Crystal Structure Communications

 

Acta Cryst. (2008). C64, i33-i34  [ doi:10.1107/S0108270108005167 ]

Hexacopper(I) phosphorus(V) bromide penta(selenide/sulfide), Cu₆P(Se_0.7S_0.3)₅Br

A. Gagor, A. Pietraszko and V. V. Panko

Synopsis: The Cu₆P(Se_0.7S_0.3)₅Br cubic structure is built from a [P(Se_0.7S_0.3)₅Br] framework in which Cu^I ions are distributed in various tetrahedral, triangular and linear sites. The compound is a solid solution of two efficient ionic conductors, namely Cu₆PSe₅Br and Cu₆PS₅Br, in which high ionic conductivity results from order-disorder phenomena in the copper substructure.

Formula: Cu₆P(Se_0.7S_0.3)₅Br

Online 15 March 2008

 

Acta Cryst. (2008). C64, i35-i37  [ doi:10.1107/S0108270108005179 ]

K₂[O(HgSO₃)₃], a new sulfitomercurate with an [OHg₃] core

M. Weil, S. Baumann and D. K. Breitinger

Synopsis: The crystal structure of K₂[O(HgSO₃)₃] features a layered assembly of K⁺ cations and complex [O(HgSO₃)₃]^2- anions with m symmetry and a slightly distorted trigonal-pyramidal OHg₃ core.

Formula: K₂[Hg₃O(SO₃)₃]

Online 15 March 2008

 

Acta Cryst. (2008). C64, i38-i40  [ doi:10.1107/S0108270108002801 ]

Ba₃Li₂V₂O₇Cl₄, a new vanadate with a channel structure

T. Reeswinkel, K. M. Sparta and G. Roth

Synopsis: The title compound contains a unique framework of LiO₄ and VO₄ tetrahedra, which are linked to produce porous double layers separated along the c direction by isolated chains of face-sharing LiCl₆ octahedra. Within the layers, six-tetrahedron Li₂V₄O₁₈ rings form large channels filled by Ba²⁺ and Cl^- ions.

Formula: Ba₃Li₂V₂O₇Cl₄

Online 15 March 2008

 

Acta Cryst. (2008). C64, m147-m148  [ doi:10.1107/S0108270108004666 ]

1,5-Asymmetric induction during nucleophilic additions to arenetricarbonylchromium complexes: tricarbonyl(⁶-1-methyl-4-{spiro[(1R,2S)-1,7,7-trimethylbicyclo[2.2.1]heptane-3,2'-1,3-dioxolan]-2-yloxy}benzene)chromium

H. Paramahamsan, A. J. Pearson, N. M. Pinkerton and A. A. Pinkerton

Formula: [Cr(C₁₉H₂₆O₃)(CO)₃]

Online 8 March 2008

 

Acta Cryst. (2008). C64, m149-m152  [ doi:10.1107/S0108270108003296 ]

Diacetonitrile-1N,3N-bis{-trans-N-[3-(dimethylamino)propyl]-N'-(2-hydroxyethyl)oxamidato(2-)}-1:2⁵N,N',O:O',N'';2:3⁵O',N'':N,N',O-dithiocyanato-1N,3N-tricopper(II)

J.-L. Liu, C.-W. Yan, Y.-T. Li, Z.-Y. Wu and W.-J. Zhang

Formula: [Cu₃(C₉H₁₇N₃O₃)₂(NCS)₂(C₂H₃N)₂]

Online 8 March 2008

 

Acta Cryst. (2008). C64, m153-m155  [ doi:10.1107/S0108270108005003 ]

Dibromido(dimethyl sulfoxide-O)(1,10-phenanthroline-²N,N')copper(II)

M.-J. Oh, H.-J. Kim, S. K. Kang, S.-N. Choi and Y.-M. Lee

Formula: [CuBr₂(C₁₂H₈N₂)(C₂H₆OS)]

Online 8 March 2008

 

Acta Cryst. (2008). C64, m156-m160  [ doi:10.1107/S0108270108004289 ]

Mononuclear nickel(II) and zinc(II) complexes with deprotonated forms of the tripodal hexadentate ligand 1,3-bis(2-hydroxybenzylidene)-2-(2-hydroxybenzylideneaminomethyl)-2-methylpropane-1,3-diamine

T. Yamaguchi, Y. Sunatsuki and H. Ishida

Formula: [Ni(C₂₆H_25.5N₃O₃)]₂Cl·2CH₄O and [Zn(C₂₆H₂₅N₃O₃)]ClO₄·[Zn(C₂₆H₂₆N₃O₃)]·3CH₄O

Online 8 March 2008

 

Acta Cryst. (2008). C64, m161-m163  [ doi:10.1107/S0108270108005970 ]

Low-dimensional compounds containing cyano groups. XVI. (Dicyanamido-N¹)bis(1,10-phenanthroline-²N,N')copper(II) tetrafluoridoborate

