################################################################## # 2-(2-aminophenyl)-1H-benzimidazol-3-ium dihydrogen phosphate: # # anion-anion one-dimensional chain # # Shylaja et al. (2008) Acta Crystallographica-C # ################################################################## # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title 'Benzimidazolylaniline dihydrogen phosphate in C2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 247.27 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.8111 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 18.3700 _cell_length_b 10.0050 _cell_length_c 7.9145 _cell_angle_alpha 90.000 _cell_angle_beta 113.575 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -12 0 2.50 0.41 10.30 o 2 -12 0 9.15 8.38 7.79 o 4 -12 0 1.34 7.18 8.46 o 1 -11 0 573.53 580.31 26.00 o 3 -11 0 519.66 518.95 26.16 o 5 -11 0 138.88 146.81 13.79 o 7 -11 0 2.73 -10.78 12.66 o 9 -11 0 24.02 30.16 19.85 o 0 -10 0 182.03 174.93 18.76 o 2 -10 0 214.00 218.29 15.05 o 4 -10 0 90.21 80.55 9.88 o 6 -10 0 188.07 189.09 14.42 o 8 -10 0 49.74 50.38 13.34 o 10 -10 0 4.01 -5.91 5.91 o 12 -10 0 32.69 14.40 8.73 o 1 -9 0 2176.93 2257.30 47.22 o 3 -9 0 594.30 577.50 23.08 o 5 -9 0 888.11 882.08 29.00 o 7 -9 0 168.27 172.82 13.23 o 9 -9 0 430.30 395.86 29.10 o 11 -9 0 37.46 44.23 11.26 o 13 -9 0 26.80 2.05 8.26 o 0 -8 0 296.24 278.29 20.95 o 2 -8 0 103.36 123.39 10.54 o 4 -8 0 182.63 161.68 21.83 o 6 -8 0 157.01 163.33 9.94 o 8 -8 0 698.69 657.39 20.54 o 10 -8 0 195.00 200.60 11.80 o 12 -8 0 259.57 253.71 13.93 o 14 -8 0 145.27 143.46 14.87 o 1 -7 0 14.17 11.32 3.20 o 3 -7 0 166.50 173.61 12.81 o 5 -7 0 1257.60 1307.99 26.43 o 7 -7 0 676.16 670.32 19.13 o 9 -7 0 239.32 222.25 11.70 o 11 -7 0 1016.28 955.00 36.00 o 13 -7 0 819.98 779.20 24.01 o 15 -7 0 368.53 332.92 21.45 o 17 -7 0 89.53 95.70 13.11 o 0 -6 0 833.01 912.06 23.20 o 2 -6 0 1.47 1.47 2.42 o 4 -6 0 12.20 7.28 4.37 o 6 -6 0 194.87 213.77 7.67 o 8 -6 0 1030.98 1000.83 23.11 o 10 -6 0 296.96 281.09 13.23 o 12 -6 0 158.98 158.65 10.13 o 14 -6 0 176.35 189.99 12.63 o 16 -6 0 137.74 147.33 14.77 o 18 -6 0 139.46 146.51 15.77 o 1 -5 0 616.23 585.47 11.92 o 3 -5 0 1374.94 1481.96 28.10 o 5 -5 0 163.23 143.44 5.77 o 7 -5 0 1004.87 934.30 15.86 o 9 -5 0 166.57 175.51 9.72 o 11 -5 