Acta Crystallographica Section C

Crystal Structure Communications

Volume 65, Part 2 (February 2009)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: Displacement ellipsoid plots for bis(acetato-[kappa]2O,O')diaquazinc(II) at 110 K (left) and 250 K (right). Ellipsoids are drawn at the 50% probability level and H atoms are shown as small spheres of arbitrary radii. See Lutz & Spek [Acta Cryst. (2009), C65, m69-m74].

metal-organic compounds


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Acta Cryst. (2009). C65, m45-m47  [ doi:10.1107/S0108270108043643 ]

A two-dimensional network formed by self-associating silver(I) perchlorate with 3-[4-(2-thienyl)-2H-cyclopenta[d]pyridazin-1-yl]benzonitrile

X.-Y. Li, Q.-K. Liu, J.-P. Ma, R.-Q. Huang and Y.-B. Dong

Formula: [Ag(C18H11N3S)]ClO4·CH4O

Online 10 January 2009


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Acta Cryst. (2009). C65, m48-m51  [ doi:10.1107/S0108270108043631 ]

Robust packing in cyclopalladated primary amines: isomorphous crystal structures of four complexes with varying substitution patterns

B. Calmuschi-Cula, I. Kalf, C. Timofte and U. Englert

Formula: [Pd(C8H10N)Cl(C5H5N)], [PdBr(C8H10N)(C5H5N)], [PdBr(C8H9BrN)(C6H7N)] and [Pd(C8H9BrN)I(C6H7N)]

Online 10 January 2009


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Acta Cryst. (2009). C65, m52-m55  [ doi:10.1107/S0108270108043783 ]

Luminescence properties of three structures built from 3-cyano-4-dicyanomethylene-5-oxo-4,5-dihydro-1H-pyrrol-2-olate and alkaline metals (Na, K and Rb)

V. A. Tafeenko, S. I. Gurskiy, A. N. Baranov, T. V. Kaisarova and L. A. Aslanov

Formula: Rb+·C8HN4O2- and Na+·C8HN4O2-·2H2O

Online 10 January 2009


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Acta Cryst. (2009). C65, m56-m58  [ doi:10.1107/S0108270108042637 ]

A three-dimensional homochiral metal-organic framework constructed from manganese(II) with S-carboxymethyl-N-(p-tosyl)-L-cysteine and 4,4'-bipyridine

W. Xiong, Y. Su, Z. Chen and F. Liang

Formula: [Mn(C12H13NO6S2)(C10H8N2)(H2O)]

Online 10 January 2009


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Acta Cryst. (2009). C65, m59-m61  [ doi:10.1107/S0108270108043400 ]

A novel three-dimensional copper(I) coordination polymer constructed from a copper-bromide net and nicotinic acid ligands

M.-H. Yang

Formula: [CuBr(C6H5NO2)]

Online 10 January 2009


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Acta Cryst. (2009). C65, m62-m65  [ doi:10.1107/S0108270109000353 ]

Square-grid coordination networks of diaquabis(4,4'-bipyridyl)copper(II) crosslinked by hydrogen bonds through two monoanions of 1-benzofuran-2,3-dicarboxylic acid and five molecules of water

R. Koner and I. Goldberg

Formula: [Cu(C10H8N2)2(H2O)2](C10H5O5)2·5H2O

Online 10 January 2009


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Acta Cryst. (2009). C65, m66-m68  [ doi:10.1107/S0108270109000341 ]

A novel two-dimensional framework based on unprecedented cadmium(II) chains

J. Qin, J.-P. Ma, L.-L. Liu, R.-Q. Huang and Y.-B. Dong

Formula: [Cd(C10H8N3O2)Cl(H2O)]

Online 10 January 2009


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Acta Cryst. (2009). C65, m69-m74  [ doi:10.1107/S0108270108043242 ]

Directed anisotropy in bis(acetato-[kappa]2O,O')diaquazinc(II) at 110 and 250 K

M. Lutz and A. L. Spek

Formula: [Zn(C2H3O2)2(H2O)2] at 110 and 250 K

Online 10 January 2009


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Acta Cryst. (2009). C65, m75-m77  [ doi:10.1107/S0108270109000092 ]

A three-dimensional AlIII/NaI metal-organic framework resulting from dimethylformamide hydrolysis

A. Plutecka and U. Rychlewska

Formula: (C2H8N)2[AlNa(HCO2)6]

Online 10 January 2009


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Acta Cryst. (2009). C65, m78-m81  [ doi:10.1107/S0108270108043667 ]

Two bicyclic dinuclear complexes generated from 3,3'-[1,3,4-thiadiazole-2,5-diyldi(thiomethylene)]dibenzoic acid (L) and dimethylformamide (DMF): [Cu(L)(DMF)]2 and [Zn(L)(DMF)]2

