Acta Crystallographica Section C

Crystal Structure Communications

Volume 65, Part 8 (August 2009)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: Packing diagrams for the two forms of 2,2,3,3,4,4-hexafluoropentane-1,5-diol, both at 173 K, viewed with respect to the (012) plane and with the [100] axis parallel to the horizontal axis. The hydrogen-bonding network (dashed lines) is preserved through the phase transition. See Ha & Young [Acta Cryst. (2009), C65, o388-o395].

inorganic compounds


 

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Acta Cryst. (2009). C65, i45-i47  [ doi:10.1107/S010827010902397X ]

Co0.50VOPO4·2H2O

L. Meng, Y. Ma, X. Zhang and Y. Xu

Synopsis: The title cobalt vanadophosphate dihydrate contains flat layers of VO5 and PO4 polyhedra covalently linked by CoII ions coordinated to vanadyl O atoms. This is believed to be the first example of a layered vanadophosphate bridged by a transition metal ion in this manner.

Formula: Co0.50VOPO4·2H2O

Online 15 July 2009


 

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Acta Cryst. (2009). C65, i48-i51  [ doi:10.1107/S0108270109021519 ]

Reinvestigation of Sr2[Cu(OH)6]

S. Sutovic, L. Karanovic and D. Poleti

Synopsis: Sr2[Cu(OH)6] crystallizes in the monoclinic system in the space group P21/n (No. 14). The crystal structure is built up from mutually isolated highly elongated Cu(OH)6 octahedra and trigonal Sr(OH)6 prisms, forming layers parallel to (110). The Cu(OH)6 octahedra are connected into an infinite three-dimensional framework of hydrogen bonds.

Formula: Sr2[Cu(OH)6]

Online 18 July 2009


 

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Acta Cryst. (2009). C65, i52-i53  [ doi:10.1107/S0108270109027188 ]

Na10(Na,Mn)7Mn43(PO4)36: a new synthetic fillowite-type phosphate

F. Hatert, P. Keller, F. Lissner and T. Schleid

Synopsis: The title compound, Na10(Na,Mn)7Mn43(PO4)36, has been synthesized hydrothermally. Its crystal structure is similar to that of natural fillowite-type phosphates and can be described as a hexagonal packing of three types of rods parallel to the c axis, which show an alternation of Mn, Na and P sites and lattice vacancies.

Formula: Na10(Na,Mn)7Mn43(PO4)36

Online 22 July 2009


 

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Acta Cryst. (2009). C65, i54-i56  [ doi:10.1107/S0108270109027218 ]

[CrBr2(NH3)4][CrBr4(NH3)2], a new chromium(III) complex

L. Stork, X. Liu, B. P. T. Fokwa and R. Dronskowski

Synopsis: The title compound, tetraamminedibromidochromium(III) diamminetetrabromidochromium(III), crystallizes in the space group P\\overline{1} (Z = 1). The structure is composed of octahedral trans-[CrBr2(NH3)4]+ cations and octahedral trans-[CrBr4(NH3)2]- anions adopting a distorted CsCl-type lattice.

Formula: [CrBr2(NH3)4][CrBr4(NH3)2]

Online 22 July 2009


metal-organic compounds


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Acta Cryst. (2009). C65, m273-m275  [ doi:10.1107/S010827010902438X ]

A new three-dimensional cobalt(II) coordination polymer with a 4-connected CdSO4-like topology

Z.-L. Xu, Z.-G. Kong, S.-B. Sun and X.-Y. Wang

Formula: [Co(C12H8O4)(H2O)2]

Online 7 July 2009


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Acta Cryst. (2009). C65, m276-m278  [ doi:10.1107/S0108270109022331 ]

Poly[diaqua[[mu]-1,4-bis(imidazol-1-ylmethyl)benzene-[kappa]2N3:N3']([mu]-trans-cyclohexane-1,4-carboxylato-[kappa]2O1:O4)manganese(II)]: a three-dimensional hydrogen-bonding [alpha]-polonium net

Q.-W. Wang, X.-Y. Wang, M. Wang, B.-Y. Li and X.-Y. Ma

Formula: [Mn(C8H10O4)(C14H14N4)(H2O)2]

Online 7 July 2009


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Acta Cryst. (2009). C65, m279-m283  [ doi:10.1107/S0108270109023968 ]

