# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' d R = New: P21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 213.54 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.7713 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 11.1240 _cell_length_b 15.7090 _cell_length_c 11.3370 _cell_angle_alpha 90.000 _cell_angle_beta 106.480 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18683.88 20572.67 615.55 o 3 0 0 5.99 32.71 9.17 o 4 0 0 903.42 731.87 37.04 o 5 0 0 235.10 244.52 17.90 o 6 0 0 2029.28 2061.40 82.80 o 7 0 0 278.72 248.61 14.38 o 8 0 0 3618.97 3644.88 84.32 o 9 0 0 549.52 597.21 37.40 o 10 0 0 196.49 174.59 20.89 o 11 0 0 462.09 602.67 70.85 o 12 0 0 121.39 117.67 30.57 o 13 0 0 330.42 330.41 128.64 o 2 1 0 4812.23 4665.43 87.22 o 3 1 0 6303.70 6699.48 76.08 o 4 1 0 820.21 845.48 17.68 o 5 1 0 7214.20 6799.88 106.96 o 6 1 0 1742.28 1742.37 35.54 o 7 1 0 2277.20 2199.68 53.49 o 8 1 0 2424.40 2554.80 60.61 o 9 1 0 935.75 1049.05 25.95 o 10 1 0 873.29 932.33 35.28 o 11 1 0 1183.59 1321.04 40.46 o 12 1 0 535.95 508.93 26.65 o 13 1 0 258.19 290.86 58.31 o 1 2 0 370.16 360.56 5.31 o 2 2 0 32700.98 31577.70 759.55 o 3 2 0 2.41 10.41 4.75 o 4 2 0 110.75 137.78 9.89 o 5 2 0 5405.72 5442.69 65.19 o 6 2 0 1470.64 1477.86 29.91 o 7 2 0 270.00 330.17 16.28 o 8 2 0 92.20 112.74 22.14 o 9 2 0 235.46 260.95 17.85 o 10 2 0 773.00 773.94 30.56 o 11 2 0 27.21 16.45 13.47 o 12 2 0 15.99 4.63 13.33 o 13 2 0 44.39 39.42 20.43 o 1 3 0 9432.62 9621.31 88.94 o 2 3 0 141.45 146.57 6.03 o 3 3 0 1279.00 1159.09 14.13 o 4 3 0 2879.48 2667.96 35.20 o 5 3 0 1246.66 1119.22 16.29 o 6 3 0 18.84 22.10 7.07 o 7 3 0 1611.44 1799.67 48.11 o 8 3 0 131.95 154.57 15.36 o 9 3 0 30.67 40.05 11.20 o 10 3 0 93.81 101.87 16.38 o 11 3 0 46.96 32.79 17.11 o 12 3 0 16.15 30.16 19.49 o 13 3 0 22.36 58.74 24.70 o 0 4 0 8848.14 9355.31 111.26 o 1 4 0 3.73 8.79 3.63 o 2 4 0 161.48 201.00 11.19 o 3 4 0 6805.29 6391.46 64.98 o 4 4 0 21088.53 21572.08 351.87 o 5 4 0 221.71 285.08 9.72 o 6 4 0 4472.87 4243.03 63.01 o 7 4 0 2364.31 2395.59 41.04 o 8 4 0 1019.95 1025.38 28.81 o 9 4 0 615.85 617.77 29.54 o 10 4 0 505.14 523.79 21.97 o 11 4 0 184.26 186.47 19.78 o 12 4 0 291.58 365.09 21.52 o 13 4 0 24.48 29.90 19.34 o 1 5 0 14458.08 14190.09 