0 604.56 614.45 20.34 o 13 -5 0 293.74 275.73 13.14 o 15 -5 0 18.42 23.47 5.57 o 17 -5 0 41.89 50.71 19.38 o 0 -4 0 3562.28 3952.46 49.68 o 2 -4 0 67.35 66.89 3.51 o 4 -4 0 698.09 698.89 11.68 o 6 -4 0 2640.22 2905.12 28.97 o 8 -4 0 269.15 270.11 8.15 o 10 -4 0 307.26 291.61 9.24 o 12 -4 0 1699.61 1730.78 32.03 o 14 -4 0 322.88 332.27 14.52 o 16 -4 0 223.28 226.52 16.71 o 18 -4 0 12.32 5.21 7.70 o 1 -3 0 1193.02 957.95 26.84 o 3 -3 0 2315.45 2688.95 24.17 o 5 -3 0 162.98 147.26 5.00 o 7 -3 0 280.23 299.55 7.82 o 9 -3 0 581.91 594.22 12.31 o 11 -3 0 184.82 190.18 7.59 o 13 -3 0 194.23 191.18 10.01 o 15 -3 0 448.31 434.88 21.83 o 17 -3 0 104.24 104.00 11.89 o 19 -3 0 15.29 20.09 10.51 o 0 -2 0 29055.56 29232.38 264.82 o 2 -2 0 2501.19 2483.38 20.58 o 4 -2 0 4100.10 3928.94 31.10 o 6 -2 0 1644.37 1787.55 19.66 o 8 -2 0 643.13 643.33 11.97 o 10 -2 0 302.20 281.12 8.71 o 12 -2 0 1522.59 1378.16 26.16 o 14 -2 0 387.96 347.54 18.25 o 16 -2 0 529.37 470.35 25.48 o 18 -2 0 17.43 30.49 8.60 o 20 -2 0 137.48 142.30 19.61 o 1 -1 0 323.02 209.18 3.73 o 3 -1 0 17673.99 18183.47 112.33 o 5 -1 0 680.23 599.20 7.82 o 7 -1 0 58.27 61.68 3.13 o 9 -1 0 1156.99 1341.69 22.39 o 11 -1 0 477.80 436.63 13.50 o 13 -1 0 882.30 864.52 21.02 o 15 -1 0 735.83 756.18 21.03 o 17 -1 0 43.02 55.55 9.04 o 19 -1 0 74.15 63.16 10.08 o 2 0 0 10275.93 11200.48 82.65 o 4 0 0 7879.85 8049.65 59.45 o 6 0 0 128.42 165.73 5.33 o 8 0 0 1837.52 1775.23 21.50 o 10 0 0 100.39 121.04 6.01 o 12 0 0 44.61 44.20 5.05 o 14 0 0 47.58 39.02 6.27 o 16 0 0 505.97 487.25 17.66 o 18 0 0 46.92 42.37 6.62 o 20 0 0 104.10 137.75 22.38 o 1 1 0 338.99 218.51 4.29 o 3 1 0 17659.21 18151.39 136.86 o 5 1 0 657.09 598.46 11.79 o 7 1 0 50.79 52.88 7.14 o 9 1 0 1159.17 1326.48 19.75 o 11 1 0 464.81 442.36 12.06 o 13 1 0 876.29 875.61 21.70 o 15 1 0 742.68 729.65 26.70 o 17 1 0 43.41 45.13 6.15 o 19 1 0 75.21 69.05 10.30 o 0 2 0 29062.06 29551.07 365.32 o 2 2 0 2509.51 2477.43 21.80 o 4 2 0 4097.49 3952.68 57.63 o 6 2 0 1649.07 1790.91 19.07 o 8 2 0 647.63 629.70 15.35 o 10 2 0 309.45 288.34 20.15 o 12 2 0 1531.30 1445.94 24.10 o 14 2 0 381.62 366.64 14.42 o 16 2 0 527.02 525.50 18.70 o 18 2 0 18.11 31.54 6.94 o 20 2 0 136.40 162.07 23.40 o 1 3 0 1184.31 953.74 12.52 o 3 3 0 2317.13 2696.50 25.69 o 5 3 0 167.67 142.23 