I. Potocnák, M. Spilovský and Z. Trávnícek

Formula: [Cu(C₂N₃)(C₁₂H₈N₂)₂]BF₄

Online 15 March 2008

 

Acta Cryst. (2008). C64, m164-m166  [ doi:10.1107/S0108270108006057 ]

catena-Poly[[(acetato-²O,O')triaquabarium(II)]-₃-acetato-⁴O:O,O':O']

E. Freire and R. Baggio

Formula: [Ba(C₂H₃O₂)₂(H₂O)₃]

Online 15 March 2008

 

Acta Cryst. (2008). C64, m167-m169  [ doi:10.1107/S0108270108005349 ]

A mixed bridged trinuclear copper(II)-1,10-phenanthroline complex with a linear structure

F. Chen, W.-M. Lu and Y. Zhu

Formula: [Cu₃(C₄H₅O₂)₂(OH)₂(C₁₂H₈N₂)₂(H₂O)₂](NO₃)₂·2H₂O

Online 15 March 2008

 

Acta Cryst. (2008). C64, m170-m172  [ doi:10.1107/S0108270108005143 ]

Poly[(₂-2,2-dimethylpropane-1,3-diyl diisocyanide)-₂-nitrato-silver(I)]: a powder study

M. Rukiah and M. Al-Ktaifani

Formula: [Ag(NO₃)(C₇H₁₀N₂)]

Online 15 March 2008

 

Acta Cryst. (2008). C64, m173-m175  [ doi:10.1107/S0108270108005428 ]

Poly[[diaquabis(₂-1-oxo-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane-4-carboxylato)copper(II)] dihydrate]

M.-L. Guo and H.-J. Zang

Formula: [Cu(C₅H₆O₆P)₂(H₂O)₂]·2H₂O

Online 20 March 2008

 

Acta Cryst. (2008). C64, m176-m178  [ doi:10.1107/S0108270108006975 ]

Hexaquacobalt(II) bis(5-hydroxy-7-methoxy-4-oxo-2-phenyl-4H-chromene-6-sulfonate) tetrahydrate

W.-W. Li and Z.-T. Zhang

Formula: [Co(H₂O)₆](C₁₆H₁₁O₇S)₂·4H₂O

Online 20 March 2008

 

Acta Cryst. (2008). C64, m179-m181  [ doi:10.1107/S0108270108006306 ]

(N-{[4-(1,3-Benzothiazol-2-yl)anilino]carbonylmethyl-O}iminodiacetato-³O,N,O')(1,10-phenanthroline-²N,N')cobalt(II) pentahydrate

G.-W. Lin, Y. Wang and T. Lu

Formula: [Co(C₁₉H₁₅N₃O₅S)(C₁₂H₈N₂)]·5H₂O

Online 29 March 2008

 

Acta Cryst. (2008). C64, m182-m184  [ doi:10.1107/S0108270108007166 ]

Bis{-(E)-2-[(2-pyridylamino)(2-pyridylimino)methyl]benzato}bis[acetatozinc(II)] tetrahydrate

L.-N. Zhu, S. Gao and L.-H. Huo

Formula: [Zn₂(C₁₈H₁₃N₄O₂)₂(C₂H₃O₂)₂]·4H₂O

Online 29 March 2008

 

Acta Cryst. (2008). C64, o187-o190  [ doi:10.1107/S0108270108003776 ]

5-Iodobenzofurazan 1-oxide: polymorphs, pseudosymmetry and disorder

D. Britton, W. E. Noland and C. M. Clark

Formula: Two polymorphs of C₆H₃IN₂O₂

Online 8 March 2008

 

Acta Cryst. (2008). C64, o191-o194  [ doi:10.1107/S0108270108002096 ]

Hydrogen-bonded chains of rings in 1-(4-chloroanilinomethyl)-5-(4-chlorophenyl)-1,3,5-triazinane-2-thione and hydrogen-bonded sheets in 1-anilinomethyl-5-phenyl-1,3,5-triazinane-2-thione

Z. Zhang, D. Xian, J. Li and G. Zhang

Formula: C₁₆H₁₆Cl₂N₄S and C₁₆H₁₈N₄S

Online 8 March 2008

 

Acta Cryst. (2008). C64, o195-o198  [ doi:10.1107/S0108270108005593 ]

Geometry and bond-length alternation in nonlinear optical materials. II. Effects of donor strength in two push-pull molecules

G. J. Gainsford, M. D. H. Bhuiyan and A. J. Kay

Formula: C₂₀H₁₆N₄O₂ and C₁₇H₁₈N₄O·0.376H₂O

Online 8 March 2008

 

Acta Cryst. (2008). C64, o199-o204  [ doi:10.1107/S0108270108004290 ]

