N3O)]

Online 14 November 2007


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Acta Cryst. (2007). C63, m563-m565  [ doi:10.1107/S0108270107051104 ]

Lithium aspirinate hemihydrate

J.-B. Arlin, F. Addison and A. R. Kennedy

Formula: [Li(C9H7O4)]·0.5H2O

Online 14 November 2007


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Acta Cryst. (2007). C63, m566-m569  [ doi:10.1107/S0108270107052419 ]

Setting ambiguity in C2/c with dibromidotetrakis(1H-pyrazole-[kappa]N2)manganese(II) as an example

K. Ruth, K. Kunz, H.-W. Lerner and M. Bolte

Formula: [MnBr2(C3H4N2)4]

Online 14 November 2007


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Acta Cryst. (2007). C63, m570-m572  [ doi:10.1107/S0108270107052638 ]

An unusual chain cadmium(II) coordination polymer: catena-poly[[(2,2'-bipyridyl-[kappa]2N,N')cadmium(II)]-di-[mu]-chlorido-[(2,2'-bipyridyl-[kappa]2N,N')cadmium(II)]-di-[mu]-thiocyanato-[kappa]2N:S;[kappa]2S:N]

M. Chen, X.-D. Chen and M. Du

Formula: [CdCl(NCS)(C10H8N2)]

Online 14 November 2007


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Acta Cryst. (2007). C63, m573-m575  [ doi:10.1107/S0108270107053851 ]

A one-dimensional nickel(II) coordination polymer containing 2,6-dipicolinate and dipyrido[3,2-a:2',3'-c]phenazine

Y. Ma, L.-T. Zhang, X.-F. Wang, Y.-K. He and Z.-B. Han

Formula: [Ni(C7H3NO4)(C18H10N4)]

Online 24 November 2007


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Acta Cryst. (2007). C63, m576-m578  [ doi:10.1107/S0108270107053875 ]

Poly[[diaquamanganese(II)]-[mu]3-4-oxido-2-oxo-1,2-dihydropyrimidine-5-carboxylato-[kappa]4O4,O5:O2:O2]

Z. Chen, H. Xing and F. Liang

Formula: [Mn(C5H2N2O4)(H2O)2]

Online 24 November 2007


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Acta Cryst. (2007). C63, m579-m582  [ doi:10.1107/S0108270107052870 ]

Two mononuclear Tc complexes: [2,2'-(3-phenylpropylimino)- and [2,2'-(propylimino)bis(ethanethiolato)](4-methoxybenzenethiolato)oxidotechnate(V)

F. Emmerling, W. Kraus, B. Noll, S. Noll and H.-J. Pietzsch

Formula: [Tc(C14H21NS2)(C7H7OS)O] and [Tc(C7H15NS2)(C7H7OS)O]

Online 24 November 2007


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Acta Cryst. (2007). C63, m583-m585  [ doi:10.1107/S0108270107053292 ]

A new three-dimensional neutral framework of lanthanum oxalate: [La2(C2O4)3(DMF)(H2O)3]n

J. Wang, X. Huang, C. Huang, H. Song and D. Yang

Formula: [La2(C2O4)3(C3H7NO)(H2O)3]

Online 24 November 2007


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Acta Cryst. (2007). C63, m586-m588  [ doi:10.1107/S0108270107052742 ]

Dichlorido[(S,RS)-1-diphenylphosphino-2-(ethylsulfanylmethyl)ferrocene]palladium(II)

L. Diab, J.-C. Daran, M. Gouygou, E. Manoury and M. Urrutigoïty

Formula: [PdFe(C5H5)(C20H20PS)Cl2]

Online 24 November 2007


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Acta Cryst. (2007). C63, m589-m591  [ doi:10.1107/S0108270107054650 ]

catena-Poly[[aquacopper(II)]-[mu]-hydroxido-[mu]-naphthalene-1-carboxylato-[kappa]2O:O']: effect of a bulky aromatic skeleton in self-assembly

C.-S. Liu, Z. Chang and J.-J. Wang

Formula: [Cu(C11H7O2)(OH)(H2O)]

Online 24 November 2007


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Acta Cryst. (2007). C63, m592-m594  [ doi:10.1107/S0108270107054960 ]

Bis[N,N'-(2-chlorobenzylidene)ethylenediamine-[kappa]2N,N']copper(I) dichloridocuprate(I) acetonitrile solvate