154.31 o 2 5 0 900.55 809.56 10.28 o 3 5 0 1981.80 2006.53 31.03 o 4 5 0 964.99 1068.81 18.90 o 5 5 0 1517.25 1536.91 24.44 o 6 5 0 634.82 652.25 13.94 o 7 5 0 302.03 375.19 45.82 o 8 5 0 1.01 4.73 12.63 o 9 5 0 533.88 529.50 21.91 o 10 5 0 13.02 2.30 12.77 o 11 5 0 4.45 -6.26 18.84 o 12 5 0 50.63 86.05 24.16 o 13 5 0 45.20 36.51 16.16 o 0 6 0 5268.12 5434.15 67.36 o 1 6 0 2171.42 2224.89 19.46 o 2 6 0 869.84 797.27 9.33 o 3 6 0 816.23 865.27 17.10 o 4 6 0 320.91 340.52 14.58 o 5 6 0 389.42 443.78 11.85 o 6 6 0 381.56 398.66 18.49 o 7 6 0 53.35 40.30 8.95 o 8 6 0 218.29 215.67 11.95 o 9 6 0 350.34 344.98 22.09 o 10 6 0 98.73 80.41 14.30 o 11 6 0 19.28 -8.87 18.46 o 12 6 0 1.02 10.01 20.22 o 13 6 0 0.00 -15.29 15.29 o 1 7 0 223.35 321.62 8.93 o 2 7 0 269.62 306.13 9.27 o 3 7 0 167.38 178.83 11.23 o 4 7 0 261.50 269.18 10.17 o 5 7 0 797.77 758.55 14.86 o 6 7 0 264.67 297.86 20.11 o 7 7 0 908.49 855.79 22.50 o 8 7 0 380.59 352.23 12.95 o 9 7 0 275.77 298.85 17.27 o 10 7 0 677.18 602.06 42.02 o 11 7 0 93.64 99.81 18.72 o 12 7 0 24.80 20.94 15.39 o 0 8 0 3177.79 2955.20 48.93 o 1 8 0 1410.83 1437.06 17.16 o 2 8 0 5527.55 5314.26 52.60 o 3 8 0 69.20 98.29 7.04 o 4 8 0 1284.25 1227.81 16.06 o 5 8 0 179.68 172.00 13.14 o 6 8 0 278.02 295.29 14.33 o 7 8 0 82.53 75.94 8.89 o 8 8 0 129.57 151.42 10.18 o 9 8 0 179.55 183.70 24.18 o 10 8 0 568.37 530.16 22.37 o 11 8 0 4.09 22.14 19.66 o 12 8 0 28.19 60.23 40.52 o 1 9 0 698.20 631.18 14.34 o 2 9 0 383.04 380.20 10.31 o 3 9 0 360.02 354.81 10.33 o 4 9 0 13.56 20.32 6.99 o 5 9 0 1675.61 1640.46 27.66 o 6 9 0 128.58 94.53 20.41 o 7 9 0 116.63 89.57 11.61 o 8 9 0 244.06 213.66 11.99 o 9 9 0 28.19 30.47 13.68 o 10 9 0 1.92 6.99 14.72 o 11 9 0 15.32 11.09 26.52 o 12 9 0 5.72 6.51 56.22 o 0 10 0 1095.60 1096.89 32.86 o 1 10 0 935.87 918.89 21.13 o 2 10 0 568.10 628.81 19.88 o 3 10 0 8.07 17.92 8.17 o 4 10 0 1056.36 1043.85 26.93 o 5 10 0 14.74 11.60 5.41 o 6 10 0 88.70 80.03 9.42 o 7 10 0 3.95 2.41 7.23 o 8 10 0 15.76 13.43 8.86 o 9 10 0 246.26 155.41 15.64 o 10 10 0 20.50 30.46 18.49 o 11 10 0 1.51 -19.95 33.40 o 12 10 0 18.41 28.62 41.96 o 1 11 0 1476.52 1617.84 23.26 o 2 11 0 302.88 324.79 15.38 o 3 11 0 337.11 327.96 12.92 o 4 11 0 968.55 954.74 30.44 o 5 11 0 408.58 410.55 27.85 o 6 