Acta Crystallographica Section C

Crystal Structure Communications

Volume 65, Part 2 (February 2009)


	Cover illustration: Displacement ellipsoid plots for bis(acetato-²O,O')diaquazinc(II) at 110 K (left) and 250 K (right). Ellipsoids are drawn at the 50% probability level and H atoms are shown as small spheres of arbitrary radii. See Lutz & Spek [Acta Cryst. (2009), C65, m69-m74].

metal-organic compounds
organic compounds

metal-organic compounds

Acta Cryst. (2009). C65, m45-m47 [ doi:10.1107/S0108270108043643 ]

A two-dimensional network formed by self-associating silver(I) perchlorate with 3-[4-(2-thienyl)-2H-cyclopenta[d]pyridazin-1-yl]benzonitrile

X.-Y. Li, Q.-K. Liu, J.-P. Ma, R.-Q. Huang and Y.-B. Dong

Formula: [Ag(C₁₈H₁₁N₃S)]ClO₄·CH₄O

Online 10 January 2009

Acta Cryst. (2009). C65, m48-m51 [ doi:10.1107/S0108270108043631 ]

Robust packing in cyclopalladated primary amines: isomorphous crystal structures of four complexes with varying substitution patterns

B. Calmuschi-Cula, I. Kalf, C. Timofte and U. Englert

Formula: [Pd(C₈H₁₀N)Cl(C₅H₅N)], [PdBr(C₈H₁₀N)(C₅H₅N)], [PdBr(C₈H₉BrN)(C₆H₇N)] and [Pd(C₈H₉BrN)I(C₆H₇N)]

Online 10 January 2009

Acta Cryst. (2009). C65, m52-m55 [ doi:10.1107/S0108270108043783 ]

Luminescence properties of three structures built from 3-cyano-4-dicyanomethylene-5-oxo-4,5-dihydro-1H-pyrrol-2-olate and alkaline metals (Na, K and Rb)

V. A. Tafeenko, S. I. Gurskiy, A. N. Baranov, T. V. Kaisarova and L. A. Aslanov

Formula: Rb⁺·C₈HN₄O₂^- and Na⁺·C₈HN₄O₂^-·2H₂O

Online 10 January 2009

Acta Cryst. (2009). C65, m56-m58 [ doi:10.1107/S0108270108042637 ]

A three-dimensional homochiral metal-organic framework constructed from manganese(II) with S-carboxymethyl-N-(p-tosyl)-L-cysteine and 4,4'-bipyridine

W. Xiong, Y. Su, Z. Chen and F. Liang

Formula: [Mn(C₁₂H₁₃NO₆S₂)(C₁₀H₈N₂)(H₂O)]

Online 10 January 2009

Acta Cryst. (2009). C65, m59-m61 [ doi:10.1107/S0108270108043400 ]

A novel three-dimensional copper(I) coordination polymer constructed from a copper-bromide net and nicotinic acid ligands

M.-H. Yang

Formula: [CuBr(C₆H₅NO₂)]

Online 10 January 2009

Acta Cryst. (2009). C65, m62-m65 [ doi:10.1107/S0108270109000353 ]

Square-grid coordination networks of diaquabis(4,4'-bipyridyl)copper(II) crosslinked by hydrogen bonds through two monoanions of 1-benzofuran-2,3-dicarboxylic acid and five molecules of water

R. Koner and I. Goldberg

Formula: [Cu(C₁₀H₈N₂)₂(H₂O)₂](C₁₀H₅O₅)₂·5H₂O

Online 10 January 2009

Acta Cryst. (2009). C65, m66-m68 [ doi:10.1107/S0108270109000341 ]

A novel two-dimensional framework based on unprecedented cadmium(II) chains

J. Qin, J.-P. Ma, L.-L. Liu, R.-Q. Huang and Y.-B. Dong

Formula: [Cd(C₁₀H₈N₃O₂)Cl(H₂O)]

