Crystal Structure Communications

 

Acta Cryst. (2011). C67, i13-i16  [ doi:10.1107/S0108270111002137 ]

La_4.27Mg_2.89Zn₃₀, a new structure type with strong positional disorder

V. Pavlyuk, E. Rozycka-Sokolowska and B. Marciniak

Synopsis: La_4.27Mg_2.89Zn₃₀, an intermetallic compound, is a new structure type which crystallizes in the hexagonal space group P6₃/mmc. The structure is an intergrowth of fragments of the CaCu₅ and Th₂Ni₁₇ types. Strong positional disorder is observed along the six- and threefold axes.

Formula: La_4.27Mg_2.89Zn₃₀

Online 4 February 2011

 

Acta Cryst. (2011). C67, i17-i20  [ doi:10.1107/S0108270110054521 ]

Structure and ³¹P NMR spectroscopy of a new phosphate, Na₈Ca_1.5Mg_12.5(PO₄)₁₂

H. Jerbi, M. Hidouri, M. Rzeigui and M. Ben Amara

Synopsis: The novel structure of Na₈Ca_1.5Mg_12.5(PO₄)₁₂ consists of MgO_x (x = 5 and 6) polyhedra and MO₇ (M = Mg or Na) octahedra linked directly through common corners or edges to form a rigid three-dimensional skeleton, reinforced by corner-sharing between identical Mg₁₂MO₄₈ units.

Formula: Na₈Ca_1.5Mg_12.5(PO₄)₁₂

Online 4 February 2011

 

Acta Cryst. (2011). C67, i21-i23  [ doi:10.1107/S0108270110054156 ]

Copper(II) manganese(II) orthophosphate, Cu_0.5Mn_2.5(PO₄)₂

A. D. Bond, S. P. V. Foghmoes and T. E. Warner

Synopsis: The copper-manganese phosphate solid solution Cu_0.5Mn_2.5(PO₄)₂ was prepared by a reaction between its constituent oxides at 1223 K under argon. The compound has a graftonite-type structure, viz. (Mn,Fe,Ca,Mg)₃(PO₄)₂, with Cu^II located in one of three distinct metal cation sites.

Formula: Cu_0.5Mn_2.5(PO₄)₂

Online 22 February 2011

 

Acta Cryst. (2011). C67, i24-i26  [ doi:10.1107/S0108270111005889 ]

Disordered La₃Cu_4.88Se₇

L. D. Gulay, M. Daszkiewicz, O. M. Strok and A. Pietraszko

Synopsis: The crystal structure of La₃Cu_4.88Se₇ contains edge-sharing [LaSe₆] and [LaSe₇] polyhedra, which are surrounded by copper ions. The five positions for copper determine an ionic diffusion pathway.

Formula: La₃Cu_4.88Se₇

Online 22 February 2011

 

Acta Cryst. (2011). C67, m65-m68  [ doi:10.1107/S0108270110053497 ]

Hexaaquacobalt(II) and hexaaquanickel(II) bis(-pyridine-2,6-dicarboxylato)bis[(pyridine-2,6-dicarboxylato)bismuthate(III)] dihydrate

V. Stavila, I. Bulimestru, A. Gulea, A. C. Colson and K. H. Whitmire

Formula: [Co(H₂O)₆][Bi₂(C₇H₄NO₄)₄]·2H₂O and [Ni(H₂O)₆][Bi₂(C₇H₄NO₄)₄]·2H₂O

Online 5 February 2011

 

Acta Cryst. (2011). C67, m69-m72  [ doi:10.1107/S0108270111004227 ]

Supramolecular architectures of two novel organic-inorganic hybrid materials containing identical monomeric uranyl units

S. J. Jenniefer and P. T. Muthiah

Formula: (C₁₀H₁₀N₂)_0.5[U(C₅H₂ClO₂S)₃O₂]·H₂O and (C₁₂H₁₄N₂)_0.5[U(C₅H₂ClO₂S)₃O₂]·H₂O

Online 12 February 2011

    

Acta Cryst. (2011). C67, m73-m76  [ doi:10.1107/S0108270111005105 ]

A three-dimensional tin(II) phosphonatobenzenesulfonate with Sn₄O₁₂ clusters

P. Maniam and N. Stock

Formula: [Sn₂(C₆H₄O₆PS)(OH)]

Online 16 February 2011

 

Acta Cryst. (2011). C67, m77-m80  [ doi:10.1107/S0108270111005403 ]

Poly[[tetra-₃-acetato-hexa-₂-acetato-diaqua-₂-oxalato-tetrapraseodymium(III)] dihydrate]