11 0 1558.20 1487.98 48.51 o 7 11 0 124.14 127.14 19.90 o 8 11 0 179.31 108.80 24.50 o 9 11 0 251.31 246.32 53.42 o 10 11 0 55.31 92.74 30.65 o 11 11 0 160.74 156.72 51.03 o 0 12 0 2777.18 2809.37 54.27 o 1 12 0 22.12 21.27 7.70 o 2 12 0 3640.05 3516.54 47.53 o 3 12 0 651.52 759.96 23.13 o 4 12 0 532.94 555.37 12.98 o 5 12 0 1.33 3.07 6.32 o 6 12 0 4722.45 4760.26 118.61 o 7 12 0 72.19 53.16 10.23 o 8 12 0 144.35 135.94 26.47 o 9 12 0 150.56 163.81 29.02 o 10 12 0 44.64 20.81 24.47 o 11 12 0 51.84 58.66 35.42 o 1 13 0 1024.87 1071.67 30.25 o 2 13 0 433.98 443.05 13.00 o 3 13 0 298.55 354.39 13.56 o 4 13 0 73.08 76.36 10.34 o 5 13 0 459.03 403.82 25.18 o 6 13 0 89.29 103.33 20.36 o 7 13 0 795.39 742.66 48.45 o 8 13 0 238.73 234.46 30.53 o 9 13 0 184.57 149.14 31.19 o 10 13 0 37.70 24.01 22.71 o 0 14 0 406.83 383.40 30.45 o 1 14 0 23.51 20.17 10.94 o 2 14 0 63.78 45.51 13.94 o 3 14 0 24.20 9.45 8.08 o 4 14 0 1181.92 1157.32 29.59 o 5 14 0 80.68 73.78 13.42 o 6 14 0 73.86 88.74 17.38 o 7 14 0 0.27 39.56 24.88 o 8 14 0 14.72 4.21 18.76 o 9 14 0 2.08 18.05 25.15 o 10 14 0 7.34 -0.15 40.63 o 1 15 0 1143.40 1252.83 31.32 o 2 15 0 36.12 35.61 13.42 o 3 15 0 185.52 173.67 14.90 o 4 15 0 231.70 209.08 24.60 o 5 15 0 151.42 118.14 22.04 o 6 15 0 71.37 88.62 29.74 o 7 15 0 27.33 61.72 26.63 o 8 15 0 38.26 57.74 30.52 o 9 15 0 1.38 -18.52 28.08 o 0 16 0 639.51 605.15 35.46 o 1 16 0 322.36 286.47 21.45 o 2 16 0 195.71 150.18 19.69 o 3 16 0 131.48 110.27 17.38 o 4 16 0 120.80 138.17 16.57 o 5 16 0 342.71 523.96 68.59 o 6 16 0 132.84 159.37 24.73 o 7 16 0 30.31 45.32 23.35 o 8 16 0 95.34 105.07 33.30 o 1 17 0 814.06 944.96 31.47 o 2 17 0 113.13 84.31 13.59 o 3 17 0 943.55 862.93 67.49 o 4 17 0 57.43 84.70 23.88 o 5 17 0 172.96 141.16 26.83 o 6 17 0 31.14 33.45 26.82 o 7 17 0 60.38 63.25 27.95 o 0 18 0 69.24 42.42 32.11 o 1 18 0 0.54 -9.60 21.09 o 2 18 0 27.46 48.45 17.65 o 3 18 0 309.43 315.99 35.32 o 4 18 0 4.90 45.91 51.08 o 5 18 0 99.08 99.26 36.65 o 6 18 0 1.94 39.21 26.19 o 1 19 0 42.69 42.90 15.39 o 2 19 0 40.37 50.20 23.96 o 3 19 0 0.27 13.24 52.35 o 4 19 0 234.36 201.62 43.75 o 0 20 0 253.00 196.40 46.94 o 1 20 0 22.91 23.03 30.43 o 2 20 0 159.44 267.55 49.72 o -14 1 1 224.65 292.83 40.18 o -13 1 1 55.52 53.52 25.75 o -12 1 