# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' s4346b' _shelx_refln_list_code 4 _shelx_F_calc_maximum 79.02 _exptl_crystal_F_000 215.00 _reflns_d_resolution_high 0.7697 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 5.1376 _cell_length_b 8.1188 _cell_length_c 9.7529 _cell_angle_alpha 73.126 _cell_angle_beta 76.885 _cell_angle_gamma 76.025 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 390.12 382.83 3.46 o 2 0 0 76.15 73.21 0.63 o 3 0 0 226.04 232.42 1.82 o 4 0 0 840.89 818.77 6.17 o 5 0 0 16.63 17.74 0.78 o 6 0 0 186.63 189.59 1.93 o -6 1 0 76.36 74.79 1.18 o -5 1 0 16.08 15.44 0.37 o -4 1 0 360.00 364.71 2.64 o -3 1 0 888.37 921.90 7.01 o -2 1 0 253.89 243.80 1.94 o -1 1 0 91.07 95.47 0.48 o 0 1 0 1533.99 1525.18 11.64 o 1 1 0 267.91 284.43 1.35 o 2 1 0 1400.62 1413.90 12.00 o 3 1 0 58.75 64.29 0.87 o 4 1 0 57.31 61.08 0.68 o 5 1 0 435.10 439.26 3.46 o 6 1 0 103.69 105.43 1.38 o -6 2 0 5.94 4.78 0.76 o -5 2 0 195.51 198.74 1.72 o -4 2 0 13.86 12.64 0.29 o -3 2 0 942.09 911.21 6.68 o -2 2 0 111.83 109.43 0.56 o -1 2 0 214.13 176.35 0.85 o 0 2 0 1202.59 1226.11 5.99 o 1 2 0 3892.85 3772.62 21.33 o 2 2 0 64.81 62.00 0.36 o 3 2 0 435.67 439.71 3.28 o 4 2 0 2.63 3.00 0.26 o 5 2 0 446.90 445.32 3.78 o 6 2 0 1.22 0.43 0.32 o -5 3 0 56.80 63.19 1.14 o -4 3 0 1.11 2.18 0.30 o -3 3 0 414.30 416.10 2.42 o -2 3 0 411.84 457.19 2.48 o -1 3 0 974.42 1002.53 4.60 o 0 3 0 326.65 337.24 1.60 o 1 3 0 407.99 363.57 1.84 o 2 3 0 26.77 34.69 0.31 o 3 3 0 643.42 616.93 3.89 o 4 3 0 9.57 6.87 0.26 o 5 3 0 211.58 204.89 2.46 o 6 3 0 6.34 7.03 0.57 o -5 4 0 4.01 4.10 0.69 o -4 4 0 163.25 161.24 1.42 o -3 4 0 97.97 100.96 0.78 o -2 4 0 921.68 896.90 4.78 o -1 4 0 62.24 78.83 0.48 o 0 4 0 650.27 649.99 3.14 o 1 4 0 22.76 21.99 0.21 o 2 4 0 2455.66 2604.80 18.47 o 3 4 0 74.65 83.90 0.64 o 4 4 0 155.93 160.06 1.26 o 5 4 0 43.10 40.65 0.84 o 6 4 0 111.25 114.07 1.49 o -4 5 0 505.48 505.11 4.16 o -3 5 0 86.93 82.76 0.80 o -2 5 0 341.93 359.08 2.12 o -1 5 0 1.23 0.54 0.16 o 0 5 0 1804.70 1776.08 9.85 o 1 5 0 61.21 67.68 0.55 o 2 5 0 831.85 846.15 5.95 o 3 5 0 12.60 13.94 0.32 o 4 5 0 833.06 818.59 5.69 o 5 5 0 16.36 20.17 0.48 o 6 5 0 201.31 185.73 7.26 o -4 6 0 152.33 161.05 1.84 o -3 6 0 56.00 54.38 0.74 o -2 6 0 3.39 3.18 0.31 o -1 6 0 315.43 300.75 2.44 o 0 6 0 19.58 21.07 0.36 o 1 6 0 484.25 498.29 3.33 o 2 6 0 174.91 159.16 1.31 o 3 6 0 82.96 92.52 0.99 o 4 6 0 175.11 168.19 1.74 o 5 6 0 229.34 242.09 3.53 o -3 7 0 238.30 246.25 2.34 o -2 7 0 11.84 