Acta Crystallographica Section C

Crystal Structure Communications

Volume 66, Part 7 (July 2010)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The structure of tris(4-bromophenyl)aminium hexachloridoantimonate. Displacement ellipsoids are drawn at the 50% probability level. For clarity, H atoms have been omitted. See Quiroz-Guzman & Brown [Acta Cryst. (2010), C66, m171-m173].

inorganic compounds


 

[HTML version][PDF version][CIF][3d view][Structure Factors]  [Buy article online]

Acta Cryst. (2010). C66, i71-i74  [ doi:10.1107/S0108270110017695 ]

A novel In3O16 fragment in Cs3In3(PO4)4

I. V. Zatovsky, V. N. Baumer, N. Yu. Strutynska, N. S. Slobodyanik and O. V. Shishkin

Synopsis: Tricaesium triindium tetraphosphate, Cs3In3(PO4)4, features a three-dimensional structure composed of an In3O16 fragment of corner-sharing InO6 polyhedra interlinked by PO4 groups into an anionic network, providing tunnels along c where two distinct Cs+ cations reside. The structure is closely related to that of K3In3(PO4)4, with the main difference being in the geometry of the In3O16 fragments due to the different coordination requirements of Cs and K.

Formula: Cs3In3(PO4)4

Online 17 June 2010


 

[HTML version][PDF version][CIF][3d view][Structure Factors]  [Buy article online]

Acta Cryst. (2010). C66, i75-i78  [ doi:10.1107/S0108270110017038 ]

Cs6Nb4Se22 and K12Nb6Se35.3: two new compounds containing the M4Q22 building block

J. W. Krizan, S. H. Pulido, S. E. Wehrhan and B. C. Chan

Synopsis: Cs6Nb4Se22 contains two Nb2Se11 building blocks linked by an Se-Se bond to form isolated Nb4Se22 tetrameric building blocks surrounded by caesium ions. K12Nb6Se35.3 contains similar Nb4Se22 tetramers that are linked by an Se-Se-Se unit to an Nb2Se11 dimer to form one-dimensional anionic chains surrounded by potassium ions.

Formula: Cs6Nb4Se22 and K12Nb6Se35.30

Online 17 June 2010


 

[HTML version][PDF version][CIF][3d view][Structure Factors]  [Buy article online]

Acta Cryst. (2010). C66, i79-i81  [ doi:10.1107/S0108270110022869 ]

(NH4)2WTe2O8 at 5.09 GPa: a single-crystal study using synchrotron radiation

A. Grzechnik, P. S. Halasyamani, J.-H. Kim and K. Friese

Synopsis: The crystal structure of (NH4)2WTe2O8 was determined at 5.09 GPa using single-crystal X-ray diffraction in a diamond-anvil cell. No phase transition was observed up to 7.16 GPa. However, a full structure determination at 5.09 GPa shows that the coordination number of one of the two non-equivalent Te atoms has decreased from four to three.

Formula: (NH4)2WTe2O8

Online 17 June 2010


 

[HTML version][PDF version][CIF][3d view][Structure Factors]  [Buy article online]

Acta Cryst. (2010). C66, i82-i84  [ doi:10.1107/S0108270110021670 ]

K2ScSn(AsO4)3: an arsenate-containing langbeinite

W. T. A. Harrison

Synopsis: The title compound is the first arsenate-containing langbeinite to be structurally characterized: the ScIII and SnIV cations show slight segregation over the two octahedral sites.

Formula: K2ScSn(AsO4)3

Online 17 June 2010


metal-organic compounds


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m171-m173  [ doi:10.1107/S0108270110019748 ]

Tris(4-bromophenyl)aminium hexachloridoantimonate (`Magic Blue'): a strong oxidant with low inner-sphere reorganization

M. Quiroz-Guzman and S. N. Brown

Formula: (C18H12Br3N)[SbCl6] and C18H12Br3N

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m174-m176  [ doi:10.1107/S0108270110020585 ]

Diamminesilver(I) bis(2-amino-5-nitrobenzoato-[kappa]2O1,O1')silver(I): a two-dimensional supramolecular sheet with a short intersheet distance containing a rare four-coordinate planar silver(I) centre

D. Sun, N. Zhang, R.-B. Huang and L.-S. Zheng

Formula: [Ag(NH3)2][Ag(C7H5N2O4)2]

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m177-m179  [ doi:10.1107/S0108270110018238 ]