4.93 o 7 3 0 276.78 303.76 10.57 o 9 3 0 572.93 587.54 16.13 o 11 3 0 181.08 171.40 10.09 o 13 3 0 196.93 202.13 10.94 o 15 3 0 451.92 441.52 16.75 o 17 3 0 103.24 115.78 9.43 o 19 3 0 15.91 0.92 5.92 o 0 4 0 3563.59 3895.62 69.62 o 2 4 0 66.72 54.38 4.49 o 4 4 0 698.18 704.55 12.27 o 6 4 0 2640.87 2950.24 30.60 o 8 4 0 268.93 244.35 10.45 o 10 4 0 307.62 291.39 12.17 o 12 4 0 1699.60 1724.34 33.26 o 14 4 0 322.83 306.03 14.29 o 16 4 0 223.39 224.21 12.54 o 18 4 0 12.36 17.10 6.19 o 1 5 0 608.72 585.13 11.86 o 3 5 0 1377.01 1522.23 24.56 o 5 5 0 167.99 157.25 6.37 o 7 5 0 1000.09 968.83 16.61 o 9 5 0 165.45 175.75 9.58 o 11 5 0 602.51 611.41 18.97 o 13 5 0 294.59 275.68 13.62 o 15 5 0 18.88 24.43 5.19 o 17 5 0 40.83 54.65 10.78 o 0 6 0 847.94 909.88 23.05 o 2 6 0 2.52 3.75 2.88 o 4 6 0 10.31 14.02 4.69 o 6 6 0 188.47 186.38 7.54 o 8 6 0 1042.38 1066.94 23.83 o 10 6 0 299.03 292.10 17.14 o 12 6 0 160.45 157.77 15.93 o 14 6 0 169.68 165.88 17.30 o 16 6 0 139.67 135.94 19.31 o 18 6 0 139.56 171.18 20.40 o 1 7 0 12.35 11.23 3.48 o 3 7 0 159.82 161.73 9.24 o 5 7 0 1262.83 1364.93 22.16 o 7 7 0 673.25 700.61 25.50 o 9 7 0 230.46 226.65 15.32 o 11 7 0 1011.16 931.07 32.24 o 13 7 0 822.78 748.88 29.89 o 15 7 0 370.38 345.30 30.97 o 17 7 0 89.31 113.82 12.69 o 0 8 0 300.27 281.38 14.96 o 2 8 0 103.64 108.94 6.91 o 4 8 0 189.19 184.11 13.48 o 6 8 0 149.02 134.39 12.14 o 8 8 0 710.09 673.33 28.79 o 10 8 0 199.03 196.93 19.61 o 12 8 0 262.22 279.66 18.60 o 14 8 0 141.77 124.99 13.57 o 1 9 0 2170.58 2276.02 32.96 o 3 9 0 597.52 601.95 19.69 o 5 9 0 893.08 893.73 30.90 o 7 9 0 168.79 148.95 13.55 o 9 9 0 423.55 347.16 20.37 o 11 9 0 36.55 31.92 12.62 o 13 9 0 27.68 50.01 9.47 o 0 10 0 190.98 191.24 21.49 o 2 10 0 211.08 192.91 12.07 o 4 10 0 87.06 92.85 10.79 o 6 10 0 186.39 174.71 16.03 o 8 10 0 52.09 44.36 11.19 o 10 10 0 4.91 -5.70 5.70 o 12 10 0 33.43 17.75 7.20 o 1 11 0 572.40 550.15 27.23 o 3 11 0 521.71 524.65 25.09 o 5 11 0 138.50 137.80 45.57 o 7 11 0 3.16 4.50 6.57 o 9 11 0 24.72 15.96 9.62 o 0 12 0 2.50 -2.46 9.89 o 2 12 0 9.10 13.44 11.26 o 4 12 0 1.33 6.48 10.30 o -4 -12 1 516.08 554.24 26.80 o -2 -12 1 397.47 419.20 36.54 o 0 -12 1 312.80 341.03 20.94 o 2 -12 1 256.25 271.63 19.12 o -9 -11 1 146.05 152.55 20.19 o -7 -11 1 135.51 145.38 13.43 