11.97 0.59 o -1 7 0 198.73 207.81 1.80 o 0 7 0 306.00 313.75 2.21 o 1 7 0 1669.08 1629.31 11.04 o 2 7 0 0.83 0.80 0.22 o 3 7 0 37.67 41.09 1.13 o 4 7 0 19.18 21.79 1.39 o 5 7 0 201.77 201.51 2.55 o -2 8 0 30.62 26.63 0.61 o -1 8 0 174.74 176.37 1.63 o 0 8 0 1.55 2.39 0.30 o 1 8 0 15.77 14.77 0.48 o 2 8 0 41.66 43.69 1.08 o 3 8 0 80.15 74.25 0.94 o 4 8 0 8.69 11.46 0.60 o -1 9 0 10.06 9.02 0.47 o 0 9 0 74.34 76.33 1.02 o 1 9 0 8.97 8.76 0.44 o 2 9 0 491.62 492.39 4.42 o 3 9 0 0.87 0.76 0.36 o 1 10 0 74.67 75.34 1.43 o 2 10 0 99.21 100.04 1.47 o -3 -9 1 25.61 25.73 0.72 o -2 -9 1 24.58 24.63 0.63 o -1 -9 1 1.76 1.83 0.41 o 0 -9 1 90.55 94.13 1.34 o 1 -9 1 2.71 2.11 0.41 o -4 -8 1 142.43 145.36 2.04 o -3 -8 1 24.97 30.77 0.67 o -2 -8 1 163.79 163.50 2.65 o -1 -8 1 6.38 6.30 0.37 o 0 -8 1 276.35 269.72 2.83 o 1 -8 1 2.62 2.38 0.53 o 2 -8 1 193.49 195.45 2.00 o -5 -7 1 4.50 4.63 1.28 o -4 -7 1 24.64 27.39 0.73 o -3 -7 1 232.62 214.77 2.00 o -2 -7 1 79.10 83.24 0.92 o -1 -7 1 117.74 117.12 1.15 o 0 -7 1 31.57 34.31 0.56 o 1 -7 1 120.40 126.83 1.27 o 2 -7 1 42.63 41.21 0.77 o 3 -7 1 54.74 62.40 1.18 o -5 -6 1 471.98 465.92 5.84 o -4 -6 1 26.66 27.38 1.34 o -3 -6 1 349.73 340.07 2.55 o -2 -6 1 26.96 27.36 0.45 o -1 -6 1 962.80 960.20 7.90 o 0 -6 1 146.02 146.71 1.27 o 1 -6 1 770.34 766.18 5.27 o 2 -6 1 2.06 2.56 0.25 o 3 -6 1 216.92 216.19 2.05 o 4 -6 1 18.70 14.93 0.63 o -5 -5 1 229.71 234.77 2.77 o -4 -5 1 189.25 181.15 1.73 o -3 -5 1 59.68 69.45 0.65 o -2 -5 1 3.25 0.79 0.22 o -1 -5 1 871.59 886.37 5.94 o 0 -5 1 172.32 181.04 1.26 o 1 -5 1 494.85 499.06 3.49 o 2 -5 1 74.74 85.11 0.72 o 3 -5 1 265.36 258.33 1.92 o 4 -5 1 334.21 326.21 3.28 o -6 -4 1 84.88 81.32 1.22 o -5 -4 1 190.92 187.13 2.30 o -4 -4 1 997.48 971.64 6.33 o -3 -4 1 16.63 20.40 0.27 o -2 -4 1 414.04 394.52 2.36 o -1 -4 1 49.11 47.40 0.52 o 0 -4 1 670.72 665.68 3.13 o 1 -4 1 616.96 629.66 3.87 o 2 -4 1 805.81 819.96 4.24 o 3 -4 1 271.96 273.53 1.80 o 4 -4 1 317.66 317.67 2.55 o 5 -4 1 0.16 0.86 0.79 o -6 -3 1 40.53 37.44 0.98 o -5 -3 1 8.71 8.97 0.36 o -4 -3 1 172.24 168.57 1.30 o -3 -3 1 0.42 0.43 0.08 o -2 -3 1 3354.79 3501.85 18.34 o -1 -3 1 945.45 1050.48 5.20 o 0 -3 1 5.98 2.92 0.09 o 1 -3 1 381.09 410.17 2.00 o 2 -3 1 186.07 175.48 1.05 o 3 -3 1 23.76 23.33 0.26 o 4 -3 1 128.46 128.23 1.14 o 5 -3 1 1.98 1.74 0.34 o -6 -2 1 21.20 22.25 0.77 o -5 -2 1 446.01 445.99 3.80 o -4 -2 1 67.18 63.96 0.71 o -3 -2 1 535.45 527.60 3.02 o -2 -2 1 484.37 527.35 2.52 o -1 -2 1 69.50 53.61 0.33 