Bis(1,3,4-trimethylpyridinium) tetrachloridocuprate(II) and bis(1,3,4-trimethylpyridinium) tetrabromidocuprate(II): an examination of the A2CuX4 Fdd2 structure type

M. R. Bond

Formula: (C8H12N)2[CuCl4] and (C8H12N)2[CuBr4]

Online 7 July 2009


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Acta Cryst. (2009). C65, m284-m286  [ doi:10.1107/S010827010902575X ]

The chiral helical structure of a copper(II) complex with a tridentate Schiff base ligand

W.-J. Shi

Formula: [Cu(C9H9N2O2)(H2O)]ClO4

Online 9 July 2009


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Acta Cryst. (2009). C65, m287-m290  [ doi:10.1107/S0108270109021337 ]

Poly[hexaaquabis([mu]4-4-carboxybenzenesulfonato)bis([mu]3-4-carboxybenzenesulfonato)calcium(II)dipotassium(I)]

G. Prochniak and V. Videnova-Adrabinska

Formula: [CaK2(C7H5O5S)4(H2O)6]

Online 9 July 2009


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Acta Cryst. (2009). C65, m291-m295  [ doi:10.1107/S0108270109025311 ]

Two related lithium calixarene complexes, [p-tert-butylcalix[4]arene(OMe)(OH)2(OLi)]2·4MeCN and {p-tert-butylcalix[4]arene(OH)2(OLi)[OLi(NCMe)2]}2·8MeCN, determined using synchrotron radiation

D. S. Lee, M. R. J. Elsegood, C. Redshaw and S. Zhan

Formula: [Li2(C45H57O4)2]·4C2H3N and [Li4(C44H54O4)2(C2H3N)4]·8C2H3N

Online 9 July 2009


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Acta Cryst. (2009). C65, m296-m298  [ doi:10.1107/S0108270109025293 ]

Diaqua(oxydiacetato-[kappa]3O,O',O'')(pyridine-3-carboxamide-[kappa]N1)copper(II)

M. Perec and R. Baggio

Formula: [Cu(C4H4O5)(C6H6N2O)(H2O)2]

Online 9 July 2009


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Acta Cryst. (2009). C65, m299-m301  [ doi:10.1107/S0108270109017831 ]

A monomeric gold(I) carbanion complex with an uncoordinated thioether: [2-(methylsulfanyl)phenyl](triphenylphosphine)gold(I)

D. Y. Melgarejo, G. M. Chiarella and J. P. Fackler

Formula: [Au(C7H7S)(C18H15P)]

Online 11 July 2009


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Acta Cryst. (2009). C65, m302-m304  [ doi:10.1107/S0108270109024500 ]

Diaquatetrakis(tert-butyl isocyanide)cobalt(II) bis(perchlorate): an example of cobalt(II) coordinated by only four alkyl isocyanide ligands

C. A. L. Becker, R. P. Forbes and R. S. Black

Formula: [Co(C5H9N)4(H2O)2](ClO4)2

Online 11 July 2009


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Acta Cryst. (2009). C65, m305-m307  [ doi:10.1107/S010827010902695X ]

catena-Poly[[[(iminodiacetato-[kappa]O)silver(I)]-[mu]3-2-aminopyrimidine-[kappa]3N1:N2:N3] monohydrate]: a one-dimensional silver(I) coordination polymer with mixed ligands

D. Sun, G.-G. Luo, R.-B. Huang, N. Zhang and L.-S. Zheng

Formula: [Ag(C4H6NO4)(C4H5N3)]·H2O

Online 15 July 2009


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Acta Cryst. (2009). C65, m308-m310  [ doi:10.1107/S0108270109024445 ]

A novel metallo-organically templated pentaborate: acetato[N,N'-bis(2-aminoethyl)ethane-1,2-diamine]zinc(II) 4,4',6,6'-tetrahydroxy-2,2'-spirobi[cyclotriboroxane](1-)

S.-L. Wu, H.-X. Liu, X. Jiang, Z.-D. Shao and Y.-X. Liang

Formula: [Zn(C2H3O2)(C6H18N4)](B5H4O10)

Online 18 July 2009


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Acta Cryst. (2009). C65, m311-m313  [ doi:10.1107/S0108270109028005 ]

(Acetato-[kappa]O)aqua(1H-imidazole-[kappa]N3)(picolinato-[kappa]2N,O)copper(II) 0.87-hydrate: a Z' > 1 structure