Synthesis and molecular structure of Cr(salen)([mu]-N)RhCl(COD): the first example of a heterobimetallic nitride-bridged complex containing chromium

J. Vibenholt, M. Magnussen, C. Anthon and J. Bendix

Formula: [CrRh(C16H14N2O2)ClN(C8H12)]

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m180-m183  [ doi:10.1107/S0108270110021050 ]

Cadmium(II) thio- and selenocyanate complexes of 3,3'-bis(1,2,4-triazol-4-yl)-1,1'-biadamantane, a ligand designed with an `extended nanodiamond' aliphatic platform

G. A. Senchyk, A. B. Lysenko, E. B. Rusanov, A. N. Chernega and K. V. Domasevitch

Formula: [Cd(C24H32N6)2(H2O)2](NCS)2·2H2O and [Cd(C24H32N6)2(H2O)2](NCSe)2·2H2O

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m184-m187  [ doi:10.1107/S0108270110020433 ]

Poly[diaquabis([mu]3-2,2-dimethylpropanedioato)calcium(II)copper(II)]

M.-L. Guo and F.-Q. Wang

Formula: [CaCu(C5H6O4)2(H2O)2]

Online 10 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m188-m190  [ doi:10.1107/S0108270110022201 ]

Propane-1,3-diaminium tetrachloridozincate(II) 18-crown-6 clathrate

M. M. Zhao and Z. R. Qu

Formula: (C3H12N2)[ZnCl4]·C12H24O6

Online 17 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m191-m193  [ doi:10.1107/S0108270110023176 ]

Chlorido([eta]5-cyclopentadienyl)bis(dimethylamido)titanium, [TiCl([eta]5-C5H5)(NMe2)2]

B. M. Chapin, L. D. Hughs, J. A. Golen, A. L. Rheingold and A. R. Johnson

Formula: [Ti(C5H5)(C2H6N)2Cl]

Online 24 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, m194-m196  [ doi:10.1107/S0108270110021165 ]

Poly[([mu]6-rac-cis-cyclohexane-1,2-dicarboxylato)strontium]

K. A. Robertson and W. T. A. Harrison

Formula: [Sr(C8H10O4)]

Online 24 June 2010


organic compounds


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o321-o323  [ doi:10.1107/S0108270110019888 ]

Methyl [beta]-D-fructopyranoside

T. Allscher and P. Klüfers

Formula: C7H14O6

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o324-o328  [ doi:10.1107/S0108270110014150 ]

Charge-assisted hydrogen-bonded supramolecular networks in acetoguanaminium hydrogen phthalate, acetoguanaminium hydrogen maleate and acetoguanaminium 3-hydroxypicolinate monohydrate

K. Thanigaimani, P. Devi, P. T. Muthiah, D. E. Lynch and R. J. Butcher

Formula: C4H8N5+·C8H5O4-, C4H8N5+·C4H3O4- and C4H8N5+·C6H4NO3-·H2O

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o329-o333  [ doi:10.1107/S0108270110020317 ]

Lamivudine hemihydrate

A. Bhattacharya, B. N. Roy, G. P. Singh, D. Srivastava and A. K. Mukherjee

Formula: C8H11N3O3S·0.5H2O

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o334-o336  [ doi:10.1107/S0108270110020858 ]

25-Allyloxy-5,11,17,23-tetra-tert-butyl-26,27,28-trihydroxycalix[4]arene chloroform disolvate

T. Gruber, F. Eissmann, W. Seichter and E. Weber

Formula: C47H60O4·2CHCl3

Online 5 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o337-o340  [ doi:10.1107/S0108270110020846 ]

Two-dimensional networks in 2-methylanilinium picrate and 2,5-dichloroanilinium picrate

G.-X. Meng, H.-L. Yang, C.-X. Cheng and X.-T. Huang

Formula: C7H10N+·C6H2N3O7- and C6H6Cl2N+·C6H2N3O7-

Online 8 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Powder data file][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o341-o344  [ doi:10.1107/S0108270110019190 ]

Ezetimibe anhydrate, determined from laboratory powder diffraction data

J. Brüning, E. Alig and M. U. Schmidt

Formula: C24H21F2NO3

Online 8 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o345-o348  [ doi:10.1107/S0108270110020597 ]

Phenyl-ring rotational disorder in the two-dimensional hydrogen-bonded structure of the 1:1 proton-transfer salt of the diazo-dye precursor 4-(phenyldiazenyl)aniline (aniline yellow) with L-tartaric acid