o 0 -2 1 39.09 38.54 0.26 o 1 -2 1 120.51 114.71 0.68 o 2 -2 1 68.30 71.88 0.47 o 3 -2 1 1931.20 1959.88 9.58 o 4 -2 1 77.29 76.35 0.77 o 5 -2 1 154.08 151.38 1.52 o 6 -2 1 65.21 62.51 1.30 o -6 -1 1 9.24 7.85 0.57 o -5 -1 1 407.02 405.51 4.00 o -4 -1 1 0.33 0.85 0.22 o -3 -1 1 791.10 755.36 5.54 o -2 -1 1 212.88 224.35 1.29 o -1 -1 1 2981.88 2925.55 19.33 o 0 -1 1 366.54 377.95 2.01 o 1 -1 1 6244.32 5894.78 83.07 o 2 -1 1 576.12 627.46 3.59 o 3 -1 1 756.76 780.82 7.30 o 4 -1 1 9.54 8.64 0.21 o 5 -1 1 300.62 303.58 2.68 o 6 -1 1 1.18 0.44 0.49 o -6 0 1 98.80 98.75 1.55 o -5 0 1 237.49 234.41 2.11 o -4 0 1 60.28 59.77 0.64 o -3 0 1 11.41 13.91 0.25 o -2 0 1 3565.44 3580.25 33.00 o -1 0 1 3261.77 3164.13 37.78 o 0 0 1 357.20 356.16 1.89 o 1 0 1 231.19 247.84 1.29 o 2 0 1 221.66 196.18 1.48 o 3 0 1 934.63 953.31 6.74 o 4 0 1 538.24 537.53 4.10 o 5 0 1 63.57 60.24 0.70 o 6 0 1 245.11 240.09 2.34 o -6 1 1 245.34 246.75 3.00 o -5 1 1 0.19 0.78 0.26 o -4 1 1 630.59 622.88 5.15 o -3 1 1 4.65 3.50 0.13 o -2 1 1 894.89 861.64 6.70 o -1 1 1 170.65 167.82 0.88 o 0 1 1 4794.07 4860.46 48.47 o 1 1 1 2551.05 2515.33 28.32 o 2 1 1 471.96 437.62 3.22 o 3 1 1 330.82 344.93 2.98 o 4 1 1 379.54 387.25 3.24 o 5 1 1 4.85 4.38 0.25 o 6 1 1 402.62 412.95 3.34 o -5 2 1 60.16 61.66 0.84 o -4 2 1 23.97 24.57 0.35 o -3 2 1 75.09 69.94 0.72 o -2 2 1 163.19 171.39 1.10 o -1 2 1 970.04 1082.36 4.80 o 0 2 1 2611.76 2531.31 15.28 o 1 2 1 90.72 93.82 0.52 o 2 2 1 139.39 124.24 0.66 o 3 2 1 37.07 35.15 0.34 o 4 2 1 83.25 78.25 0.96 o 5 2 1 347.64 342.14 2.75 o 6 2 1 1.88 3.03 0.35 o -5 3 1 247.50 247.70 2.34 o -4 3 1 289.86 286.11 2.54 o -3 3 1 838.94 820.21 5.62 o -2 3 1 94.73 98.93 0.63 o -1 3 1 1684.50 1659.43 9.64 o 0 3 1 2.09 6.11 0.09 o 1 3 1 211.36 198.11 1.00 o 2 3 1 268.27 289.07 1.43 o 3 3 1 1859.42 1882.16 10.49 o 4 3 1 335.66 349.37 2.31 o 5 3 1 233.59 235.04 2.76 o 6 3 1 9.20 7.84 0.42 o -5 4 1 170.29 167.34 1.98 o -4 4 1 77.00 73.33 0.79 o -3 4 1 402.65 410.58 2.71 o -2 4 1 5.67 4.51 0.17 o -1 4 1 3387.36 3549.18 21.87 o 0 4 1 21.68 24.00 0.20 o 1 4 1 241.02 232.34 1.19 o 2 4 1 134.77 136.46 0.73 o 3 4 1 688.89 673.51 3.99 o 4 4 1 26.75 28.16 0.51 o 5 4 1 365.71 358.04 4.06 o 6 4 1 42.99 40.67 0.82 o -4 5 1 268.32 258.26 2.73 o -3 5 1 0.28 0.70 0.19 o -2 5 1 242.83 220.88 1.42 o -1 5 1 75.54 80.36 0.67 o 0 5 1 1173.32 1184.63 6.06 o 1 5 1 3.45 3.51 0.14 o 2 5 1 327.69 347.20 2.73 o 3 5 1 98.68 90.23 0.71 o 4 5 1 1019.70 1016.30 6.65 o 5 5 1 12.75 11.52 0.73 o 6 5 