o -5 -11 1 176.29 176.41 14.68 o -3 -11 1 178.93 177.83 14.69 o -1 -11 1 613.98 601.58 26.24 o 1 -11 1 232.73 231.06 38.55 o 3 -11 1 95.85 94.09 11.72 o 5 -11 1 134.90 157.55 22.72 o 7 -11 1 24.65 21.41 7.65 o -12 -10 1 52.15 55.26 13.85 o -10 -10 1 12.07 10.44 8.60 o -8 -10 1 180.36 193.34 26.34 o -6 -10 1 54.57 51.63 8.37 o -4 -10 1 60.14 61.05 8.56 o -2 -10 1 90.43 95.26 10.39 o 0 -10 1 331.30 331.66 18.57 o 2 -10 1 689.24 710.79 27.50 o 4 -10 1 222.52 215.06 19.65 o 6 -10 1 202.85 178.87 14.11 o 8 -10 1 146.66 159.70 13.82 o 10 -10 1 116.17 138.35 14.67 o -13 -9 1 59.47 71.42 13.58 o -11 -9 1 35.03 56.76 15.76 o -9 -9 1 203.17 204.31 12.09 o -7 -9 1 508.55 483.85 19.57 o -5 -9 1 4.90 3.58 4.94 o -3 -9 1 459.26 459.52 20.27 o -1 -9 1 242.15 266.99 15.44 o 1 -9 1 112.70 117.90 10.66 o 3 -9 1 257.38 224.80 16.37 o 5 -9 1 488.20 487.81 21.83 o 7 -9 1 153.29 163.01 18.56 o 9 -9 1 112.78 139.19 12.64 o 11 -9 1 232.14 267.23 31.76 o 13 -9 1 85.33 88.74 11.33 o -16 -8 1 105.05 116.15 13.65 o -14 -8 1 44.43 75.30 11.25 o -12 -8 1 128.84 153.22 14.31 o -10 -8 1 16.17 8.70 4.53 o -8 -8 1 954.72 909.60 23.96 o -6 -8 1 330.20 314.68 11.00 o -4 -8 1 660.32 634.37 19.18 o -2 -8 1 121.57 136.08 9.03 o 0 -8 1 411.45 384.30 22.48 o 2 -8 1 21.96 33.50 6.37 o 4 -8 1 131.64 101.35 9.74 o 6 -8 1 793.82 727.04 25.62 o 8 -8 1 178.99 152.40 12.25 o 10 -8 1 31.00 36.45 6.89 o 12 -8 1 1.26 -2.28 4.96 o 14 -8 1 73.42 108.60 21.29 o -17 -7 1 38.49 31.50 8.18 o -15 -7 1 98.68 119.86 13.34 o -13 -7 1 12.09 25.34 7.05 o -11 -7 1 873.24 827.37 42.89 o -9 -7 1 323.27 279.39 19.73 o -7 -7 1 523.50 523.57 13.36 o -5 -7 1 101.29 89.99 5.68 o -3 -7 1 291.85 287.10 13.73 o -1 -7 1 184.94 176.80 9.35 o 1 -7 1 98.83 111.35 8.17 o 3 -7 1 234.37 238.39 10.57 o 5 -7 1 1200.67 1223.77 25.72 o 7 -7 1 176.28 188.23 11.11 o 9 -7 1 114.65 108.14 8.79 o 11 -7 1 37.55 35.69 6.71 o 13 -7 1 18.37 27.69 6.48 o 15 -7 1 8.20 4.07 7.03 o -18 -6 1 56.76 46.79 13.88 o -16 -6 1 27.19 42.36 8.19 o -14 -6 1 265.50 229.60 18.28 o -12 -6 1 72.43 74.00 7.04 o -10 -6 1 16.79 13.68 3.55 o -8 -6 1 570.84 533.69 12.85 o -6 -6 1 1085.75 1125.78 23.88 o -4 -6 1 238.75 212.34 7.77 o -2 -6 1 185.02 193.70 8.97 o 0 -6 1 157.78 183.15 7.15 o 2 -6 1 346.27 368.95 11.81 o 4 -6 1 990.88 913.98 20.21 o 6 -6 1 1393.98 