Online 10 January 2009

Acta Cryst. (2009). C65, m69-m74 [ doi:10.1107/S0108270108043242 ]

Directed anisotropy in bis(acetato-²O,O')diaquazinc(II) at 110 and 250 K

M. Lutz and A. L. Spek

Formula: [Zn(C₂H₃O₂)₂(H₂O)₂] at 110 and 250 K

Online 10 January 2009

Acta Cryst. (2009). C65, m75-m77 [ doi:10.1107/S0108270109000092 ]

A three-dimensional Al^III/Na^I metal-organic framework resulting from dimethylformamide hydrolysis

A. Plutecka and U. Rychlewska

Formula: (C₂H₈N)₂[AlNa(HCO₂)₆]

Online 10 January 2009

Acta Cryst. (2009). C65, m78-m81 [ doi:10.1107/S0108270108043667 ]

Two bicyclic dinuclear complexes generated from 3,3'-[1,3,4-thiadiazole-2,5-diyldi(thiomethylene)]dibenzoic acid (L) and dimethylformamide (DMF): [Cu(L)(DMF)]₂ and [Zn(L)(DMF)]₂

P. Wang, J.-P. Ma, X.-Y. Li, R.-Q. Huang and Y.-B. Dong

Formula: [Cu₂(C₁₈H₁₂N₂O₄S₃)₂(C₃H₇NO)₂] and [Zn₂(C₁₈H₁₂N₂O₄S₃)₂(C₃H₇NO)₂]

Online 14 January 2009

Acta Cryst. (2009). C65, m82-m85 [ doi:10.1107/S0108270109000559 ]

A novel threefold-interpenetrating primitive cubic network based on a dinuclear Zn₂ node

Y.-P. Diao, K. Li, S.-S. Huang, X.-H. Shu, K.-X. Liu and X.-M. Deng

Formula: [Zn₂(C₈H₄O₄)₂(C₁₂H₁₀N₄)]

Online 14 January 2009

Acta Cryst. (2009). C65, m86-m90 [ doi:10.1107/S0108270109000869 ]

Influence of solvent on the structures of two one-dimensional cobalt(II) coordination polymers with tetrachloroterephthalate

Y.-Q. Fang, M. Lu and C.-X. Lu

Formula: [Co(C₈Cl₄O₄)(C₅H₅N)₃(H₂O)]·C₅H₅N and [Co(C₈Cl₄O₄)(C₅H₅N)₂(H₂O)₂]·C₄H₈O₂·3H₂O

Online 14 January 2009

Acta Cryst. (2009). C65, m91-m93 [ doi:10.1107/S0108270109000742 ]

An unprecedented three-dimensional silver(I) cluster built up from pyrazine-2,3-dicarboxylate ligands

J. Wu

Formula: [Ag₃(C₆H₂N₂O₄)(C₆H₃N₂O₄)]

Online 14 January 2009

Acta Cryst. (2009). C65, m94-m96 [ doi:10.1107/S0108270109001139 ]

A polymorph of tetrakis(acetonitrile-N)copper(I) tetrafluoridoborate

J. W. Bats, T. Kretz and H.-W. Lerner

Formula: [Cu(C₂H₃N)₄]BF₄

Online 17 January 2009

Acta Cryst. (2009). C65, m97-m99 [ doi:10.1107/S0108270109001917 ]

Bis[2-(2-hydroxyethyl)pyridinium] -decavanadato-bis[pentaaquamanganate(II)] tetrahydrate

L. Klistincová, E. Rakovský and P. Schwendt

Formula: (C₇H₁₀NO)₂[Mn₂V₁₀O₂₈(H₂O)₁₀]·4H₂O

Online 24 January 2009

Acta Cryst. (2009). C65, m100-m102 [ doi:10.1107/S010827010803521X ]

{[SmCl(en)₄][In₂Te₄]}_n: an indium telluride with a one-dimensional sinusoidal chain