M. H. Habibi, M. Montazerozohori, K. Barati, R. W. Harrington and W. Clegg

Formula: [Cu(C16H14Cl2N2)2][CuCl2]·C2H3N

Online 24 November 2007


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Acta Cryst. (2007). C63, m595-m597  [ doi:10.1107/S0108270107054509 ]

Poly[[triaquazinc(II)]-[mu]3-4-nitrophthalato-[kappa]3O1:O2:O2']

M.-L. Guo and C.-H. Guo

Formula: [Zn(C8H3NO6)(H2O)3]

Online 24 November 2007


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Acta Cryst. (2007). C63, m598-m600  [ doi:10.1107/S0108270107053723 ]

Diaquabis(quinoxaline-2-carboxylato-[kappa]2N1,O)copper(II)

Y. Feng, G. Liu, X.-M. Tian and J.-D. Wang

Formula: [Cu(C9H5N2O2)2(H2O)2]

Online 24 November 2007


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Acta Cryst. (2007). C63, m601-m603  [ doi:10.1107/S0108270107052353 ]

Two isomers of Pd2(S2NC7H4)4

S. Vuoti, M. Haukka and J. Pursiainen

Formula: [Pd2(C7H4NS2)4]·CH2Cl2

Online 24 November 2007


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Acta Cryst. (2007). C63, m604-m609  [ doi:10.1107/S0108270107052286 ]

5-Aminonaphthalene-1-sulfonic acid and its manganese, nickel and cobalt salts

D. J. Genther, P. J. Squattrito, K. Kirschbaum, E. J. Yearley and A. A. Pinkerton

Formula: C10H9NO3S·H2O, [Mn(H2O)6](C10H8NO3S)2·3H2O, [Ni(H2O)6](C10H8NO3S)2·3H2O and [Co(H2O)6](C10H8NO3S)2·2H2O

Online 24 November 2007


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Acta Cryst. (2007). C63, m610-m614  [ doi:10.1107/S0108270107058519 ]

The dinuclear copper(II) complexes di-[mu]-chlorido-bis{[N,N'-bis(4-chlorobenzyl)propane-1,2-diamine]chloridocopper(II)} and di-[mu]-chlorido-bis{[N,N'-bis(3,4-methylenedioxybenzyl)propane-1,2-diamine]chloridocopper(II)}

S.-P. Yang, L.-J. Han, H.-T. Xia, D.-Q. Wang and Y.-F. Liu

Formula: [Cu2Cl4(C17H20Cl2N2)2] and [Cu2Cl4(C19H22N2O4)2]

Online 30 November 2007


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Acta Cryst. (2007). C63, m615-m617  [ doi:10.1107/S0108270107056570 ]

A new coordination mode of 6-methylnicotinic acid in trans-tetraaquabis(6-methylpyridine-3-carboxylato-[kappa]O)cobalt(II) tetrahydrate

B.-M. Kukovec, Z. Popovic and G. Pavlovic

Formula: [Co(C7H6NO2)2(H2O)4]·4H2O

Online 30 November 2007


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Acta Cryst. (2007). C63, m618-m621  [ doi:10.1107/S0108270107055023 ]

[2-(2-Pyridyl)-1H-benzimidazole-[kappa]2N2,N3]bis(p-toluato-[kappa]2O,O')manganese(II)

C.-B. Ma, C.-N. Chen and Q.-T. Liu

Formula: [Mn(C8H7O2)2(C12H9N3)]

Online 30 November 2007


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Acta Cryst. (2007). C63, m622-m624  [ doi:10.1107/S0108270107050597 ]

Intramolecular [pi]-[pi] stacking in diaquabis(2-hydroxybenzoato-[kappa]O)bis(1,10-phenanthroline-[kappa]2N,N')strontium(II)

D.-J. Xu, B.-Y. Zhang, J.-R. Su and J.-J. Nie

Formula: [Sr(C7H5O3)2(C12H8N2)2(H2O)2]

Online 30 November 2007


organic compounds


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Acta Cryst. (2007). C63, o685-o689  [ doi:10.1107/S0108270107049001 ]

Three sterically hindered 6-amino-5-cyano-2-methyl-4-(1-naphthyl)-4H-pyran-3-carboxylate derivatives

V. N. Nesterov, D. J. Wiedenfeld, S. V. Nesterova and L. F. Hastings

Formula: C21H20N2O4, C21H20N2O3 and C20H18N2O3

Online 14 November 2007


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Acta Cryst. (2007). C63, o690-o692  [ doi:10.1107/S0108270107049621 ]