1317.51 31.02 o 8 -6 1 3021.60 3028.86 69.62 o 10 -6 1 380.31 342.45 15.68 o 12 -6 1 596.42 596.27 21.02 o 14 -6 1 125.27 124.89 10.48 o 16 -6 1 41.81 55.27 7.93 o -19 -5 1 139.43 144.35 17.47 o -17 -5 1 228.02 275.09 18.96 o -15 -5 1 355.50 345.26 19.75 o -13 -5 1 69.10 61.85 6.53 o -11 -5 1 841.85 790.16 16.27 o -9 -5 1 669.51 639.22 13.78 o -7 -5 1 1074.36 1092.13 17.38 o -5 -5 1 293.79 304.48 12.52 o -3 -5 1 369.93 391.34 8.00 o -1 -5 1 581.52 667.50 12.23 o 1 -5 1 357.79 361.85 10.43 o 3 -5 1 3065.24 3271.58 47.83 o 5 -5 1 2231.07 2149.19 23.85 o 7 -5 1 1679.45 1615.90 49.30 o 9 -5 1 2434.64 2448.33 39.19 o 11 -5 1 1902.49 1875.50 35.67 o 13 -5 1 272.49 259.12 13.55 o 15 -5 1 99.47 100.09 13.04 o 17 -5 1 29.27 25.79 10.00 o -20 -4 1 99.38 115.78 21.63 o -18 -4 1 102.95 123.54 13.11 o -16 -4 1 645.63 607.13 33.29 o -14 -4 1 330.41 322.23 10.96 o -12 -4 1 463.34 434.28 11.81 o -10 -4 1 290.51 261.05 8.53 o -8 -4 1 2460.84 2553.62 28.26 o -6 -4 1 2353.62 2538.76 26.75 o -4 -4 1 448.00 443.29 9.48 o -2 -4 1 417.27 430.38 7.44 o 0 -4 1 378.95 368.75 9.06 o 2 -4 1 1950.29 2061.96 26.71 o 4 -4 1 2205.75 2247.79 33.10 o 6 -4 1 3175.67 3270.18 38.32 o 8 -4 1 2119.13 2033.79 32.97 o 10 -4 1 1492.16 1449.61 28.94 o 12 -4 1 976.04 929.53 24.19 o 14 -4 1 250.21 256.88 13.48 o 16 -4 1 109.37 105.65 13.68 o 18 -4 1 123.21 154.65 16.02 o -19 -3 1 163.47 165.80 15.04 o -17 -3 1 83.31 60.42 9.17 o -15 -3 1 336.86 319.67 13.40 o -13 -3 1 476.85 456.16 17.04 o -11 -3 1 340.37 324.42 9.59 o -9 -3 1 2890.69 2940.51 30.47 o -7 -3 1 2262.32 2206.90 23.73 o -5 -3 1 6026.04 5961.80 45.87 o -3 -3 1 5951.85 5915.92 44.46 o -1 -3 1 1418.49 1410.28 17.86 o 1 -3 1 71.24 92.14 8.71 o 3 -3 1 662.04 602.64 12.77 o 5 -3 1 1945.01 1968.09 20.68 o 7 -3 1 1450.53 1370.69 18.21 o 9 -3 1 830.23 840.63 15.31 o 11 -3 1 488.87 514.61 16.93 o 13 -3 1 1012.20 983.94 25.62 o 15 -3 1 63.62 71.94 9.94 o 17 -3 1 84.77 91.85 18.76 o 19 -3 1 42.27 50.69 10.76 o -20 -2 1 23.18 61.34 15.62 o -18 -2 1 10.99 -0.19 13.07 o -16 -2 1 1087.66 1073.36 25.60 o -14 -2 1 6.60 -0.04 3.98 o -12 -2 1 598.99 594.70 16.01 o -10 -2 1 3159.97 3290.35 29.42 o -8 -2 1 2242.76 2274.53 24.05 o -6 -2 1 4565.49 4703.74 37.75 o -4 -2 1 4094.56 4283.59 35.95 o -2 -2 1 5154.85 5426.70 62.27 o 0 -2 1 588.26 615.32 8.23 