C.-Y. Li, J. Zhou, Y. Zhang, G.-Q. Bian and J. Dai

Formula: [SmCl(C₂H₈N₂)₄][In₂Te₄]

Online 24 January 2009

Acta Cryst. (2009). C65, m103-m106 [ doi:10.1107/S0108270109001590 ]

Poly[triaqua(₄-4-carboxybenzenesulfonato-⁴O:O':O'':O''')(4-carboxybenzenesulfonato-O)strontium(II)]

G. Prochniak and V. Videnova-Adrabinska

Formula: [Sr(C₇H₅O₅S)₂(H₂O)₃]

Online 24 January 2009

Acta Cryst. (2009). C65, m107-m109 [ doi:10.1107/S0108270109002674 ]

Poly[[[-1,1'-(butane-1,4-diyl)diimidazole-²N:N'](-cyclohexane-1,4-dicarboxylato-⁴O¹,O^1':O⁴,O^4')cadmium(II)] hemihydrate]: a parallel interpenetrating two-dimensional (4,4) network

S. Zhou, B. Liu and C.-B. Li

Formula: [Cd(C₈H₁₀O₄)(C₁₀H₁₄N₄)]·0.5H₂O

Online 28 January 2009

Acta Cryst. (2009). C65, m110-m114 [ doi:10.1107/S0108270109002492 ]

trans-Chlorido(phenyl)bis(triphenylphosphine)nickel(II) and its 1:1 cocrystal with chloridobis(triphenylphosphine)nickel(I)

L. Li, C. S. B. Gomes, C. A. Figueira, P. T. Gomes and M. T. Duarte

Formula: [Ni(C₆H₅)Cl(C₁₈H₁₅P)₂] and [Ni(C₆H₅)Cl(C₁₈H₁₅P)₂]·[NiCl(C₁₈H₁₅P)₂]

Online 28 January 2009

organic compounds

Acta Cryst. (2009). C65, o31-o34 [ doi:10.1107/S0108270108042911 ]

A new polymorph of triphenylmethylamine: the effect of hydrogen bonding

V. N. Khrustalev, I. V. Borisova, N. N. Zemlyansky and M. Y. Antipin

Formula: C₁₉H₁₇N

Online 10 January 2009

Acta Cryst. (2009). C65, o35-o38 [ doi:10.1107/S0108270108043655 ]

Tetrameric aggregate of 1,c-3-diphenyltetran-r-1-ol via an R₄⁴(8) homodromic ring

D. R. Vega, J. D. Mufato, J. M. Aguirre, E. V. Drago and B. Lantaño

Formula: C₂₂H₂₀O

Online 10 January 2009

Acta Cryst. (2009). C65, o39-o41 [ doi:10.1107/S0108270108042431 ]

gem-Dimethylcyclopropanation of dibenzylideneacetone using triisopropyl sulfoxonium tetrafluoroborate

M. G. Edwards, D. S. Pugh, A. C. Whitwood and R. J. K. Taylor

Formula: C₂₃H₂₆O

Online 10 January 2009

Acta Cryst. (2009). C65, o42-o45 [ doi:10.1107/S0108270108044223 ]

Hydrogen-bonded supramolecular motifs in 2-amino-4,6-dimethoxypyrimidinium picrate and pyrimethaminium picrate dimethyl sulfoxide solvate

K. Thanigaimani, A. Subashini, P. T. Muthiah, D. E. Lynch and R. J. Butcher

Formula: C₆H₁₀N₃O₂⁺·C₆H₂N₃O₇^- and C₁₂H₁₄ClN₄⁺·C₆H₂N₃O₇^-·C₂H₆OS

Online 10 January 2009

Acta Cryst. (2009). C65, o46-o50 [ doi:10.1107/S010827010804287X ]

Two enantiomerically pure cyclic arenesulfonamide hydrochloride salts

L. Kiefer, P. Dauban, R. H. Dodd and P. Retailleau

Formula: C₂₀H₂₁N₂O₂S⁺·Cl^- and C₂₆H₂₅N₂O₂S⁺·Cl^-

Online 10 January 2009

Acta Cryst. (2009). C65, o51-o53 [ doi:10.1107/S010827010804300X ]