K. Gutkowski, E. Freire and R. Baggio

Formula: [Pr₄(C₂H₃O₂)₁₀(C₂O₄)(H₂O)₂]·2H₂O

Online 18 February 2011

 

Acta Cryst. (2011). C67, o85-o88  [ doi:10.1107/S0108270111002836 ]

Novel hydrazone derivatives of 7-hydroxy-3',3'-dimethyl-3'H-spiro[chromene-2,1'-isobenzofuran]-8-carbaldehyde

A. Bulanov, I. N. Shcherbakov, L. D. Popov, E. Y. Shasheva, P. A. Belikov and Z. A. Starikova

Formula: C₂₇H₂₅N₃O₃S and C₂₇H₂₄N₂O₄·C₃H₆O

Online 4 February 2011

 

Acta Cryst. (2011). C67, o89-o91  [ doi:10.1107/S0108270111003064 ]

A sulfur(II) complex of a dithioimidodiphosphinate

J. S. Ritch and T. Chivers

Formula: C₃₂H₇₂N₂P₄S₅·C₇H₈

Online 4 February 2011

 

Acta Cryst. (2011). C67, o92-o99  [ doi:10.1107/S0108270111003714 ]

Six two- and three-component ammonium carboxylate salt structures with a ladder-type hydrogen-bonding motif, three incorporating neutral carboxylic acid molecules

A. Lemmerer

Formula: C₃H₁₀N⁺·C₇H₅O₂^-, C₆H₁₀N⁺·C₉H₉O₂^-, C₈H₁₂N⁺·C₁₁H₇O₂^-, C₆H₁₀N⁺·C₇H₅O₂^-·C₇H₆O₂, C₃H₈N⁺·C₇H₅O₂^-·C₇H₆O₂ and 2C₃H₈N⁺·C₈H₁₀O₄^2-·C₈H₁₂O₄

Online 8 February 2011

 

Acta Cryst. (2011). C67, o100-o103  [ doi:10.1107/S0108270110053357 ]

Optically active diaryl tetrahydroisoquinoline derivatives

T. Naicker, T. Govender, H. G. Kruger and G. E. M. Maguire

Formula: C₃₁H₃₁NO₃ and C₄₀H₄₃NO₃Si

Online 8 February 2011

 

Acta Cryst. (2011). C67, o104-o106  [ doi:10.1107/S0108270111004069 ]

Cyclopentanone and cyclobutanone

D. S. Yufit and J. A. K. Howard

Formula: C₅H₈O and C₄H₆O

Online 9 February 2011

 

Acta Cryst. (2011). C67, o107-o110  [ doi:10.1107/S0108270111004951 ]

4-Aminopyridinium 2-(anthracen-9-yl)-3-oxo-3H-inden-1-olate monohydrate

G. J. Gainsford, M. Ashraf, M. D. H. Bhuiyan and A. J. Kay

Formula: 2C₅H₇N₂⁺·2C₂₃H₁₃O₂^-·H₂O

Online 11 February 2011

 

Acta Cryst. (2011). C67, o111-o114  [ doi:10.1107/S0108270111005087 ]

1,N⁶-Etheno-2'-deoxytubercidin hemihydrate

F. Seela, P. Ding, P. Leonard, H. Eickmeier and H. Reuter

Formula: 2C₁₃H₁₄N₄O₃·H₂O

Online 16 February 2011

 

Acta Cryst. (2011). C67, o115-o119  [ doi:10.1107/S0108270111005191 ]

Multiple hydrogen bonds in cytosinium zoledronate trihydrate

B. Sridhar and K. Ravikumar

Formula: C₄H₆N₃O⁺·C₅H₉N₂O₇P₂^-·3H₂O

Online 16 February 2011

 

Acta Cryst. (2011). C67, o120-o124  [ doi:10.1107/S0108270111005488 ]

Intermolecular interactions, disorder and twinning in ciprofloxacin-2,2-difluoroethanol (2/3) and ciprofloxacin-water (3/14.5)

F. P. A. Fabbiani, J.-B. Arlin, G. Buth, B. Dittrich, A. J. Florence, R. Herbst-Irmer and H. Sowa

Formula: 2C₁₇H₁₈FN₃O₃·3C₂H₄F₂O and 3C₁₇H₁₈FN₃O₃·14.5H₂O

Online 18 February 2011

 

Acta Cryst. (2011). C67, o125-o128  [ doi:10.1107/S0108270111005816 ]

(+)-Geodin from Aspergillus terreus

M. H. Rønnest, M. T. Nielsen, B. Leber, U. H. Mortensen, A. Krämer, M. H. Clausen, T. O. Larsen and P. Harris

Formula: C₁₇H₁₂Cl₂O₇

Online 23 February 2011