1 173.39 131.47 16.94 o -11 1 1 918.65 907.02 22.57 o -10 1 1 361.67 399.58 28.29 o -9 1 1 342.04 380.04 14.36 o -8 1 1 2506.58 2519.29 39.71 o -7 1 1 304.61 283.46 12.38 o -6 1 1 3660.04 3679.03 39.98 o -5 1 1 448.40 388.57 16.65 o -4 1 1 631.08 629.32 12.69 o -3 1 1 299.82 229.34 8.66 o -2 1 1 24.80 35.57 5.46 o 1 1 1 1707.24 1794.99 14.47 o 2 1 1 2033.03 1710.83 18.75 o 3 1 1 2222.51 2006.31 34.62 o 4 1 1 264.78 249.62 13.27 o 5 1 1 280.73 284.79 13.39 o 6 1 1 2861.67 2928.22 102.68 o 7 1 1 631.47 766.64 35.64 o 8 1 1 2945.84 3091.78 132.97 o 9 1 1 3136.97 3177.57 146.94 o 10 1 1 220.98 237.49 17.06 o 11 1 1 102.27 96.57 17.90 o 12 1 1 25.21 23.40 12.86 o 13 1 1 64.55 79.92 25.33 o -14 2 1 81.40 115.44 53.03 o -13 2 1 54.66 74.81 31.50 o -12 2 1 14.49 29.41 10.98 o -11 2 1 689.53 777.91 26.81 o -10 2 1 135.26 150.51 10.86 o -9 2 1 398.38 398.71 12.46 o -8 2 1 29.06 29.97 7.11 o -7 2 1 4748.75 4738.10 67.55 o -6 2 1 976.04 1004.09 21.42 o -5 2 1 10230.66 10230.54 158.14 o -4 2 1 79.49 61.87 5.72 o -3 2 1 36914.18 35948.11 661.51 o -2 2 1 1.90 13.46 2.99 o -1 2 1 10259.15 11169.15 112.06 o 0 2 1 1.98 12.87 3.28 o 1 2 1 28333.41 28574.73 492.78 o 2 2 1 685.37 565.00 14.74 o 3 2 1 4667.78 4600.82 49.41 o 4 2 1 5581.85 5219.54 64.22 o 5 2 1 807.36 686.39 15.33 o 6 2 1 385.97 399.45 22.53 o 7 2 1 2399.29 2449.45 59.27 o 8 2 1 1233.79 1281.59 49.11 o 9 2 1 162.64 168.18 16.53 o 10 2 1 441.33 430.35 50.66 o 11 2 1 9.89 1.72 12.55 o 12 2 1 260.22 233.12 22.25 o 13 2 1 66.24 110.50 26.50 o -13 3 1 145.05 142.31 32.49 o -12 3 1 321.00 319.32 21.14 o -11 3 1 50.99 70.45 12.90 o -10 3 1 968.62 990.76 21.11 o -9 3 1 289.05 314.32 13.94 o -8 3 1 582.54 570.33 20.05 o -7 3 1 303.10 352.54 13.82 o -6 3 1 85.55 68.06 11.87 o -5 3 1 4648.32 4567.72 54.04 o -4 3 1 9238.33 9620.30 114.30 o -3 3 1 152.59 152.35 7.93 o -2 3 1 19099.79 19372.70 239.66 o -1 3 1 2058.33 2139.50 17.36 o 0 3 1 2190.20 2419.84 33.65 o 1 3 1 7613.73 7410.55 91.74 o 2 3 1 3090.67 2900.62 46.63 o 3 3 1 1142.92 1235.85 13.63 o 4 3 1 1689.05 1755.47 34.46 o 5 3 1 3360.55 3688.68 53.11 o 6 3 1 3885.43 3799.15 54.09 o 7 3 1 1188.87 1247.88 24.70 o 8 3 1 319.10 302.30 53.59 o 9 3 1 439.60 447.77 21.29 o 10 3 1 530.56 571.74 35.35 o 11 3 1 198.30 154.35 17.30 o 12 3 