G. Smith, U. D. Wermuth and D. J. Young

Formula: C12H12N3+·C4H5O6-

Online 8 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o349-o352  [ doi:10.1107/S0108270110020895 ]

L-Isoleucyl-L-asparagine 1.094-hydrate: a hybrid hydrogen-bonding pattern

C. H. Görbitz and P. H. Backe

Formula: C10H19N3O4·1.094H2O

Online 10 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o353-o355  [ doi:10.1107/S0108270110020688 ]

Ethyl 3-[1-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorin-2-yl)propan-2-ylidene]carbazate: a combined X-ray and density functional theory (DFT) study

Y. Arfaoui, S. Kouass, N. Salah, A. Ben Akacha and A. Guesmi

Formula: C11H21N2O5P

Online 10 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o356-o360  [ doi:10.1107/S0108270110021736 ]

Cocrystals of 2,3,5,6-tetrafluorobenzene-1,4-diol with diaza aromatic compounds

A. Czapik and M. Gdaniec

Formula: C6H2F4O2·C4H4N2, C6H2F4O2·C8H6N2 and C6H2F4O2·2C12H8N2

Online 11 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o361-o363  [ doi:10.1107/S0108270110022092 ]

Influence of 1,4-dioxane solvent inclusion on the crystal structure of 5,5'-diphenyl-2,2'-(p-phenylene)di-1,3-oxazole (POPOP)

D. Schindler, M. Felsmann and E. Weber

Formula: C24H16N2O2 and C24H16N2O2·2C4H8O2

Online 23 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o364-o368  [ doi:10.1107/S0108270110019827 ]

Structural comparison of three N-(4-halogenophenyl)-N'-[1-(2-pyridyl)ethylidene]hydrazine hydrochlorides

J. Heilmann-Brohl, M. Wagner, H.-W. Lerner and M. Bolte

Formula: C13H13ClN3+·Cl-·CH3OH, C13H13FN3+·Cl- and C13H13FN3+·Cl-·2CH3OH

Online 23 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o369-o373  [ doi:10.1107/S0108270110023188 ]

N,N'-Diethyl-4-nitrobenzene-1,3-diamine, 2,6-bis(ethylamino)-3-nitrobenzonitrile and bis(4-ethylamino-3-nitrophenyl) sulfone

T. J. Payne, C. R. Thurman, H. Yu, Q. Sun, D. K. Mohanty, P. J. Squattrito, M.-R. Giolando, C. R. Brue and K. Kirschbaum

Formula: C10H15N3O2, C11H14N4O2 and C16H18N4O6S

Online 23 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o374-o380  [ doi:10.1107/S0108270110022328 ]

Low-dimensional hydrogen-bonded structures in the 1:1 and 1:2 proton-transfer compounds of 4,5-dichlorophthalic acid with the aliphatic Lewis bases triethylamine, diethylamine, n-butylamine and piperidine

G. Smith and U. D. Wermuth

Formula: C6H16N+·C8H3Cl2O4-, C4H12N+·C8H3Cl2O4-, 2C4H12N+·C8H2Cl2O42-·H2O and 2C5H12N+·C8H2Cl2O42-·H2O

Online 23 June 2010


contents scheme thumbnail

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2010). C66, o381-o384  [ doi:10.1107/S0108270110024261 ]

Conformational disorder in 4-(5,5'-dibromo-2'-chloro-4,4'-bipyridyl-2-yl)benzaldehyde: role of [pi]-[pi] and halogen interactions

M. Abboud, A. Kadimi, V. Mamane and E. Aubert

Formula: C17H9Br2ClN2O

Online 29 June 2010


addenda and errata


 

[HTML version][PDF version]  [Open access]

Acta Cryst. (2010). C66, e13  [ doi:10.1107/S0108270110025035 ]

Two isomorphous crotonatolanthanide complexes: tetra-[mu]-but-2-enoato-bis[diaqua(but-2-enoato)Ln]-2,6-diaminopurine (1/2) (Ln = Dy and Ho). Corrigendum

A. M. Atria, A. Astete, M. T. Garland and R. Baggio

Synopsis: Corrigendum to Acta Cryst. (2009), C65, m411-m414.

Formula: [Dy2(C4H5O2)6(H2O)4]·2C5H6N6 and [Ho2(C4H5O2)6(H2O)4]·2C5H6N6

Online 29 June 2010


Copyright © International Union of Crystallography
IUCr Webmaster