Two 9-[(E)-nitrophenylvinyl]-9H-carbazoles

M. Kubicki, W. Prukala and B. Marciniec

Formula: Two isomers of C20H14N2O2

Online 14 November 2007


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Acta Cryst. (2007). C63, o693-o696  [ doi:10.1107/S0108270107049797 ]

Supramolecular structures of bis-thionooxalamic acid esters derived from (±)-cyclohexane-1,2-diamine and (±)-1,2-diphenylethylenediamine

B. Piotrkowska, T. Polonski and M. Gdaniec

Formula: C14H22N2O4S2 and C22H24N2O4S2

Online 14 November 2007


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Acta Cryst. (2007). C63, o697-o700  [ doi:10.1107/S0108270107049931 ]

A three-dimensional hydrogen-bonded framework in 2-amino-6-(N-methylanilino)pyrimidin-4(3H)-one and a ribbon of fused hydrogen-bonded rings in 2-amino-6-(N-methylanilino)-5-nitropyrimidin-4(3H)-one

R. Rodríguez, J. Cobo, M. Nogueras, J. N. Low and C. Glidewell

Formula: C11H12N4O and C11H11N5O3

Online 14 November 2007


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Acta Cryst. (2007). C63, o701-o703  [ doi:10.1107/S0108270107051591 ]

1,3-Bis[2-(dimethylaminomethyl)phenyl]triselenide

M. Kulcsar, A. Silvestru and F. Cziple

Formula: C18H24N2Se3

Online 14 November 2007


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Acta Cryst. (2007). C63, o704-o710  [ doi:10.1107/S0108270107049426 ]

A series of substituted (2E)-3-(2-fluoro-4-phenoxyphenyl)-1-phenylprop-2-en-1-ones

D. Chopra, T. P. Mohan, B. Vishalakshi and T. N. Guru Row

Formula: C21H15FO2, C21H14F2O2, C21H14ClFO2, C22H17FO2 and C22H17FO3

Online 14 November 2007


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Acta Cryst. (2007). C63, o711-o713  [ doi:10.1107/S0108270107050937 ]

The `cyclophene' [2.2.2](1,2,4)cyclophan-9-ene

K. Broschinski, A. Kannan, P. G. Jones, I. Dix and H. Hopf

Formula: C18H16

Online 14 November 2007


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Acta Cryst. (2007). C63, o714-o716  [ doi:10.1107/S0108270107051049 ]

Hydrogen-bonding interactions in the 4-aminobenzoic acid salt of atenolol monohydrate

B. Lou, D. Boström and S. P. Velaga

Formula: C14H23N2O3+·C7H6NO2-·H2O

Online 14 November 2007


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Acta Cryst. (2007). C63, o717-o719  [ doi:10.1107/S010827010705281X ]

(E)-N'-[5-Chloro-3-methoxy-2-(4-methylphenylsulfonyloxy)benzylidene]isonicotinohydrazide acetic acid solvate: hydrogen-bonded network of alternating R44(42), R55(33) and R66(40) rings

C.-H. Diao, Z. Fan and X. Chen

Formula: C21H18ClN3O5S·C2H4O2

Online 14 November 2007


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Acta Cryst. (2007). C63, o720-o722  [ doi:10.1107/S0108270107046975 ]

Hydrogen-bonded networks in 1-(4-methoxyphenyl)-2,2-dimethylpropan-1-ol

M. Glinski, E. Wilczkowska, I. D. Madura and J. Zachara

Formula: C12H18O2

Online 14 November 2007


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Acta Cryst. (2007). C63, o723-o725  [ doi:10.1107/S0108270107052535 ]

Weak C-H...N[triple bond]C hydrogen bonds in the structures of two poly(cyano)-substituted ring systems

P. G. Jones, H. Hopf, C. Mlynek and V. N. Swaminathan

Formula: C9H3N3 and C20H12N4

Online 14 November 2007


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Acta Cryst. (2007). C63, o726-o728  [ doi:10.1107/S0108270107048664 ]

Packing in three cyclooctitol acetates

G. Mehta, S. Sen and K. Pallavi

Formula: C17H26O8 and C18H28O8

Online 14 November 2007


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Acta Cryst. (2007). C63, o729-o730  [ doi:10.1107/S0108270107050986 ]