o 2 -2 1 864.88 776.89 12.98 o 4 -2 1 106.19 85.27 3.28 o 6 -2 1 671.54 681.78 11.39 o 8 -2 1 186.57 222.70 7.20 o 10 -2 1 181.46 177.63 8.66 o 12 -2 1 223.03 203.39 14.33 o 14 -2 1 206.31 179.23 14.28 o 16 -2 1 107.75 105.61 15.76 o 18 -2 1 23.33 26.37 8.66 o -21 -1 1 6.82 6.14 10.44 o -19 -1 1 8.76 9.06 5.63 o -17 -1 1 257.59 257.17 12.78 o -15 -1 1 80.72 76.91 8.99 o -13 -1 1 262.50 259.84 12.37 o -11 -1 1 258.26 250.98 8.44 o -9 -1 1 1330.22 1381.05 18.89 o -7 -1 1 6063.23 6417.41 49.98 o -5 -1 1 6202.94 6735.58 46.90 o -3 -1 1 802.75 923.20 13.00 o -1 -1 1 1491.86 1465.92 14.28 o 1 -1 1 2453.00 2236.64 22.37 o 3 -1 1 886.96 816.61 11.20 o 5 -1 1 697.47 698.05 10.91 o 7 -1 1 810.72 826.56 14.35 o 9 -1 1 21.72 21.73 3.30 o 11 -1 1 347.47 330.59 12.36 o 13 -1 1 418.34 372.15 14.86 o 15 -1 1 214.54 197.53 15.43 o 17 -1 1 46.27 60.44 13.03 o 19 -1 1 42.04 45.24 11.70 o -20 0 1 10.34 11.29 5.76 o -18 0 1 128.09 162.42 13.16 o -16 0 1 98.47 106.35 7.88 o -14 0 1 92.18 100.13 8.05 o -12 0 1 32.05 23.29 3.74 o -10 0 1 244.00 275.34 8.51 o -8 0 1 597.21 534.49 10.58 o -6 0 1 1344.62 1153.97 14.34 o -4 0 1 7.64 6.00 2.19 o -2 0 1 127.40 67.26 2.99 o 0 0 1 68.67 45.41 1.79 o 2 0 1 0.44 0.45 1.14 o 4 0 1 949.87 877.37 12.77 o 6 0 1 4043.71 4455.27 37.79 o 8 0 1 4.86 6.45 2.26 o 10 0 1 23.28 26.45 3.29 o 12 0 1 170.81 189.05 9.95 o 14 0 1 770.79 720.38 20.74 o 16 0 1 0.60 -0.83 5.26 o 18 0 1 17.61 18.48 14.60 o -21 1 1 6.88 13.94 6.47 o -19 1 1 8.37 4.16 5.50 o -17 1 1 254.87 242.66 15.83 o -15 1 1 81.73 84.63 7.06 o -13 1 1 264.47 274.99 10.12 o -11 1 1 263.47 245.03 8.65 o -9 1 1 1336.46 1374.60 19.21 o -7 1 1 6069.63 6487.30 103.83 o -5 1 1 6207.50 6719.11 50.42 o -3 1 1 808.36 959.39 11.01 o -1 1 1 1490.44 1492.86 15.49 o 1 1 1 2447.71 2233.52 19.85 o 3 1 1 875.32 808.46 13.04 o 5 1 1 687.92 679.09 13.14 o 7 1 1 799.12 834.57 16.21 o 9 1 1 23.60 26.19 3.31 o 11 1 1 340.92 331.27 10.47 o 13 1 1 423.41 393.36 14.90 o 15 1 1 218.44 227.93 13.07 o 17 1 1 45.99 72.14 7.74 o 19 1 1 41.79 74.43 11.22 o -20 2 1 22.42 27.39 8.36 o -18 2 1 12.33 19.69 12.38 o -16 2 1 1094.55 1059.78 32.90 o -14 2 1 7.78 7.07 5.52 o -12 2 1 591.73 580.33 14.37 o -10 2 1 3150.99 3242.27 42.11 o -8 2 1 2256.70 2283.88 25.17 o -6 2 1 4570.28 4737.50 39.79 o -4 2 1 4086.61 4267.39 