A.-C. Chamayou, C. Biswas, A. Ghosh and C. Janiak

Formula: [Cu(C6H4NO2)(C2H3O2)(C3H4N2)(H2O)]·0.87H2O

Online 25 July 2009


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Acta Cryst. (2009). C65, m314-m316  [ doi:10.1107/S0108270109027516 ]

(Acetato-[kappa]O)[tris(3,5-dimethylpyrazol-1-yl-[kappa]N2)hydroborato]zinc(II)

A. Beheshti, W. Clegg, S. H. Dale and R. Hyvadi

Formula: [Zn(C15H22BN6)(C2H3O2)]

Online 25 July 2009


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Acta Cryst. (2009). C65, m317-m320  [ doi:10.1107/S0108270109027735 ]

A novel trinuclear zinc(II) cluster with a tetrahedral ZnO4 core

O. Q. Munro, K. Gillham and M. P. Akerman

Formula: [Zn3(C11H11NO2)2(C2H3O2)2(CH4O)2]

Online 25 July 2009


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Acta Cryst. (2009). C65, m321-m324  [ doi:10.1107/S0108270109028571 ]

Three-dimensional framework structures: isomorphous bis(2,6-diamino-3,5-dibromopyridinium) tetrabromidometallate(II) salts with CdII and MnII

R. H. Al-Far, S. F. Haddad and B. F. Ali

Formula: (C5H6Br2N3)2[CdBr4] and (C5H6Br2N3)2[MnBr4]

Online 25 July 2009


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Acta Cryst. (2009). C65, m325-m327  [ doi:10.1107/S0108270109027589 ]

catena-Poly[[bis(acetylacetonato-[kappa]2O,O')cobalt(II)]-[mu]-1,3-di-4-pyridylpropane-[kappa]2N:N']: a one-dimensional coordination polymer capable of forming clathrates with prochiral aldehydes

A. Lennartson and M. Håkansson

Formula: [Co(C5H7O2)2(C13H14N2)]

Online 30 July 2009


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Acta Cryst. (2009). C65, m328-m330  [ doi:10.1107/S010827010902839X ]

The anionic coordination polymer {K2[PtII2AgI8(2,2'-bipyridine)2(O2CCF3)14]}n

Z. M. Hudson, Y. Sun, B. Ross, R.-Y. Wang and S. Wang

Formula: K2[Pt2Ag8(C2F3O2)14(C10H8N2)2]

Online 30 July 2009


organic compounds


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Acta Cryst. (2009). C65, o365-o370  [ doi:10.1107/S0108270109022203 ]

Structural comparisons between methylated and unmethylated nitrophenyl lophines

D. Yanover and M. Kaftory

Formula: C21H15N3O2, C21H15N3O2·C2H3N, C21H15N3O2·CH4O, C22H17N3O2·CH4O, C22H17N3O2 and C22H17N3O2

Online 7 July 2009


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Acta Cryst. (2009). C65, o371-o373  [ doi:10.1107/S010827010902410X ]

N,N'-Bis(2-ammonioethyl)propane-1,3-diaminium tris(perchlorate) chloride

H. B. Szczesniak, V. Patroniak, W. Radecka-Paryzek and M. Kubicki

Formula: C7H24N44+·3ClO4-·Cl-

Online 7 July 2009


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Acta Cryst. (2009). C65, o374-o376  [ doi:10.1107/S0108270109025566 ]

4-(2-Fluorophenyl)-6-(1H-indol-1-yl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carbonitrile: a chain of rings built from N-H...N, C-H...N and C-H...[pi](arene) hydrogen bonds

J. Quiroga, A. Sánchez, J. Cobo and C. Glidewell

Formula: C28H18FN5

Online 9 July 2009


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Acta Cryst. (2009). C65, o377-o380  [ doi:10.1107/S0108270109025451 ]

2-Oxo-2-phenyl-N-[(R)-1-phenylethyl]acetamide and N,N-dimethyl-2-(1-naphthyl)-2-oxoacetamide: possibility of Yang photocyclization in a crystal

J. Bakowicz and I. Turowska-Tyrk

Formula: C16H15NO2 and C14H13NO2

Online 9 July 2009


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Acta Cryst. (2009). C65, o381-o384  [ doi:10.1107/S0108270109024457 ]

Polymorphism and phase transition behavior of 6,6'-bis(chloromethyl)-1,1',4,4'-tetramethyl-3,3'-(p-phenylenedimethylene)bis(piperazine-2,5-dione)

