Crystal Structure Communications

 

Acta Cryst. (2008). C64, i69-i70  [ doi:10.1107/S0108270108020398 ]

Tl₂CO₃ at 3.56 GPa

A. Grzechnik and K. Friese

Synopsis: The structure of Tl₂CO₃ (C2/m, Z = 4) was investigated at 3.56 GPa. No pressure-induced phase transition was observed.

Formula: Tl₂CO₃

Online 12 July 2008

 

Acta Cryst. (2008). C64, i71-i72  [ doi:10.1107/S0108270108021045 ]

A new bismuth iron oxyphosphate, Bi₆(Bi_0.32Fe_0.68)(PO₄)₄O₄

N. Arumugam, V. Lynch and H. Steinfink

Synopsis: Fe substitution in Bi₆(Bi_0.32Fe_0.68)(PO₄)₄O₄ occurs in the Bi-deficient site. The Fe/Bi atoms are disordered around the center of symmetry.

Formula: Bi₆(Bi_0.32Fe_0.68)(PO₄)₄O₄

Online 12 July 2008

 

Acta Cryst. (2008). C64, i73-i75  [ doi:10.1107/S0108270108022476 ]

Li₁₂Cu_16+xAl_26-x (x = 3.2): a new intermetallic structure type

V. Pavlyuk, G. Dmytriv, I. Tarasiuk, H. Pauly and H. Ehrenberg

Synopsis: Li₁₂Cu_16+xAl_26-x (x = 3.2) is a new intermetallic structure type that is related to the CaCu₅, LiCuAl₂ and Li₈Cu_12+xAl_6-x structures because of the presence of hexagonal channels and pseudo-Frank-Kasper polyhedra packing.

Formula: Li₁₂Cu_19.21Al_22.84

Online 26 July 2008

 

Acta Cryst. (2008). C64, i76-i78  [ doi:10.1107/S0108270108020386 ]

Partial Cu occupancy in uranium copper diantimonide, UCu_0.60(4)Sb₂

E. Ringe and J. A. Ibers

Synopsis: UCu_0.60(4)Sb₂ crystallizes in the tetragonal space group P4/nmm. From this and previous studies of UCu_xSb₂, it is found that the a axis is invariant to x but that a linear relation holds between x and the length of the c axis for x between 0 and 1.

Formula: UCu_0.60(4)Sb₂ at 100 and 120 K

Online 26 July 2008

 

Acta Cryst. (2008). C64, m271-m273  [ doi:10.1107/S0108270108018441 ]

A novel one-dimensional zinc coordination polymer containing 4-methylbenzoate and 4,4-bipyridine

D.-Y. Ma and G.-H. Deng

Formula: [Zn₂(C₈H₇O₂)₄(C₁₀H₈N₂)]

Online 5 July 2008

 

Acta Cryst. (2008). C64, m274-m276  [ doi:10.1107/S0108270108019239 ]

[(8a,9,9a-)-9-(⁵-Cyclopentadienyl)-9-nickelafluorenyl](⁵-pentamethylcyclopentadienyl)nickel(II)

P. Buchalski, A. Koziol and K. Suwinska

Formula: [Ni₂(C₅H₅)(C₁₀H₁₅)(C₁₂H₈)]

Online 5 July 2008

 

Acta Cryst. (2008). C64, m277-m279  [ doi:10.1107/S0108270108018039 ]

An interpenetrating primitive cubic net formed by hydrogen bonds and coordination bonds in catena-poly[[bis(methanol-O)bis(thiocyanato-N)iron(II)]--1,2-bis(4-pyridylmethylene)hydrazine-²N:N']

L. Öhrström, V. Langer and M. Ghazzali

Formula: [Fe(NCS)₂(C₁₂H₁₀N₄)(CH₄O)₂]

Online 5 July 2008

 

Acta Cryst. (2008). C64, m280-m282  [ doi:10.1107/S0108270108018404 ]

A novel tetranuclear copper(I) sulfanide complex with bis(diphenylphosphino)amine

W.-N. Zhao, L. Han and C.-C. Luo

Formula: [Cu₄(SH)₄(C₂₄H₂₁NP₂)₂]·2CH₄O

Online 5 July 2008

 

Acta Cryst. (2008). C64, m283-m285  [ doi:10.1107/S0108270108017630 ]

A novel three-dimensional heterometallic coordination polymer: poly[[hexaaquabis[₃-3,5-dicarboxylatopyrazolato-⁵O³,N²:N¹,O⁵:O^5'](₂-oxalato-⁴O¹,O²:O^1',O^2')copper(II)dierbium(III)] trihydrate]

Y. Wang and Y.-Z. Shen

Formula: [CuEr₂(C₅HN₂O₄)₂(C₂O₄)(H₂O)₆]·3H₂O

Online 12 July 2008

 

Acta Cryst. (2008). C64, m286-m291  [ doi:10.1107/S010827010801648X ]

Three-dimensional frameworks built from piperazine-2,5-dione and simple metal salts (M = Co, Ni, Cu and Ag)