Three-dimensional networks in the 1:2 organic salts 2,2'-biimidazolium bis(3-carboxy-4-hydroxybenzenesulfonate) and 2,2'-bibenzimidazolium bis(3-carboxy-4-hydroxybenzenesulfonate) trihydrate

C.-S. Zhou, L.-L. Ding, H. Zhang, M.-N. Cao and X.-G. Meng

Formula: C₆H₈N₄²⁺·2C₇H₅O₆S^- and C₁₄H₁₂N₄²⁺·2C₇H₅O₆S^-·3H₂O

Online 10 January 2009

Acta Cryst. (2009). C65, o54-o57 [ doi:10.1107/S0108270109000225 ]

Two modes of O-HO hydrogen bonding utilized in dimorphs of racemic 6-O-acryloyl-2-O-benzoyl-myo-inositol 1,3,5-orthoformate

S. Krishnaswamy, R. G. Gonnade, M. M. Bhadbhade and M. S. Shashidhar

Formula: Two forms of C₁₇H₁₆O₈

Online 10 January 2009

Acta Cryst. (2009). C65, o58-o61 [ doi:10.1107/S0108270108044132 ]

Salts of maleic and fumaric acids with oxine: the role of isomeric acids in hydrogen-bonding patterns

S. Franklin and T. Balasubramanian

Formula: C₉H₈NO⁺·C₄H₃O₄^- and C₉H₈NO⁺·C₄H₃O₄^-

Online 14 January 2009

Acta Cryst. (2009). C65, o62-o65 [ doi:10.1107/S0108270109000237 ]

Bis[2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidin-1-ium] DL-malate

S. Franklin, T. Balasubramanian and B. Varghese

Formula: 2C₁₄H₁₉N₄O₃⁺·C₄H₄O₅^2-

Online 14 January 2009

Acta Cryst. (2009). C65, o66-o69 [ doi:10.1107/S010827010900047X ]

Quinolin-6-ol at 100 K

A. Michta, M. Nowak and J. Kusz

Formula: C₉H₇NO

Online 14 January 2009

Acta Cryst. (2009). C65, o70-o75 [ doi:10.1107/S0108270108043060 ]

The influence of sulfur substituents on the molecular geometry and packing of thio derivatives of N-methylphenobarbital

A. Janik, A. Olech, A. Stasiewicz-Urban and K. Stadnicka

Formula: C₁₃H₁₄N₂O₂S, C₁₃H₁₄N₂O₂S, C₁₃H₁₄N₂OS₂, C₁₃H₁₄N₂S₃ and C₁₃H₁₄N₂O₃

Online 14 January 2009

Acta Cryst. (2009). C65, o76-o80 [ doi:10.1107/S0108270109001619 ]

4,6-Dinitro-N,N'-di-n-octylbenzene-1,3-diamine, 4,6-dinitro-N,N'-di-n-undecylbenzene-1,3-diamine and N,N'-bis(2,4-dinitrophenyl)octane-1,8-diamine

G. Teng, C. P. Walczak, P. J. Squattrito, D. K. Mohanty, W. Scharer, M. R. Giolando and K. Kirschbaum

Formula: C₂₂H₃₈N₄O₄, C₂₈H₅₀N₄O₄ and C₂₀H₂₄N₆O₈

Online 17 January 2009

Acta Crystallographica Section C

Crystal Structure Communications

Volume 65, Part 2 (February 2009)

metal-organic compounds

A two-dimensional network formed by self-associating silver(I) perchlorate with 3-[4-(2-thienyl)-2H-cyclopenta[d]pyridazin-1-yl]benzonitrile

X.-Y. Li, Q.-K. Liu, J.-P. Ma, R.-Q. Huang and Y.-B. Dong

Robust packing in cyclopalladated primary amines: isomorphous crystal structures of four complexes with varying substitution patterns