1 124.34 132.65 1.92 o -4 6 1 128.19 129.95 1.41 o -3 6 1 0.75 1.07 0.25 o -2 6 1 61.12 67.11 0.74 o -1 6 1 5.98 5.14 0.20 o 0 6 1 1435.35 1485.99 9.25 o 1 6 1 302.50 302.66 2.14 o 2 6 1 1010.99 1004.55 6.75 o 3 6 1 17.42 18.16 0.40 o 4 6 1 159.90 156.16 1.54 o 5 6 1 2.80 1.69 0.41 o 6 6 1 86.40 85.35 1.50 o -3 7 1 76.78 74.51 0.96 o -2 7 1 8.21 6.56 0.38 o -1 7 1 202.10 188.20 1.53 o 0 7 1 146.67 148.19 1.38 o 1 7 1 168.00 178.28 1.43 o 2 7 1 3.11 2.70 0.31 o 3 7 1 8.41 7.06 0.33 o 4 7 1 37.25 33.58 0.64 o 5 7 1 260.74 269.76 3.34 o -2 8 1 2.64 2.96 0.45 o -1 8 1 228.35 230.57 1.90 o 0 8 1 35.05 40.46 0.60 o 1 8 1 603.02 598.69 5.77 o 2 8 1 23.02 24.41 0.53 o 3 8 1 217.55 221.19 2.01 o 4 8 1 1.11 0.94 0.41 o 5 8 1 276.21 274.05 4.87 o -1 9 1 161.52 169.37 1.78 o 0 9 1 0.70 1.13 0.33 o 1 9 1 188.74 185.23 2.13 o 2 9 1 332.61 335.07 3.12 o 3 9 1 98.31 99.39 1.22 o 4 9 1 41.56 46.86 2.72 o 0 10 1 234.26 241.50 2.43 o 1 10 1 9.18 10.08 0.52 o 2 10 1 235.39 241.50 2.45 o -2 -9 2 72.34 75.21 1.37 o -1 -9 2 83.48 85.78 1.27 o 0 -9 2 66.97 66.73 1.45 o 1 -9 2 44.69 41.02 1.08 o -4 -8 2 85.89 86.90 2.09 o -3 -8 2 2.22 3.08 0.43 o -2 -8 2 175.63 168.61 1.75 o -1 -8 2 6.94 6.31 0.42 o 0 -8 2 115.32 119.07 1.51 o 1 -8 2 0.71 0.81 0.37 o 2 -8 2 252.79 247.35 4.10 o -4 -7 2 200.93 204.00 2.58 o -3 -7 2 65.55 62.51 0.87 o -2 -7 2 342.08 342.47 2.87 o -1 -7 2 15.31 15.61 0.60 o 0 -7 2 242.93 243.66 2.35 o 1 -7 2 22.33 22.18 0.49 o 2 -7 2 354.25 348.07 3.10 o 3 -7 2 10.35 10.48 0.72 o -5 -6 2 118.28 122.35 2.02 o -4 -6 2 170.57 174.81 2.28 o -3 -6 2 113.98 105.42 1.05 o -2 -6 2 0.32 0.55 0.19 o -1 -6 2 818.24 800.17 5.51 o 0 -6 2 54.77 52.38 0.97 o 1 -6 2 52.60 54.19 0.90 o 2 -6 2 143.94 136.81 1.32 o 3 -6 2 287.90 284.79 3.55 o 4 -6 2 41.67 39.71 0.95 o -5 -5 2 370.48 372.32 5.04 o -4 -5 2 53.42 53.14 1.55 o -3 -5 2 213.05 212.84 1.57 o -2 -5 2 84.65 82.45 0.81 o -1 -5 2 829.94 832.65 5.63 o 0 -5 2 5.46 5.60 0.29 o 1 -5 2 918.61 915.37 5.80 o 2 -5 2 0.45 0.51 0.17 o 3 -5 2 599.52 586.98 4.92 o 4 -5 2 0.16 0.42 0.50 o -5 -4 2 48.22 48.60 2.43 o -4 -4 2 177.23 170.86 4.25 o -3 -4 2 42.19 44.27 0.42 o -2 -4 2 25.54 33.08 0.33 o -1 -4 2 974.13 1052.22 5.94 o 0 -4 2 745.14 735.32 3.97 o 1 -4 2 2.17 3.82 0.16 o 2 -4 2 7.43 7.59 0.20 o 3 -4 2 52.25 48.63 0.50 o 4 -4 2 104.51 106.39 1.16 o 5 -4 2 15.47 18.63 1.36 o -6 -3 2 99.97 96.73 1.98 o -5 -3 2 23.41 23.79 0.59 o -4 -3 2 1582.79 1559.17 15.24 o -3 -3 2 76.15 69.72 0.56 o -2 -3 2 1.40 1.39 0.08 o -1 -3 2 140.48 