1 107.95 88.13 18.40 o 13 3 1 16.07 28.55 19.98 o -13 4 1 1.83 -24.69 25.28 o -12 4 1 1.18 20.53 13.35 o -11 4 1 22.19 28.83 12.35 o -10 4 1 90.91 94.55 9.95 o -9 4 1 4.70 1.56 8.95 o -8 4 1 168.21 183.06 11.97 o -7 4 1 99.06 112.20 12.55 o -6 4 1 199.58 246.98 32.94 o -5 4 1 3516.07 3840.53 57.45 o -4 4 1 2700.99 2579.99 30.16 o -3 4 1 11938.02 12122.53 132.08 o -2 4 1 144.63 162.25 9.37 o -1 4 1 2045.84 1793.57 15.00 o 0 4 1 2282.54 2248.28 23.39 o 1 4 1 61.24 89.26 5.10 o 2 4 1 1340.09 1369.42 28.68 o 3 4 1 471.63 449.76 10.56 o 4 4 1 706.20 694.99 19.88 o 5 4 1 635.95 646.11 14.70 o 6 4 1 99.43 109.76 9.79 o 7 4 1 519.35 569.04 15.30 o 8 4 1 10.33 4.87 9.92 o 9 4 1 210.96 180.76 32.06 o 10 4 1 210.15 154.77 19.46 o 11 4 1 2.82 8.42 12.56 o 12 4 1 9.17 11.71 13.86 o 13 4 1 130.09 152.64 31.39 o -13 5 1 22.54 8.07 17.55 o -12 5 1 68.51 81.50 24.66 o -11 5 1 6.77 13.77 13.84 o -10 5 1 80.11 103.30 13.87 o -9 5 1 5.22 8.73 10.06 o -8 5 1 491.78 537.39 19.99 o -7 5 1 44.78 46.53 11.26 o -6 5 1 215.32 182.74 22.79 o -5 5 1 126.18 132.95 6.58 o -4 5 1 9256.54 8773.21 103.17 o -3 5 1 861.67 852.95 11.83 o -2 5 1 82.54 108.80 6.21 o -1 5 1 1192.61 1210.46 20.17 o 0 5 1 2007.09 1887.15 18.79 o 1 5 1 1301.50 1363.78 18.38 o 2 5 1 2870.56 2528.35 29.38 o 3 5 1 964.55 1027.86 12.23 o 4 5 1 1310.48 1228.32 15.12 o 5 5 1 300.42 372.20 8.99 o 6 5 1 4.27 3.43 7.87 o 7 5 1 33.07 38.66 8.16 o 8 5 1 12.19 -0.14 9.77 o 9 5 1 2.46 7.55 14.22 o 10 5 1 21.16 16.37 13.89 o 11 5 1 218.74 197.48 19.62 o 12 5 1 9.36 29.85 21.29 o 13 5 1 65.75 50.38 30.08 o -13 6 1 33.49 27.45 19.17 o -12 6 1 120.50 76.60 27.33 o -11 6 1 170.74 199.81 26.78 o -10 6 1 195.43 160.49 17.55 o -9 6 1 1420.79 1461.85 36.23 o -8 6 1 238.58 289.55 22.33 o -7 6 1 1149.64 1168.60 30.96 o -6 6 1 1124.80 1099.77 27.06 o -5 6 1 40.85 35.18 8.20 o -4 6 1 12.56 20.58 4.67 o -3 6 1 601.47 631.94 12.89 o -2 6 1 793.42 845.42 12.65 o -1 6 1 2841.87 2817.09 26.29 o 0 6 1 672.63 721.79 8.98 o 1 6 1 6225.88 6531.27 63.72 o 2 6 1 4089.19 3957.34 33.84 o 3 6 1 7041.38 7163.55 77.72 o 4 6 1 2281.23 2121.57 19.99 o 5 6 1 3340.29 3278.62 49.50 o 6 6 1 398.09 376.08 19.80 o 7 6 1 362.72 413.79 13.32 o 8 6 1 147.66 171.62 14.19 o 9 6 1 703.94 733.17 25.77 o 10 6 1 193.69 163.70 14.33 o 