B. Calmuschi-Cula, I. Kalf, C. Timofte and U. Englert

Luminescence properties of three structures built from 3-cyano-4-dicyanomethylene-5-oxo-4,5-dihydro-1H-pyrrol-2-olate and alkaline metals (Na, K and Rb)

V. A. Tafeenko, S. I. Gurskiy, A. N. Baranov, T. V. Kaisarova and L. A. Aslanov

A three-dimensional homochiral metal-organic framework constructed from manganese(II) with S-carboxymethyl-N-(p-tosyl)-L-cysteine and 4,4'-bipyridine

W. Xiong, Y. Su, Z. Chen and F. Liang

A novel three-dimensional copper(I) coordination polymer constructed from a copper-bromide net and nicotinic acid ligands

M.-H. Yang

Square-grid coordination networks of diaquabis(4,4'-bipyridyl)copper(II) crosslinked by hydrogen bonds through two monoanions of 1-benzofuran-2,3-dicarboxylic acid and five molecules of water

R. Koner and I. Goldberg

A novel two-dimensional framework based on unprecedented cadmium(II) chains

J. Qin, J.-P. Ma, L.-L. Liu, R.-Q. Huang and Y.-B. Dong

Directed anisotropy in bis(acetato-2O,O')diaquazinc(II) at 110 and 250 K

M. Lutz and A. L. Spek

A three-dimensional AlIII/NaI metal-organic framework resulting from dimethylformamide hydrolysis

A. Plutecka and U. Rychlewska

Two bicyclic dinuclear complexes generated from 3,3'-[1,3,4-thiadiazole-2,5-diyldi(thiomethylene)]dibenzoic acid (L) and dimethylformamide (DMF): [Cu(L)(DMF)]2 and [Zn(L)(DMF)]2

P. Wang, J.-P. Ma, X.-Y. Li, R.-Q. Huang and Y.-B. Dong

A novel threefold-interpenetrating primitive cubic network based on a dinuclear Zn2 node

Y.-P. Diao, K. Li, S.-S. Huang, X.-H. Shu, K.-X. Liu and X.-M. Deng

Influence of solvent on the structures of two one-dimensional cobalt(II) coordination polymers with tetrachloroterephthalate

Y.-Q. Fang, M. Lu and C.-X. Lu

An unprecedented three-dimensional silver(I) cluster built up from pyrazine-2,3-dicarboxylate ligands

J. Wu

A polymorph of tetrakis(acetonitrile-N)copper(I) tetrafluoridoborate

J. W. Bats, T. Kretz and H.-W. Lerner

Bis[2-(2-hydroxyethyl)pyridinium] -decavanadato-bis[pentaaquamanganate(II)] tetrahydrate

L. Klistincová, E. Rakovský and P. Schwendt

{[SmCl(en)4][In2Te4]}n: an indium telluride with a one-dimensional sinusoidal chain

C.-Y. Li, J. Zhou, Y. Zhang, G.-Q. Bian and J. Dai

Poly[triaqua(4-4-carboxybenzenesulfonato-4O:O':O'':O''')(4-carboxybenzenesulfonato-O)strontium(II)]

G. Prochniak and V. Videnova-Adrabinska

Poly[[[-1,1'-(butane-1,4-diyl)diimidazole-2N:N'](-cyclohexane-1,4-dicarboxylato-4O1,O1':O4,O4')cadmium(II)] hemihydrate]: a parallel interpenetrating two-dimensional (4,4) network

S. Zhou, B. Liu and C.-B. Li

trans-Chlorido(phenyl)bis(triphenylphosphine)nickel(II) and its 1:1 cocrystal with chloridobis(triphenylphosphine)nickel(I)