T. R. Sarangarajan, B. S. Krishnamoorthy, K. Panchanatheswaran, J. N. Low and C. Glidewell

Formula: [CoCl₂(H₂O)₄]·C₄H₆N₂O₂, [NiCl₂(H₂O)₄]·C₄H₆N₂O₂, [CuCl₂(H₂O)₂]·C₄H₆N₂O₂ and [Ag(NO₃)(C₄H₆N₂O₂)]

Online 12 July 2008

 

Acta Cryst. (2008). C64, m292-m295  [ doi:10.1107/S0108270108019975 ]

Tetrakis(-anthracene-9-carboxylato)-⁴O:O';³O,O':O';³O:O,O'-bis[(anthracene-9-carboxylato-²O,O')(1,10-phenanthroline-²N,N')erbium(III)]: effects of a noncoordinating anthracene ligand ring system on the final structure of a coordination complex

C.-S. Liu, L.-Q. Guo, L.-F. Yan and J.-J. Wang

Formula: [Er₂(C₁₅H₉O₂)₆(C₁₂H₈N₂)₂]

Online 12 July 2008

 

Acta Cryst. (2008). C64, m296-m299  [ doi:10.1107/S0108270108022415 ]

Was Bijvoet right? Sodium rubidium (+)-tartrate tetrahydrate revisited

M. Lutz and A. M. M. Schreurs

Formula: Na⁺·Rb⁺·C₄H₄O₆^2-·4H₂O

Online 26 July 2008

 

Acta Cryst. (2008). C64, m300-m304  [ doi:10.1107/S0108270108022427 ]

Rock salt-urea-water (1/1/1) at 293 and 117 K

S. Müller, O. Schäfer and E. Keller

Formula: NaCl·CH₄N₂O·H₂O

Online 26 July 2008

 

Acta Cryst. (2008). C64, o411-o413  [ doi:10.1107/S0108270108017940 ]

Thioacetanilide at 120 K

A. Michta, E. Chelmecka, M. Nowak and J. Kusz

Formula: C₈H₉NS

Online 5 July 2008

 

Acta Cryst. (2008). C64, o414-o416  [ doi:10.1107/S0108270108019707 ]

Two derivatives of 1,5-disubstituted tetrazoles: 1-(4-nitrophenyl)-1H-tetrazol-5-amine and {(E)-[1-(4-ethoxyphenyl)-1H-tetrazol-5-yl]iminomethyl}dimethylamine

A. S. Lyakhov, A. N. Vorobiov, L. S. Ivashkevich and P. N. Gaponik

Formula: C₇H₆N₆O₂ and C₁₂H₁₆N₆O

Online 5 July 2008

 

Acta Cryst. (2008). C64, o417-o419  [ doi:10.1107/S0108270108019835 ]

7-Deaza-2'-deoxyinosine: a nucleoside showing ambiguous base-pairing properties against the four canonical DNA constituents

F. Seela, X. Ming, H. Eickmeier and H. Reuter

Formula: C₁₁H₁₃N₃O₄

Online 12 July 2008

 

Acta Cryst. (2008). C64, o420-o422  [ doi:10.1107/S0108270108020003 ]

Strong overcrowding in dimethyl 2-(dimethylamino)terephthalate

R. Centore, S. Fusco, A. Peluso, M. Carotenuto and A. Tuzi

Formula: C₁₂H₁₅NO₄

Online 12 July 2008

 

Acta Cryst. (2008). C64, o423-o425  [ doi:10.1107/S010827010801857X ]

5,7-syn-Bis(trimethylsilyl)-5-norbornene-2,3-endo-dicarboxylic acid: a rare co-existence of dimeric and catemeric synthons

N. S. Begum, D. E. Vasundhara, C. R. Girija and G. Nagendrappa

Formula: C₁₅H₂₆O₄Si₂

Online 12 July 2008

 

Acta Cryst. (2008). C64, o426-o427  [ doi:10.1107/S0108270108019033 ]

N-[(2-Phenyl-2H-1,2,3-triazol-4-yl)methylene]-2-(2-(2-phenyl-2H-1,2,3-triazol-4-yl)-3-{2-[(2-phenyl-2H-1,2,3-triazol-4-yl)methyleneamino]ethyl}imidazolidin-1-yl)ethanamine

Y. Feng, G. Liu, F. Yue and J.-D. Wang

Formula: C₃₃H₃₃N₁₃

Online 12 July 2008

 

Acta Cryst. (2008). C64, o428-o430  [ doi:10.1107/S0108270108020313 ]

The three-dimensional hydrogen-bonded framework structure in the 1:1 proton-transfer compound of the drug quinacrine with 5-sulfosalicylic acid

G. Smith and U. D. Wermuth

Formula: C₂₃H₃₂ClN₃O²⁺·C₇H₄O₆S^2-·2H₂O

Online 12 July 2008

 

Acta Cryst. (2008). C64, o431-o433  [ doi:10.1107/S010827010802057X ]