147.09 0.95 o 0 -3 2 401.27 388.09 2.07 o 1 -3 2 19.46 22.64 0.22 o 2 -3 2 269.84 261.55 1.49 o 3 -3 2 498.20 503.28 2.77 o 4 -3 2 1221.12 1217.42 9.67 o 5 -3 2 1.76 1.87 0.60 o -6 -2 2 259.94 251.14 4.31 o -5 -2 2 10.07 9.95 0.42 o -4 -2 2 295.68 296.87 2.32 o -3 -2 2 116.13 118.00 0.68 o -2 -2 2 1251.39 1255.27 6.13 o -1 -2 2 442.47 476.60 2.59 o 0 -2 2 160.41 148.95 0.88 o 1 -2 2 3533.30 3581.27 23.57 o 2 -2 2 625.54 650.75 3.42 o 3 -2 2 6.20 5.30 0.19 o 4 -2 2 465.99 461.44 3.10 o 5 -2 2 14.89 12.86 0.50 o 6 -2 2 221.02 218.43 2.96 o -6 -1 2 1.23 0.71 0.51 o -5 -1 2 338.00 341.95 2.97 o -4 -1 2 39.09 35.99 0.50 o -3 -1 2 314.49 299.83 2.27 o -2 -1 2 345.55 385.52 1.79 o -1 -1 2 2180.66 2229.36 15.28 o 0 -1 2 1608.20 1598.63 8.74 o 1 -1 2 1719.26 1705.62 13.10 o 2 -1 2 23.92 32.44 0.23 o 3 -1 2 1674.55 1635.23 8.66 o 4 -1 2 29.18 31.61 0.38 o 5 -1 2 345.27 340.03 3.02 o 6 -1 2 6.84 7.22 0.62 o -6 0 2 43.35 40.31 1.28 o -5 0 2 751.90 754.61 7.04 o -4 0 2 2.08 2.99 0.20 o -3 0 2 552.23 558.39 4.53 o -2 0 2 355.45 398.02 2.01 o -1 0 2 625.05 611.59 2.96 o 0 0 2 21.81 22.34 0.23 o 1 0 2 2614.47 2473.24 18.89 o 2 0 2 212.57 228.87 1.44 o 3 0 2 782.48 825.34 5.40 o 4 0 2 21.28 22.07 0.30 o 5 0 2 252.00 262.58 2.17 o 6 0 2 8.35 7.33 0.48 o -5 1 2 17.59 16.78 0.50 o -4 1 2 147.85 154.44 1.32 o -3 1 2 202.81 201.61 1.39 o -2 1 2 81.77 76.08 0.56 o -1 1 2 778.08 817.33 4.36 o 0 1 2 210.63 219.92 1.10 o 1 1 2 1183.59 1150.24 5.62 o 2 1 2 76.01 56.99 0.36 o 3 1 2 5.97 8.97 0.13 o 4 1 2 496.40 479.65 3.69 o 5 1 2 0.36 0.54 0.21 o 6 1 2 276.79 268.02 2.56 o -5 2 2 19.38 16.80 0.47 o -4 2 2 645.73 647.72 4.60 o -3 2 2 220.99 215.47 1.68 o -2 2 2 405.73 371.92 1.83 o -1 2 2 36.46 33.68 0.24 o 0 2 2 1241.62 1215.45 5.64 o 1 2 2 11.72 11.45 0.11 o 2 2 2 817.94 774.39 3.58 o 3 2 2 6.33 7.43 0.12 o 4 2 2 886.30 911.84 8.48 o 5 2 2 67.59 68.78 0.77 o 6 2 2 180.35 176.27 1.63 o -5 3 2 31.55 32.34 0.74 o -4 3 2 34.74 36.71 0.65 o -3 3 2 672.01 662.23 3.44 o -2 3 2 1322.45 1384.78 6.62 o -1 3 2 543.45 562.16 2.88 o 0 3 2 1468.32 1520.62 7.38 o 1 3 2 3058.09 3161.97 14.74 o 2 3 2 64.15 64.92 0.39 o 3 3 2 89.54 84.15 0.49 o 4 3 2 26.50 28.66 0.33 o 5 3 2 212.25 204.63 2.20 o 6 3 2 171.38 182.86 3.12 o -5 4 2 282.27 268.50 3.34 o -4 4 2 19.18 17.64 0.50 o -3 4 2 1672.05 1664.25 10.14 o -2 4 2 119.63 137.62 0.92 o -1 4 2 108.28 90.08 0.53 o 0 4 2 98.47 107.97 0.59 o 1 4 2 660.05 645.21 3.25 o 2 4 2 382.29 380.61 1.81 o 3 4 2 1697.01 1682.37 10.10 o 4 4 2 308.80 312.55 2.07 