An unusual oligomerization/oxidation reaction of a 3-boron-substituted 1-phenylbuta-1,3-diene produces 6,9,16,19-tetraphenyl-5,15-distyryl-3,13,25,26-tetraoxa-2,12-diborapentacyclo[16.2.2.28,11.12,5.112,15]hexacosa-1(20),7,10,17-tetraene

S. De, C. S. Day and M. E. Welker

Formula: C60H54B2O4

Online 14 November 2007


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Acta Cryst. (2007). C63, o731-o733  [ doi:10.1107/S0108270107053218 ]

Monohydrous dihydrogen phosphate salts of norfloxacin and ciprofloxacin

B. Lou, D. Boström and S. P. Velaga

Formula: C16H19FN3O3+·H2PO4-·H2O and C17H19FN3O3+·H2PO4-·H2O

Online 24 November 2007


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Acta Cryst. (2007). C63, o734-o738  [ doi:10.1107/S0108270107053206 ]

Hydrogen-bonding patterns in enaminones: (2Z)-1-(4-bromophenyl)-2-(pyrrolidin-2-ylidene)ethanone and its piperidin-2-ylidene and azepan-2-ylidene analogues

J. L. Balderson, M. A. Fernandes, J. P. Michael and C. B. Perry

Formula: C12H12BrNO, C13H14BrNO and C14H16BrNO

Online 24 November 2007


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Acta Cryst. (2007). C63, o739-o742  [ doi:10.1107/S0108270107053619 ]

2'-(4-Chlorophenyl)-2,3,4,5,6,7-hexahydro-4',7'-methanospiro[9H-fluorene-9,3'-1H-indazole]-1'-carbonitrile and methyl 4'-chloro-2'-(4-chlorophenyl)-1'-cyanospiro[9H-fluorene-9,3'-pyrazolidine]-4'-carboxylate

E. Bilewicz, M. Malecka, S. J. Grabowski and G. Mloston

Formula: C27H22ClN3 and C24H17Cl2N3O2

Online 24 November 2007


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Acta Cryst. (2007). C63, o743-o745  [ doi:10.1107/S0108270107054959 ]

(E)-3-(Benzo[b]thiophen-2-yl)-2-(3,4,5-trimethoxyphenyl)acrylonitrile and (Z)-3-(benzo[b]thiophen-2-yl)-2-(3,4-dimethoxyphenyl)acrylonitrile

V. N. Sonar, S. Parkin and P. A. Crooks

Formula: C20H17NO3S and C19H15NO2S

Online 24 November 2007


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Acta Cryst. (2007). C63, o746-o750  [ doi:10.1107/S0108270107052705 ]

Four substituted pyrazolines

D. Chopra, T. P. Mohan, B. Vishalakshi and T. N. Guru Row

Formula: C27H21FN2O, C27H20ClFN2O, C28H23FN2O and C28H23FN2O2

Online 24 November 2007


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Acta Cryst. (2007). C63, o751-o753  [ doi:10.1107/S0108270107057174 ]

A polymorph of butobarbital with two distinct hydrogen-bonding motifs

T. Gelbrich, N. Zencirci and U. J. Griesser

Formula: C10H16N2O3

Online 24 November 2007


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Acta Cryst. (2007). C63, o754-o757  [ doi:10.1107/S0108270107054571 ]

Three 9-[(E)-2-(4-halogenophenyl)vinyl]-9H-carbazoles

M. Kubicki, W. Prukala and B. Marciniec

Formula: C20H14FN, C20H14ClN and C20H14BrN

Online 24 November 2007


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Acta Cryst. (2007). C63, o758-o760  [ doi:10.1107/S0108270107056569 ]

(E)-3-{2-Amino-4-ethoxy-6-[N-(4-methoxyphenyl)-N-methylamino]pyrimidin-5-yl}-1-phenylprop-2-en-1-one: a boat-shaped pyrimidine ring and a chain of hydrogen-bonded R42(8) and R22(20) rings

J. Trilleras, J. Quiroga, J. N. Low, J. Cobo and C. Glidewell

Formula: C23H24N4O3

Online 30 November 2007


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Acta Cryst. (2007). C63, o761-o762  [ doi:10.1107/S0108270107057939 ]

Benzyl N,N-bis[2-(pentafluoroanilino)ethyl]carbamate

A. V. Churakov, S. S. Karlov, E. Kh. Lermontova, G. S. Zaitseva and J. A. K. Howard

Formula: C24H17F10N3O2

Online 30 November 2007


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