11 6 1 112.10 108.54 22.04 o 12 6 1 29.43 12.30 18.62 o -13 7 1 0.34 -4.82 20.16 o -12 7 1 14.32 39.42 19.60 o -11 7 1 0.33 -13.68 13.68 o -10 7 1 429.28 394.22 26.94 o -9 7 1 149.68 124.20 23.85 o -8 7 1 95.77 83.20 28.09 o -7 7 1 234.21 185.99 15.85 o -6 7 1 3257.57 3056.83 55.75 o -5 7 1 1105.78 1166.95 18.52 o -4 7 1 2948.92 2623.34 29.04 o -3 7 1 0.69 1.98 6.81 o -2 7 1 9292.33 8760.06 102.19 o -1 7 1 401.81 446.67 16.78 o 0 7 1 1353.53 1174.68 14.31 o 1 7 1 743.52 718.74 14.52 o 2 7 1 10179.07 10226.18 122.45 o 3 7 1 0.65 2.82 7.06 o 4 7 1 285.20 254.03 23.47 o 5 7 1 73.77 81.62 11.59 o 6 7 1 24.82 24.27 7.89 o 7 7 1 248.54 240.25 9.86 o 8 7 1 60.84 46.54 10.23 o 9 7 1 145.98 169.86 18.20 o 10 7 1 3.58 -5.86 16.31 o 11 7 1 59.12 37.56 15.45 o 12 7 1 19.82 45.18 49.21 o -12 8 1 1.06 9.32 14.24 o -11 8 1 120.48 91.97 14.43 o -10 8 1 240.10 219.42 18.00 o -9 8 1 67.44 12.03 13.22 o -8 8 1 212.47 215.50 12.44 o -7 8 1 25.59 21.32 11.63 o -6 8 1 182.96 150.63 12.70 o -5 8 1 730.62 765.60 21.13 o -4 8 1 38.32 41.90 6.80 o -3 8 1 2090.76 2090.36 24.69 o -2 8 1 74.18 63.31 6.87 o -1 8 1 5678.87 6030.24 62.72 o 0 8 1 2964.88 2940.47 29.70 o 1 8 1 62.60 95.09 9.12 o 2 8 1 824.83 812.83 11.20 o 3 8 1 0.99 9.70 3.37 o 4 8 1 331.23 310.35 24.26 o 5 8 1 265.87 282.71 18.04 o 6 8 1 180.34 186.24 9.27 o 7 8 1 136.18 112.05 18.51 o 8 8 1 111.04 57.90 11.47 o 9 8 1 109.80 76.19 11.39 o 10 8 1 1.42 20.60 14.16 o 11 8 1 141.56 104.51 51.34 o 12 8 1 1.60 29.95 30.57 o -12 9 1 48.53 23.55 28.09 o -11 9 1 250.23 183.70 19.81 o -10 9 1 639.50 541.02 26.26 o -9 9 1 404.71 380.08 21.03 o -8 9 1 106.11 115.25 12.43 o -7 9 1 1650.19 1652.42 28.83 o -6 9 1 164.23 193.82 13.28 o -5 9 1 90.14 110.46 8.91 o -4 9 1 62.41 92.80 7.08 o -3 9 1 148.15 141.36 9.57 o -2 9 1 6.58 22.00 6.22 o -1 9 1 2146.45 2049.02 25.61 o 0 9 1 4.50 4.72 8.76 o 1 9 1 115.45 104.24 8.02 o 2 9 1 1908.40 1932.36 21.67 o 3 9 1 1622.55 1501.15 15.83 o 4 9 1 2128.86 2146.42 49.02 o 5 9 1 1113.65 1147.78 34.64 o 6 9 1 433.01 460.78 27.81 o 7 9 1 607.47 585.09 60.85 o 8 9 1 1326.45 1255.56 80.75 o 9 9 1 154.69 90.63 10.35 o 10 9 1 195.26 170.96 34.10 o 11 9 1 50.40 25.58 36.45 o 12 9 1 108.03 66.74 40.54 o -12 10 1 40.98 64.35 33.09 o -11 10 1 96.64 71.09 30.48 o -10 10 1 