(S,S)-4''-Cyano-7,7''-dimethoxy-3',6'-dioxodispiro[indane-2,2'-piperazine-5',2''-indane]-4-carboxamide methanol solvate: interrupting the amide-to-amide hydrogen-bonded tape

B. Jagadish, M. D. Carducci, A. Dawson, G. S. Nichol and E. A. Mash

Formula: C₂₄H₂₂N₄O₅·CH₄O

Online 12 July 2008

 

Acta Cryst. (2008). C64, o434-o436  [ doi:10.1107/S0108270108018003 ]

N-Benzyloxy-1H-benzotriazole-1-carboxamide: a hydrogen-bonded tetramer based upon a rare R₄⁴(20) structural motif

I. Đilovic, D. Matkovic-Calogovic, I. Kos and M. Birus

Formula: C₁₄H₁₂N₄O₂

Online 12 July 2008

 

Acta Cryst. (2008). C64, o437-o440  [ doi:10.1107/S0108270108021380 ]

rac-3-Benzoyl-2-methylpropionic acid and its organic salts: possibilities of Yang photocyclization in crystals

J. Bakowicz and I. Turowska-Tyrk

Formula: C₁₁H₁₂O₃, C₄H₁₀NO⁺·C₁₁H₁₁O₃^-·H₂O, C₅H₆N⁺·(H⁺·2C₁₁H₁₁O₃^-) and C₄H₁₀N⁺·C₁₁H₁₁O₃^-·C₁₁H₁₂O₃

Online 19 July 2008

 

Acta Cryst. (2008). C64, o441-o444  [ doi:10.1107/S0108270108020374 ]

Nitrated isomers of 2-(trichloromethyl)quinoline

J. Sopková-de Oliveira Santos, P. Verhaeghe, J.-F. Lohier, P. Rathelot, P. Vanelle and S. Rault

Formula: Three isomers of C₁₀H₅Cl₃N₂O₂

Online 19 July 2008

 

Acta Cryst. (2008). C64, o445-o446  [ doi:10.1107/S0108270108020702 ]

2,3,4,6-Tetra-O-acetyl--D-glucopyranosyl azide

S. Dedola, S. A. Nepogodiev, D. L. Hughes and R. A. Field

Formula: C₁₄H₁₉N₃O₉

Online 19 July 2008

 

Acta Cryst. (2008). C64, o447-o449  [ doi:10.1107/S010827010802012X ]

Cyclotridecanone 2,4-dinitrophenylhydrazone

E. J. Valente, D. M. Pawar, F. R. Fronczek and E. A. Noe

Formula: C₁₉H₂₈N₄O₄

Online 19 July 2008

 

Acta Cryst. (2008). C64, o450-o452  [ doi:10.1107/S0108270108022129 ]

Partial ordering of tripivaloylmethane at 110 K

V. Stilinovic and B. Kaitner

Formula: C₁₆H₂₈O₃

Online 19 July 2008

 

Acta Cryst. (2008). C64, o453-o455  [ doi:10.1107/S0108270108020593 ]

9-Ethyl-1,4-dimethyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole and 6-bromo-9-ethyl-1,4-dimethyl-9H-carbazole

J. Sopková-de Oliveira Santos, A. Caruso, J.-F. Lohier, J.-C. Lancelot and S. Rault

Formula: C₂₂H₂₈BNO₂ and C₁₆H₁₆BrN

Online 19 July 2008

 

Acta Cryst. (2008). C64, o456-o458  [ doi:10.1107/S0108270108021392 ]

1-Ethyl 2,2-dimethyl 3-(1,3-benzodioxol-5-yl)propane-1,2,2-tricarboxylate

B. A. Hathaway, U. J. Kilgore and M. R. Bond

Formula: C₁₇H₂₀O₈ and C₁₇H₂₀O₈

Online 19 July 2008

 

Acta Cryst. (2008). C64, o459-o462  [ doi:10.1107/S010827010802221X ]

Redetermination of trans--hydromuconic acid

B. Hachula, M. Jablonska, M. Nowak and J. Kusz

Formula: C₆H₈O₄

Online 26 July 2008

 

Acta Cryst. (2008). C64, o463-o466  [ doi:10.1107/S0108270108021355 ]

2-tert-Butylamino-4-chloro-6-ethylamino-1,3,5-triazine: a structure with Z' = 4 containing two different molecular conformations and two independent chains of hydrogen-bonded R₂²(8) rings

A. Quesada, M. A. Fontecha, M. V. López, J. N. Low and C. Glidewell

Formula: C₉H₁₆ClN₅

Online 26 July 2008

 

Acta Cryst. (2008). C64, o467-o470  [ doi:10.1107/S0108270108021628 ]

A locked derivative of 8-aza-7-deazaadenosine

A. Pasternak, R. Kierzek, Z. Gdaniec and M. Gdaniec

Formula: C₁₁H₁₃N₅O₄

Online 26 July 2008