34.72 o -2 2 1 5127.54 5414.33 46.38 o 0 2 1 594.70 605.88 22.31 o 2 2 1 891.68 807.10 11.08 o 4 2 1 101.54 77.83 4.84 o 6 2 1 654.58 676.41 14.93 o 8 2 1 196.83 231.41 9.41 o 10 2 1 186.75 173.98 8.96 o 12 2 1 220.12 208.35 9.56 o 14 2 1 198.90 190.15 10.74 o 16 2 1 106.95 108.93 11.36 o 18 2 1 24.21 27.84 12.66 o -19 3 1 163.42 157.32 14.08 o -17 3 1 81.28 76.50 10.20 o -15 3 1 327.33 332.69 12.36 o -13 3 1 477.24 463.80 16.38 o -11 3 1 346.32 333.71 12.90 o -9 3 1 2874.05 2934.12 31.63 o -7 3 1 2232.40 2206.97 24.79 o -5 3 1 6017.24 5987.71 48.07 o -3 3 1 5942.00 5849.72 53.40 o -1 3 1 1436.47 1429.63 18.63 o 1 3 1 72.00 79.23 3.23 o 3 3 1 678.63 623.33 10.97 o 5 3 1 1983.52 1973.18 28.39 o 7 3 1 1459.33 1363.94 24.39 o 9 3 1 815.16 798.36 19.53 o 11 3 1 504.16 480.66 16.01 o 13 3 1 1019.95 1027.45 21.80 o 15 3 1 62.95 80.78 9.63 o 17 3 1 85.20 96.54 8.87 o 19 3 1 40.54 41.34 7.74 o -20 4 1 99.76 114.89 15.62 o -18 4 1 101.69 99.68 14.46 o -16 4 1 648.50 610.57 21.18 o -14 4 1 338.65 313.83 14.35 o -12 4 1 463.89 388.57 14.81 o -10 4 1 296.77 259.20 12.16 o -8 4 1 2475.93 2626.36 29.44 o -6 4 1 2381.17 2572.66 40.93 o -4 4 1 468.26 449.24 9.74 o -2 4 1 440.72 470.63 11.60 o 0 4 1 361.45 348.38 8.20 o 2 4 1 1897.65 1985.82 19.36 o 4 4 1 2166.82 2260.40 25.62 o 6 4 1 3154.57 3257.49 42.19 o 8 4 1 2126.29 2042.89 41.49 o 10 4 1 1481.42 1400.61 28.48 o 12 4 1 952.75 916.62 24.13 o 14 4 1 261.12 247.43 17.12 o 16 4 1 109.97 112.41 9.42 o 18 4 1 126.31 152.94 11.38 o -19 5 1 137.72 138.77 18.08 o -17 5 1 230.74 265.39 18.12 o -15 5 1 347.30 339.33 19.61 o -13 5 1 64.05 55.08 10.75 o -11 5 1 835.52 803.01 21.14 o -9 5 1 669.48 687.54 17.68 o -7 5 1 1047.61 1062.38 17.36 o -5 5 1 276.25 304.19 8.09 o -3 5 1 350.41 365.71 11.50 o -1 5 1 590.20 682.47 13.12 o 1 5 1 375.39 356.88 9.11 o 3 5 1 3119.01 3327.09 29.18 o 5 5 1 2233.11 2137.76 26.55 o 7 5 1 1687.15 1614.67 29.63 o 9 5 1 2431.31 2401.13 39.44 o 11 5 1 1926.22 1854.47 35.79 o 13 5 1 272.46 265.05 13.64 o 15 5 1 95.42 89.79 11.02 o 17 5 1 27.78 39.04 6.68 o -18 6 1 56.59 51.50 9.81 o -16 6 1 28.91 40.52 7.92 o -14 6 1 270.52 279.13 18.06 o -12 6 1 74.72 74.60 19.34 o -10 6 1 14.41 7.66 5.83 o -8 6 1 572.39 549.49 18.91 o -6 6 1 1108.79 1154.92 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