o 5 4 2 1185.42 1210.99 9.41 o 6 4 2 55.12 55.49 1.13 o -4 5 2 20.90 21.98 0.54 o -3 5 2 74.60 78.58 0.86 o -2 5 2 111.22 98.05 0.82 o -1 5 2 841.35 885.27 4.78 o 0 5 2 74.24 82.70 0.59 o 1 5 2 77.89 75.81 0.57 o 2 5 2 651.32 677.94 3.73 o 3 5 2 1088.58 1073.03 7.60 o 4 5 2 3.82 3.71 0.22 o 5 5 2 111.25 115.43 1.61 o 6 5 2 11.00 10.13 0.62 o -4 6 2 31.19 34.39 0.76 o -3 6 2 7.06 10.48 0.38 o -2 6 2 237.05 225.85 1.62 o -1 6 2 0.28 1.04 0.14 o 0 6 2 544.93 527.33 3.09 o 1 6 2 3.88 3.18 0.27 o 2 6 2 204.08 207.19 1.55 o 3 6 2 1.13 1.01 0.23 o 4 6 2 268.29 268.81 1.93 o 5 6 2 39.91 39.56 2.07 o 6 6 2 148.39 153.24 2.17 o -3 7 2 1.12 0.87 0.34 o -2 7 2 138.09 141.22 1.33 o -1 7 2 39.11 36.33 0.46 o 0 7 2 447.31 466.15 6.25 o 1 7 2 195.05 200.71 1.56 o 2 7 2 420.25 418.56 2.91 o 3 7 2 9.03 8.55 0.56 o 4 7 2 201.84 198.15 1.91 o 5 7 2 22.84 22.03 1.68 o -2 8 2 41.44 45.43 0.84 o -1 8 2 116.66 110.35 1.07 o 0 8 2 20.66 25.02 0.51 o 1 8 2 108.56 108.89 1.07 o 2 8 2 162.28 158.82 1.85 o 3 8 2 192.99 196.91 1.83 o 4 8 2 44.12 42.23 1.52 o 5 8 2 325.31 335.73 4.03 o -2 9 2 13.66 13.48 0.90 o -1 9 2 270.51 272.91 2.62 o 0 9 2 28.12 27.26 0.57 o 1 9 2 451.33 454.70 3.74 o 2 9 2 28.99 30.76 0.93 o 3 9 2 321.30 317.49 2.98 o 4 9 2 4.66 5.66 0.56 o 0 10 2 0.58 0.60 0.41 o 1 10 2 27.45 26.49 0.83 o 2 10 2 116.07 115.36 1.74 o 3 10 2 23.16 23.54 0.74 o -1 -9 3 157.60 152.71 2.24 o -3 -8 3 165.96 162.03 2.11 o -2 -8 3 0.30 0.31 0.37 o -1 -8 3 133.96 138.72 1.71 o 0 -8 3 51.18 49.11 0.92 o 1 -8 3 70.60 72.04 1.79 o 2 -8 3 1.25 2.44 0.49 o -4 -7 3 248.47 251.82 3.74 o -3 -7 3 116.05 116.05 1.29 o -2 -7 3 316.63 310.17 2.67 o -1 -7 3 131.60 124.77 1.48 o 0 -7 3 380.00 377.44 3.62 o 1 -7 3 60.24 58.68 1.08 o 2 -7 3 165.47 167.17 2.00 o 3 -7 3 5.32 5.47 0.58 o -4 -6 3 106.31 109.36 1.89 o -3 -6 3 32.71 32.35 1.43 o -2 -6 3 370.32 368.79 3.13 o -1 -6 3 18.03 16.34 0.50 o 0 -6 3 247.30 247.59 2.18 o 1 -6 3 13.09 13.24 0.61 o 2 -6 3 1111.84 1085.91 8.99 o 3 -6 3 23.86 23.55 0.74 o 4 -6 3 89.62 85.56 1.50 o -5 -5 3 23.63 25.28 2.60 o -4 -5 3 9.53 10.31 0.54 o -3 -5 3 146.73 141.71 1.25 o -2 -5 3 3.31 2.63 0.24 o -1 -5 3 1001.05 966.27 6.96 o 0 -5 3 14.29 13.73 0.43 o 1 -5 3 161.53 164.15 1.52 o 2 -5 3 288.83 285.85 2.40 o 3 -5 3 31.07 34.87 0.68 o 4 -5 3 0.46 0.43 0.38 o -5 -4 3 239.71 236.95 7.26 o -4 -4 3 18.89 18.72 0.46 o -3 -4 3 646.47 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3 9 24.22 21.65 0.45 o 2 3 9 4.46 5.80 0.25 o 3 3 9 12.43 12.24 0.36 o 4 3 9 