P. Wang, J.-P. Ma, X.-Y. Li, R.-Q. Huang and Y.-B. Dong

Formula: [Cu2(C18H12N2O4S3)2(C3H7NO)2] and [Zn2(C18H12N2O4S3)2(C3H7NO)2]

Online 14 January 2009


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Acta Cryst. (2009). C65, m82-m85  [ doi:10.1107/S0108270109000559 ]

A novel threefold-interpenetrating primitive cubic network based on a dinuclear Zn2 node

Y.-P. Diao, K. Li, S.-S. Huang, X.-H. Shu, K.-X. Liu and X.-M. Deng

Formula: [Zn2(C8H4O4)2(C12H10N4)]

Online 14 January 2009


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Acta Cryst. (2009). C65, m86-m90  [ doi:10.1107/S0108270109000869 ]

Influence of solvent on the structures of two one-dimensional cobalt(II) coordination polymers with tetrachloroterephthalate

Y.-Q. Fang, M. Lu and C.-X. Lu

Formula: [Co(C8Cl4O4)(C5H5N)3(H2O)]·C5H5N and [Co(C8Cl4O4)(C5H5N)2(H2O)2]·C4H8O2·3H2O

Online 14 January 2009


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Acta Cryst. (2009). C65, m91-m93  [ doi:10.1107/S0108270109000742 ]

An unprecedented three-dimensional silver(I) cluster built up from pyrazine-2,3-dicarboxylate ligands

J. Wu

Formula: [Ag3(C6H2N2O4)(C6H3N2O4)]

Online 14 January 2009


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Acta Cryst. (2009). C65, m94-m96  [ doi:10.1107/S0108270109001139 ]

A polymorph of tetrakis(acetonitrile-[kappa]N)copper(I) tetrafluoridoborate

J. W. Bats, T. Kretz and H.-W. Lerner

Formula: [Cu(C2H3N)4]BF4

Online 17 January 2009


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Acta Cryst. (2009). C65, m97-m99  [ doi:10.1107/S0108270109001917 ]

Bis[2-(2-hydroxyethyl)pyridinium] [mu]-decavanadato-bis[pentaaquamanganate(II)] tetrahydrate

L. Klistincová, E. Rakovský and P. Schwendt

Formula: (C7H10NO)2[Mn2V10O28(H2O)10]·4H2O

Online 24 January 2009


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Acta Cryst. (2009). C65, m100-m102  [ doi:10.1107/S010827010803521X ]

{[SmCl(en)4][In2Te4]}n: an indium telluride with a one-dimensional sinusoidal chain

C.-Y. Li, J. Zhou, Y. Zhang, G.-Q. Bian and J. Dai

Formula: [SmCl(C2H8N2)4][In2Te4]

Online 24 January 2009


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Acta Cryst. (2009). C65, m103-m106  [ doi:10.1107/S0108270109001590 ]

Poly[triaqua([mu]4-4-carboxybenzenesulfonato-[kappa]4O:O':O'':O''')(4-carboxybenzenesulfonato-[kappa]O)strontium(II)]

G. Prochniak and V. Videnova-Adrabinska

Formula: [Sr(C7H5O5S)2(H2O)3]

Online 24 January 2009


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Acta Cryst. (2009). C65, m107-m109  [ doi:10.1107/S0108270109002674 ]

Poly[[[[mu]-1,1'-(butane-1,4-diyl)diimidazole-[kappa]2N:N']([mu]-cyclohexane-1,4-dicarboxylato-[kappa]4O1,O1':O4,O4')cadmium(II)] hemihydrate]: a parallel interpenetrating two-dimensional (4,4) network

S. Zhou, B. Liu and C.-B. Li

Formula: [Cd(C8H10O4)(C10H14N4)]·0.5H2O

Online 28 January 2009


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Acta Cryst. (2009). C65, m110-m114  [ doi:10.1107/S0108270109002492 ]

trans-Chlorido(phenyl)bis(triphenylphosphine)nickel(II) and its 1:1 cocrystal with chloridobis(triphenylphosphine)nickel(I)

L. Li, C. S. B. Gomes, C. A. Figueira, P. T. Gomes and M. T. Duarte

Formula: [Ni(C6H5)Cl(C18H15P)2] and [Ni(C6H5)Cl(C18H15P)2]·[NiCl(C18H15P)2]

Online 28 January 2009


organic compounds


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Acta Cryst. (2009). C65, o31-o34  [ doi:10.1107/S0108270108042911 ]

A new polymorph of triphenylmethylamine: the effect of hydrogen bonding

V. N. Khrustalev, I. V. Borisova, N. N. Zemlyansky and M. Y. Antipin

Formula: C19H17N

Online 10 January 2009


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Acta Cryst. (2009). C65, o35-o38  [ doi:10.1107/S0108270108043655 ]