N. W. Polaske, G. S. Nichol and B. Olenyuk

Formula: Three polymorphs of C22H28Cl2N4O4

Online 9 July 2009


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Acta Cryst. (2009). C65, o385-o387  [ doi:10.1107/S0108270109025475 ]

N,N-Diethyl-N'-[(E)-4-pyridylmethylene]benzene-1,4-diamine: a combined X-ray and density functional theory study

R. W. Seidel, W. S. Sheldrick, T. M. Kolev and B. B. Koleva

Formula: C16H19N3

Online 11 July 2009


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Acta Cryst. (2009). C65, o388-o395  [ doi:10.1107/S0108270109025141 ]

Enantiotropic phase transition and twinning in 2,2,3,3,4,4-hexafluoropentane-1,5-diol

J.-M. Ha and V. Young

Formula: Four forms of C5H6F6O2

Online 11 July 2009


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Acta Cryst. (2009). C65, o396-o399  [ doi:10.1107/S0108270109020551 ]

Weak intermolecular interactions in isomorphous 5-(2-chloroethoxy)-2,3-dihydro-1,4-benzodioxine and 5-(2-bromoethoxy)-2,3-dihydro-1,4-benzodioxine: bonding or nonbonding interactions

R. Kruszynski

Formula: C10H11ClO3 and C10H11BrO3

Online 11 July 2009


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Acta Cryst. (2009). C65, o400-o403  [ doi:10.1107/S0108270109025682 ]

Similarities and differences between bis[2-(bromomethyl)phenyl] diselenide, bis[2-(chloromethyl)phenyl] diselenide and bis[2-(hydroxymethyl)phenyl] diselenide

A. Lari, F. Rominger and R. Gleiter

Formula: C14H12Br2Se2, C14H12Cl2Se2 and C14H14O2Se2

Online 15 July 2009


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Acta Cryst. (2009). C65, o404-o405  [ doi:10.1107/S0108270109026511 ]

Triclosan

A. I. Ramos, S. S. Braga and F. A. Almeida Paz

Formula: C12H7Cl3O2

Online 15 July 2009


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Acta Cryst. (2009). C65, o406-o409  [ doi:10.1107/S0108270109025165 ]

Structures of 1-hydrophenanthroimidazoles: building blocks in the synthesis of expanded-ring bis(imidazoles)

R. T. Stibrany and J. A. Potenza

Formula: C15H10N2 and C15H8Br2N2·0.5H2O

Online 15 July 2009


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Acta Cryst. (2009). C65, o410-o413  [ doi:10.1107/S0108270109026390 ]

Supramolecular motifs in the first structures of organic carboxylate salts of 1-(diaminomethylene)thiourea (HATU)

M. Holynska and M. Kubiak

Formula: C2H7N4S+·CHO2- and 2C2H7N4S+·C2O42-·2H2O

Online 15 July 2009


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Acta Cryst. (2009). C65, o414-o418  [ doi:10.1107/S0108270109025724 ]

N-H...O and O-H...O hydrogen-bonded supramolecular networks in 4-chloroanilinium, 2-hydroxyanilinium and 3-hydroxyanilinium hydrogen phthalates

R. Jagan and K. Sivakumar

Formula: C6H7ClN+·C8H5O4- and two forms of C6H8NO+·C8H5O4-

Online 18 July 2009


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Acta Cryst. (2009). C65, o419-o422  [ doi:10.1107/S0108270109027164 ]

Codeine dihydrogen phosphate hemihydrate

C. Langes, T. Gelbrich, U. J. Griesser and V. Kahlenberg

Formula: C18H22NO3+·H2PO4-·0.5H2O

Online 18 July 2009


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Acta Cryst. (2009). C65, o423-o430  [ doi:10.1107/S0108270109028017 ]

Eight 7-benzyl-3-tert-butyl-1-phenylpyrazolo[3,4-d]oxazines, encompassing structures containing no intermolecular hydrogen bonds, and hydrogen-bonded structures in one, two or three dimensions

J. C. Castillo, R. Abonía, J. Cobo and C. Glidewell

Formula: C22H25N3O, C23H27N3O, C23H27N3O2, C23H24F3N3O, C22H24N4O3, C24H29N3O3, C23H25N3O3 and C25H31N3O4

Online 30 July 2009


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