54.51 52.01 0.68 o 5 3 9 16.18 18.60 0.52 o -3 4 9 0.65 0.93 0.47 o -2 4 9 578.83 591.32 6.62 o -1 4 9 109.22 110.54 1.31 o 0 4 9 197.34 197.66 1.72 o 1 4 9 2.25 2.65 0.24 o 2 4 9 269.01 269.07 2.85 o 3 4 9 38.15 36.51 0.59 o 4 4 9 186.80 184.06 1.64 o 5 4 9 0.16 0.20 0.37 o -2 5 9 122.28 127.56 1.87 o -1 5 9 31.16 31.58 0.70 o 0 5 9 134.07 133.57 1.34 o 1 5 9 31.58 35.16 0.72 o 2 5 9 470.08 467.33 3.18 o 3 5 9 246.07 240.83 1.83 o 4 5 9 11.84 11.59 0.39 o 5 5 9 102.08 101.29 2.03 o -2 6 9 0.56 1.23 0.48 o -1 6 9 617.83 619.51 6.01 o 0 6 9 3.71 4.29 0.32 o 1 6 9 70.61 73.02 1.11 o 2 6 9 13.83 15.66 0.34 o 3 6 9 328.03 330.38 2.65 o 4 6 9 0.22 0.25 0.31 o 5 6 9 168.17 166.15 2.01 o -1 7 9 90.44 89.12 2.57 o 0 7 9 2.06 1.35 0.36 o 1 7 9 23.27 22.13 0.52 o 2 7 9 3.96 3.35 0.35 o 3 7 9 141.83 140.92 1.38 o 4 7 9 0.78 0.80 0.30 o 0 8 9 166.48 158.69 2.26 o 1 8 9 10.92 10.41 0.48 o 2 8 9 123.26 126.04 1.28 o 3 8 9 2.33 1.72 0.49 o 4 8 9 114.17 114.52 1.25 o 1 9 9 1.92 1.94 0.39 o 2 9 9 268.35 266.16 3.83 o 3 9 9 0.19 0.07 0.39 o -1 -3 10 23.36 24.70 0.75 o 0 -3 10 1.78 1.91 0.53 o 1 -3 10 117.31 124.80 2.00 o 2 -3 10 4.74 5.67 0.54 o -2 -2 10 28.79 28.46 0.74 o -1 -2 10 438.57 435.64 3.92 o 0 -2 10 2.41 2.53 0.37 o 1 -2 10 101.72 101.73 1.42 o 2 -2 10 0.49 2.02 0.49 o 3 -2 10 182.13 185.20 2.28 o -2 -1 10 9.90 8.41 0.48 o -1 -1 10 134.93 137.00 1.48 o 0 -1 10 64.70 64.83 0.98 o 1 -1 10 61.53 59.27 0.97 o 2 -1 10 92.57 93.68 1.34 o 3 -1 10 6.07 5.99 0.48 o 4 -1 10 64.39 64.72 1.19 o -2 0 10 187.81 186.01 2.13 o -1 0 10 4.37 4.88 0.50 o 0 0 10 193.07 198.70 2.23 o 1 0 10 0.71 1.20 0.26 o 2 0 10 303.72 302.17 3.24 o 3 0 10 2.78 2.49 0.39 o 4 0 10 379.14 389.20 4.21 o -2 1 10 140.78 149.57 2.04 o -1 1 10 42.32 40.62 1.15 o 0 1 10 43.20 46.11 1.01 o 1 1 10 19.58 20.52 0.75 o 2 1 10 116.35 115.66 1.70 o 3 1 10 101.95 108.41 1.28 o 4 1 10 102.53 102.50 1.48 o -2 2 10 0.50 0.68 0.40 o -1 2 10 101.02 99.86 2.26 o 0 2 10 24.94 22.63 0.60 o 1 2 10 389.24 394.29 2.84 o 2 2 10 195.99 196.34 2.54 o 3 2 10 157.59 156.36 1.50 o 4 2 10 2.02 1.63 0.34 o 5 2 10 51.02 49.45 0.90 o -2 3 10 24.57 24.70 0.78 o -1 3 10 142.24 142.43 4.47 o 0 3 10 11.18 9.74 0.70 o 1 3 10 132.41 133.23 1.20 o 2 3 10 25.28 28.40 0.55 o 3 3 10 147.42 147.96 1.31 o 4 3 10 5.78 7.28 0.41 o 5 3 10 185.94 185.21 4.15 o -2 4 10 51.03 50.54 1.09 o -1 4 10 1.43 1.91 0.35 o 0 4 10 92.78 94.75 2.38 o 1 4 10 109.85 103.42 1.00 o 2 4 10 286.22 285.02 2.03 o 3 4 10 3.38 3.90 0.50 o 4 4 10 225.47 231.54 2.09 