Tetrameric aggregate of 1,c-3-diphenyltetran-r-1-ol via an R44(8) homodromic ring

D. R. Vega, J. D. Mufato, J. M. Aguirre, E. V. Drago and B. Lantaño

Formula: C22H20O

Online 10 January 2009


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Acta Cryst. (2009). C65, o39-o41  [ doi:10.1107/S0108270108042431 ]

gem-Dimethylcyclopropanation of dibenzylideneacetone using triisopropyl sulfoxonium tetrafluoroborate

M. G. Edwards, D. S. Pugh, A. C. Whitwood and R. J. K. Taylor

Formula: C23H26O

Online 10 January 2009


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Acta Cryst. (2009). C65, o42-o45  [ doi:10.1107/S0108270108044223 ]

Hydrogen-bonded supramolecular motifs in 2-amino-4,6-dimethoxypyrimidinium picrate and pyrimethaminium picrate dimethyl sulfoxide solvate

K. Thanigaimani, A. Subashini, P. T. Muthiah, D. E. Lynch and R. J. Butcher

Formula: C6H10N3O2+·C6H2N3O7- and C12H14ClN4+·C6H2N3O7-·C2H6OS

Online 10 January 2009


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Acta Cryst. (2009). C65, o46-o50  [ doi:10.1107/S010827010804287X ]

Two enantiomerically pure cyclic arenesulfonamide hydrochloride salts

L. Kiefer, P. Dauban, R. H. Dodd and P. Retailleau

Formula: C20H21N2O2S+·Cl- and C26H25N2O2S+·Cl-

Online 10 January 2009


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Acta Cryst. (2009). C65, o51-o53  [ doi:10.1107/S010827010804300X ]

Three-dimensional networks in the 1:2 organic salts 2,2'-biimidazolium bis(3-carboxy-4-hydroxybenzenesulfonate) and 2,2'-bibenzimidazolium bis(3-carboxy-4-hydroxybenzenesulfonate) trihydrate

C.-S. Zhou, L.-L. Ding, H. Zhang, M.-N. Cao and X.-G. Meng

Formula: C6H8N42+·2C7H5O6S- and C14H12N42+·2C7H5O6S-·3H2O

Online 10 January 2009


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Acta Cryst. (2009). C65, o54-o57  [ doi:10.1107/S0108270109000225 ]

Two modes of O-H...O hydrogen bonding utilized in dimorphs of racemic 6-O-acryloyl-2-O-benzoyl-myo-inositol 1,3,5-orthoformate

S. Krishnaswamy, R. G. Gonnade, M. M. Bhadbhade and M. S. Shashidhar

Formula: Two forms of C17H16O8

Online 10 January 2009


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Acta Cryst. (2009). C65, o58-o61  [ doi:10.1107/S0108270108044132 ]

Salts of maleic and fumaric acids with oxine: the role of isomeric acids in hydrogen-bonding patterns

S. Franklin and T. Balasubramanian

Formula: C9H8NO+·C4H3O4- and C9H8NO+·C4H3O4-

Online 14 January 2009


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Acta Cryst. (2009). C65, o62-o65  [ doi:10.1107/S0108270109000237 ]

Bis[2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidin-1-ium] DL-malate

S. Franklin, T. Balasubramanian and B. Varghese

Formula: 2C14H19N4O3+·C4H4O52-

Online 14 January 2009


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Acta Cryst. (2009). C65, o66-o69  [ doi:10.1107/S010827010900047X ]

Quinolin-6-ol at 100 K

A. Michta, M. Nowak and J. Kusz

Formula: C9H7NO

Online 14 January 2009


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Acta Cryst. (2009). C65, o70-o75  [ doi:10.1107/S0108270108043060 ]

The influence of sulfur substituents on the molecular geometry and packing of thio derivatives of N-methylphenobarbital

A. Janik, A. Olech, A. Stasiewicz-Urban and K. Stadnicka

Formula: C13H14N2O2S, C13H14N2O2S, C13H14N2OS2, C13H14N2S3 and C13H14N2O3

Online 14 January 2009


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Acta Cryst. (2009). C65, o76-o80  [ doi:10.1107/S0108270109001619 ]

4,6-Dinitro-N,N'-di-n-octylbenzene-1,3-diamine, 4,6-dinitro-N,N'-di-n-undecylbenzene-1,3-diamine and N,N'-bis(2,4-dinitrophenyl)octane-1,8-diamine

G. Teng, C. P. Walczak, P. J. Squattrito, D. K. Mohanty, W. Scharer, M. R. Giolando and K. Kirschbaum

Formula: C22H38N4O4, C28H50N4O4 and C20H24N6O8

Online 17 January 2009


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