Five bicyclo[3.3.0]octa-2,6-dienes

A. Vega, O. Donoso-Tauda, A. Ibañez and C. A. Escobar

Formula: C₁₆H₁₈O₁₀, C₁₈H₂₂O₁₀, C₂₀H₂₆O₁₀ and C₂₀H₂₂O₁₂

Online 8 March 2008

 

Acta Cryst. (2008). C64, o205-o207  [ doi:10.1107/S0108270108005696 ]

-Sulfanilamide

T. Gelbrich, A. L. Bingham, T. L. Threlfall and M. B. Hursthouse

Formula: C₆H₈N₂O₂S

Online 8 March 2008

 

Acta Cryst. (2008). C64, o208-o210  [ doi:10.1107/S0108270108005799 ]

Conformation of hydrogen-bonded dimeric o-methyl-substituted benzoic acids

M. Glinski, E. Wilczkowska, I. D. Madura and J. Zachara

Formula: C₉H₁₀O₂

Online 8 March 2008

 

Acta Cryst. (2008). C64, o211-o213  [ doi:10.1107/S0108270108005957 ]

2,6-Dimethoxy-7,9-dimethylpurinium iodide hemihydrate

A. Kowalska, K. Pluta and K. Suwinska

Formula: C₉H₁₃N₄O₂⁺·I^-·0.5H₂O

Online 8 March 2008

 

Acta Cryst. (2008). C64, o214-o216  [ doi:10.1107/S0108270108005763 ]

Accurate stereochemistry for two related 22,26-epiminocholestene derivatives

J. L. Vega-Baez, J. Sandoval-Ramírez, S. Meza-Reyes, S. Montiel-Smith, V. Gómez-Calvario and S. Bernès

Formula: C₃₁H₄₇NO₄ and C₂₉H₄₇NO₃

Online 15 March 2008

 

Acta Cryst. (2008). C64, o217-o219  [ doi:10.1107/S0108270108005842 ]

1H-Indazole and 2H-indazole derivatives of androsta-5,16-dien-3-ol

M. Ramos Silva, V. M. Moreira, C. Cardoso, A. Matos Beja and J. A. R. Salvador

Formula: Two isomers of C₂₆H₃₂N₂O

Online 15 March 2008

 

Acta Cryst. (2008). C64, o220-o225  [ doi:10.1107/S0108270108005076 ]

Hydrogen-bonded sheet structures in neutral, anionic and hydrated 6-amino-2-(morpholin-4-yl)-5-nitrosopyrimidines

F. Orozco, B. Insuasty, J. N. Low, J. Cobo and C. Glidewell

Formula: C₉H₁₃N₅O₃, C₄H₁₀NO⁺·C₈H₁₀N₅O₃^- and C₈H₁₁N₅O₃·0.5H₂O

Online 15 March 2008

 

Acta Cryst. (2008). C64, o226-o229  [ doi:10.1107/S0108270108006471 ]

Hydrogen bonding in the bromide salts of 4-aminobenzoic acid and 4-aminoacetophenone

D. Cincic and B. Kaitner

Formula: C₇H₈NO₂⁺·Br^- and C₈H₁₀NO⁺·Br^-

Online 15 March 2008

 

Acta Cryst. (2008). C64, o230-o232  [ doi:10.1107/S0108270108006318 ]

(1-Pyridinio)perfluorophenacylide: a new stable pyridinium ylide in the enol form

S. Yamada and E. Ohta

Formula: C₁₃H₆F₅NO

Online 15 March 2008

 

Acta Cryst. (2008). C64, o233-o236  [ doi:10.1107/S0108270108006963 ]

Ethyl 2-methoxy-6-[(triphenylphosphoranylidene)amino]nicotinate and ethyl 2-methylsulfanyl-6-[(triphenylphosphoranylidene)amino]nicotinate

J. Cobo, C. Glidewell, J. N. Low and F. Orozco

Formula: C₂₇H₂₅N₂O₃P and C₂₇H₂₅N₂O₂PS

Online 20 March 2008

 

Acta Cryst. (2008). C64, o237-o241  [ doi:10.1107/S0108270108007117 ]

Hydrate frameworks involving the pyridazino[4,5-d]pyridazine unit as a multiple hydrogen-bond acceptor

I. S. Zhylenko, P. V. Solntsev, E. B. Rusanov, A. N. Chernega and K. V. Domasevitch

Formula: C₁₀H₁₂N₄·3H₂O and C₁₂H₁₂N₄·4H₂O

Online 20 March 2008

 

Acta Cryst. (2008). C64, o242-o244  [ doi:10.1107/S0108270108006045 ]

2,4-Bis[1-(4-hydroxyphenyl)-1-methylethyl]phenol: a three-dimensional framework built from O-HO hydrogen bonds

E. Rozycka-Sokolowska

Formula: C₂₄H₂₆O₃

Online 29 March 2008