77.47 61.70 14.11 o -9 10 1 722.67 599.28 34.33 o -8 10 1 57.44 67.40 11.94 o -7 10 1 264.21 264.62 18.77 o -6 10 1 904.88 899.33 19.28 o -5 10 1 7944.75 8102.83 110.18 o -4 10 1 22.25 18.77 6.36 o -3 10 1 9853.48 9837.19 117.47 o -2 10 1 4.35 0.94 6.98 o -1 10 1 2533.29 2160.15 59.42 o 0 10 1 1080.26 1180.09 17.39 o 1 10 1 2243.55 2162.37 29.44 o 2 10 1 31.56 16.01 5.08 o 3 10 1 4233.53 4046.32 42.15 o 4 10 1 688.22 661.34 27.45 o 5 10 1 851.91 811.08 34.70 o 6 10 1 66.93 51.05 18.12 o 7 10 1 135.67 144.15 26.70 o 8 10 1 237.21 198.68 20.11 o 9 10 1 78.30 67.68 32.45 o 10 10 1 290.58 274.35 48.96 o 11 10 1 1.22 7.81 48.14 o -11 11 1 39.14 13.13 36.74 o -10 11 1 73.25 78.07 26.91 o -9 11 1 289.32 233.65 28.68 o -8 11 1 352.65 336.10 39.05 o -7 11 1 581.15 590.17 31.37 o -6 11 1 69.10 59.33 9.36 o -5 11 1 2046.31 2046.70 37.37 o -4 11 1 4.73 -0.61 7.99 o -3 11 1 137.66 140.53 14.48 o -2 11 1 27.13 35.79 13.03 o -1 11 1 110.17 139.51 16.47 o 0 11 1 1080.21 1005.42 28.09 o 1 11 1 426.55 440.38 29.08 o 2 11 1 1407.51 1371.30 19.60 o 3 11 1 1758.33 1621.66 22.96 o 4 11 1 426.00 491.65 25.10 o 5 11 1 893.91 929.45 30.43 o 6 11 1 1005.20 1088.31 39.09 o 7 11 1 362.77 372.05 78.16 o 8 11 1 327.79 294.69 43.18 o 9 11 1 64.30 49.66 49.39 o 10 11 1 172.51 116.77 59.78 o 11 11 1 1.42 24.70 32.89 o -11 12 1 30.14 32.33 37.12 o -10 12 1 20.40 27.52 29.19 o -9 12 1 23.41 32.87 25.64 o -8 12 1 27.97 45.73 15.39 o -7 12 1 534.63 504.53 30.98 o -6 12 1 0.06 -8.15 8.15 o -5 12 1 0.60 7.11 9.41 o -4 12 1 7.09 10.33 8.55 o -3 12 1 67.14 61.69 10.09 o -2 12 1 169.28 157.27 12.56 o -1 12 1 580.88 556.36 17.02 o 0 12 1 176.26 172.21 13.18 o 1 12 1 309.79 368.92 14.38 o 2 12 1 712.12 740.15 17.17 o 3 12 1 316.60 334.43 14.86 o 4 12 1 11.44 36.09 14.23 o 5 12 1 39.80 60.78 15.67 o 6 12 1 15.95 5.50 14.45 o 7 12 1 108.27 93.32 18.26 o 8 12 1 28.38 1.30 15.59 o 9 12 1 27.28 37.30 21.10 o 10 12 1 18.17 7.18 23.02 o -10 13 1 3.07 37.44 32.34 o -9 13 1 18.85 16.61 22.92 o -8 13 1 70.82 92.16 24.07 o -7 13 1 59.20 59.18 11.44 o -6 13 1 270.80 216.03 13.61 o -5 13 1 54.63 51.86 11.00 o -4 13 1 1449.69 1484.60 31.27 o -3 13 1 0.24 -12.74 14.13 o -2 13 1 1796.85 1828.69 33.10 o -1 13 1 42.12 52.78 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