L. Li, C. S. B. Gomes, C. A. Figueira, P. T. Gomes and M. T. Duarte

organic compounds

A new polymorph of triphenylmethylamine: the effect of hydrogen bonding

V. N. Khrustalev, I. V. Borisova, N. N. Zemlyansky and M. Y. Antipin

Tetrameric aggregate of 1,c-3-diphenyltetran-r-1-ol via an R44(8) homodromic ring

D. R. Vega, J. D. Mufato, J. M. Aguirre, E. V. Drago and B. Lantaño

gem-Dimethylcyclopropanation of dibenzylideneacetone using triisopropyl sulfoxonium tetrafluoroborate

M. G. Edwards, D. S. Pugh, A. C. Whitwood and R. J. K. Taylor

Hydrogen-bonded supramolecular motifs in 2-amino-4,6-dimethoxypyrimidinium picrate and pyrimethaminium picrate dimethyl sulfoxide solvate

K. Thanigaimani, A. Subashini, P. T. Muthiah, D. E. Lynch and R. J. Butcher

Two enantiomerically pure cyclic arenesulfonamide hydrochloride salts

L. Kiefer, P. Dauban, R. H. Dodd and P. Retailleau

Three-dimensional networks in the 1:2 organic salts 2,2'-biimidazolium bis(3-carboxy-4-hydroxybenzenesulfonate) and 2,2'-bibenzimidazolium bis(3-carboxy-4-hydroxybenzenesulfonate) trihydrate

C.-S. Zhou, L.-L. Ding, H. Zhang, M.-N. Cao and X.-G. Meng

Two modes of O-HO hydrogen bonding utilized in dimorphs of racemic 6-O-acryloyl-2-O-benzoyl-myo-inositol 1,3,5-orthoformate

S. Krishnaswamy, R. G. Gonnade, M. M. Bhadbhade and M. S. Shashidhar

Salts of maleic and fumaric acids with oxine: the role of isomeric acids in hydrogen-bonding patterns

S. Franklin and T. Balasubramanian

Bis[2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidin-1-ium] DL-malate

S. Franklin, T. Balasubramanian and B. Varghese

Quinolin-6-ol at 100 K

A. Michta, M. Nowak and J. Kusz

The influence of sulfur substituents on the molecular geometry and packing of thio derivatives of N-methylphenobarbital

A. Janik, A. Olech, A. Stasiewicz-Urban and K. Stadnicka

4,6-Dinitro-N,N'-di-n-octylbenzene-1,3-diamine, 4,6-dinitro-N,N'-di-n-undecylbenzene-1,3-diamine and N,N'-bis(2,4-dinitrophenyl)octane-1,8-diamine

G. Teng, C. P. Walczak, P. J. Squattrito, D. K. Mohanty, W. Scharer, M. R. Giolando and K. Kirschbaum

Directed anisotropy in bis(acetato-²O,O')diaquazinc(II) at 110 and 250 K

A three-dimensional Al^III/Na^I metal-organic framework resulting from dimethylformamide hydrolysis

Two bicyclic dinuclear complexes generated from 3,3'-[1,3,4-thiadiazole-2,5-diyldi(thiomethylene)]dibenzoic acid (L) and dimethylformamide (DMF): [Cu(L)(DMF)]₂ and [Zn(L)(DMF)]₂

A novel threefold-interpenetrating primitive cubic network based on a dinuclear Zn₂ node

{[SmCl(en)₄][In₂Te₄]}_n: an indium telluride with a one-dimensional sinusoidal chain

Poly[triaqua(₄-4-carboxybenzenesulfonato-⁴O:O':O'':O''')(4-carboxybenzenesulfonato-O)strontium(II)]

Poly[[[-1,1'-(butane-1,4-diyl)diimidazole-²N:N'](-cyclohexane-1,4-dicarboxylato-⁴O¹,O^1':O⁴,O^4')cadmium(II)] hemihydrate]: a parallel interpenetrating two-dimensional (4,4) network

Tetrameric aggregate of 1,c-3-diphenyltetran-r-1-ol via an R₄⁴(8) homodromic ring