o 5 4 10 49.82 53.97 1.00 o -2 5 10 201.79 197.36 2.69 o -1 5 10 63.78 63.39 1.64 o 0 5 10 558.85 557.21 5.10 o 1 5 10 101.89 101.43 1.02 o 2 5 10 134.44 133.04 1.26 o 3 5 10 7.47 7.21 0.33 o 4 5 10 249.47 258.56 2.50 o 5 5 10 4.99 5.17 0.58 o -1 6 10 5.24 4.97 0.53 o 0 6 10 43.41 41.32 0.82 o 1 6 10 15.23 17.32 0.48 o 2 6 10 36.72 33.40 0.55 o 3 6 10 124.28 123.99 1.25 o 4 6 10 5.94 5.70 0.41 o 0 7 10 26.61 27.05 0.76 o 1 7 10 127.80 133.00 1.48 o 2 7 10 5.85 8.05 0.36 o 3 7 10 171.52 165.03 1.77 o 4 7 10 5.66 3.99 0.37 o 1 8 10 57.31 56.99 1.12 o 2 8 10 8.06 8.70 0.53 o 3 8 10 161.69 159.05 1.76 o 0 -2 11 17.77 14.65 1.17 o 1 -2 11 119.51 118.62 1.96 o -1 -1 11 202.36 201.85 2.29 o 0 -1 11 49.90 50.77 1.14 o 1 -1 11 314.63 320.43 4.06 o 2 -1 11 2.56 2.65 0.57 o 3 -1 11 114.50 116.49 1.68 o -1 0 11 43.06 46.43 0.78 o 0 0 11 10.23 10.65 0.48 o 1 0 11 39.01 40.67 1.00 o 2 0 11 98.89 102.16 1.45 o 3 0 11 45.89 45.20 0.96 o -1 1 11 2.54 2.62 0.34 o 0 1 11 113.40 116.62 1.31 o 1 1 11 19.73 19.73 0.73 o 2 1 11 593.05 606.32 6.11 o 3 1 11 65.22 66.71 1.01 o 4 1 11 64.30 63.84 1.15 o -1 2 11 42.80 41.44 1.39 o 0 2 11 4.05 4.96 0.34 o 1 2 11 1.33 2.12 0.29 o 2 2 11 92.69 97.39 1.20 o 3 2 11 2.36 1.98 0.35 o 4 2 11 116.64 112.35 1.18 o -1 3 11 166.54 168.36 1.95 o 0 3 11 10.72 10.51 0.47 o 1 3 11 174.40 178.70 1.73 o 2 3 11 53.62 52.66 0.83 o 3 3 11 478.37 495.51 3.77 o 4 3 11 26.75 26.13 0.55 o -1 4 11 179.11 180.31 4.36 o 0 4 11 2.88 3.33 0.55 o 1 4 11 393.65 395.67 3.94 o 2 4 11 0.75 0.78 0.39 o 3 4 11 235.12 242.72 2.34 o 4 4 11 12.87 11.65 0.51 o -1 5 11 51.56 49.57 1.68 o 0 5 11 105.10 109.69 2.18 o 1 5 11 14.40 12.71 0.54 o 2 5 11 93.71 100.03 1.04 o 3 5 11 0.20 0.23 0.36 o 4 5 11 151.40 147.44 1.65 o 0 6 11 115.80 115.09 1.54 o 1 6 11 35.90 40.43 0.96 o 2 6 11 126.59 131.05 1.30 o 3 6 11 5.54 5.71 0.47 o 4 6 11 99.50 97.26 2.13 o 1 7 11 32.11 30.50 0.77 o 2 7 11 4.88 5.17 0.41 o 3 7 11 74.76 78.49 1.11 o 1 0 12 289.35 285.71 8.63 o 2 0 12 0.10 0.43 0.54 o 0 1 12 19.04 18.83 0.80 o 1 1 12 68.40 68.48 2.40 o 2 1 12 1.63 2.06 0.53 o 0 2 12 107.82 103.60 1.97 o 1 2 12 33.40 32.28 0.96 o 2 2 12 233.48 233.30 2.66 o 3 2 12 20.53 19.42 0.56 o 0 3 12 36.50 36.86 0.78 o 1 3 12 15.12 14.98 0.88 o 2 3 12 320.76 326.96 3.51 o 3 3 12 2.08 0.88 0.44 o 0 4 12 10.74 10.72 0.82 o 1 4 12 227.81 219.82 5.56 o 2 4 12 0.14 -0.41 0.41 o 3 4 12 154.41 152.06 2.00 o 1 5 12 212.64 213.36 2.38 o 2 5 12 20.68 21.49 1.02 o 3 5 12 70.06 65.68 1.15 o 2 6 12 39.36 35.80 0.98 o