Acta Crystallographica Section C

Crystal Structure Communications

Volume 68, Part 9 (September 2012)


	Cover illustration: The structure of benzoyl(hydroxyimino)acetonitrile-18-crown-6-water (2/1/4). Displacement ellipsoids are drawn at the 40% probability level. N and O atoms are shaded and the dashed lines indicate hydrogen bonding. See Ponomarova & Domasevitch [Acta Cryst. (2012), C68, o359-o361].

metal-organic compounds
organic compounds

metal-organic compounds

Acta Cryst. (2012). C68, m235-m237 [ doi:10.1107/S0108270112033045 ]

A two-dimensional coordination polymer containing a two-dimensional zinc-carboxylate layer constructed from helical chains: poly[(₄-benzene-1,2-dicarboxylato)zinc(II)]

W.-L. Xiong, Q.-Y. Liu, N. Zhang and L. Wang

Formula: [Zn(C₈H₄O₄)]

Online 1 August 2012

Acta Cryst. (2012). C68, m238-m241 [ doi:10.1107/S0108270112032192 ]

rac-1-[(2-Methoxyethyl)sulfanyl]-2-[(2-methoxyethyl)sulfinyl]benzene and its PdCl₂ complex

J. Traeger, A. Kelling, U. Schilde and H.-J. Holdt

Formula: C₁₂H₁₈O₃S₂ and [PdCl₂(C₁₂H₁₈O₃S₂)]

Online 1 August 2012

Acta Cryst. (2012). C68, m242-m245 [ doi:10.1107/S0108270112031368 ]

Binary salt of a palladium(II) complex with (phosphonomethyl)phosphonic (medronic) acid comprising `handbell-like' [Pd{-CH₂(PO₃)₂}]₃ units

A. A. Babaryk, A. N. Kozachkova, N. V. Tsaryk, A. V. Dudko and V. I. Pekhnyo

Formula: K₂[Ni(H₂O)₆]₂[Pd₃(CH₂O₆P₂)₃]·6H₂O

Online 1 August 2012

Acta Cryst. (2012). C68, m246-m250 [ doi:10.1107/S0108270112031885 ]

1,1'-Methylenedipyridinium tetrachloridocuprate(II) and bis[tetrachloridoaurate(III)] hybrid salts by X-ray powder diffraction

M. Al-Ktaifani and M. Rukiah

Formula: (C₁₁H₁₂N₂)[CuCl₄] and (C₁₁H₁₂N₂)[AuCl₄]₂

Online 1 August 2012

Acta Cryst. (2012). C68, m251-m254 [ doi:10.1107/S0108270112033318 ]

The weakly coordinating perchlorate group in bis(N,N'-dimethylethylenediamine-²N,N')bis(perchlorato-O)copper(II) studied at 100, 250 and 400 K

S. Schnitzler, M.-D. Serb and U. Englert

Formula: [Cu(ClO₄)₂(C₄H₁₂N₂)₂]

Online 1 August 2012

Acta Cryst. (2012). C68, m255-m258 [ doi:10.1107/S0108270112033616 ]

-4,4'-Bipyridine-²N:N'-bis[tetraaqua(4,4'-bipyridine-N)dimanganese(II)] bis(4-aminobenzoate) bis(perchlorate)-4,4'-bipyridine-water (1/2/4): a supramolecular system constructed by - and hydrogen-bond interactions

J. Wang, J. Gao and W. Zhao

Formula: [Mn₂(C₁₀H₈N₂)₃(H₂O)₈](C₇H₆NO₂)₂(ClO₄)₂·2C₁₀H₈N₂·4H₂O

Online 1 August 2012

Acta Cryst. (2012). C68, m259-m264 [ doi:10.1107/S0108270112034567 ]

Tris(1,10-phenanthroline-²N,N')iron(II) bis(2,4,5-tricarboxybenzoate) monohydrate and tris(2,2'-bipyridine-²N,N')iron(II) 2,5-dicarboxybenzene-1,4-dicarboxylate-benzene-1,2,4,5-tetracarboxylic acid-water (1/1/2)

K.-L. Zhong

Formula: [Fe(C₁₂H₈N₂)₃](C₁₀H₅O₈)₂·H₂O and [Fe(C₁₀H₈N₂)₃](C₁₀H₄O₈)·C₁₀H₆O₈·2H₂O

Online 18 August 2012

Acta Cryst. (2012). C68, m265-m268 [ doi:10.1107/S0108270112034385 ]

A novel one-dimensional Co^II coordination polymer: catena-poly[[hexaaquacobalt(II)] [[diaquabis(sulfato-O)cobalt(II)]--4,4'-bipyridine-²N:N'] [[triaqua(sulfato-O)cobalt(II)]--4,4'-bipyridine-²N:N']]

K.-L. Zhong and M.-Y. Qian

Formula: [Co(H₂O)₆][Co(SO₄)(C₁₀H₈N₂)(H₂O)₃][Co(SO₄)₂(C₁₀H₈N₂)(H₂O)₂]

Online 18 August 2012

organic compounds

Acta Cryst. (2012). C68, o327-o331 [ doi:10.1107/S0108270112030168 ]

Hydrogen bonding in cyclic imides and amide carboxylic acid derivatives from the facile reaction of cis-cyclohexane-1,2-carboxylic anhydride with o- and p-anisidine and m- and p-aminobenzoic acids

G. Smith and U. D. Wermuth

Formula: C₁₅H₁₉NO₄, C₁₅H₁₇NO₃, C₁₅H₁₅NO₄ and C₁₅H₁₅NO₄·H₂O

Online 1 August 2012

Acta Cryst. (2012). C68, o332-o334 [ doi:10.1107/S0108270112032933 ]

An optically resolved crystal of thiomalate: (S)-1-phenylethanaminium (R)-thiomalate

K. Igawa, N. Yoshinari and T. Konno

Formula: C₈H₁₂N⁺·C₄H₅O₄S^-

Online 1 August 2012

Acta Cryst. (2012). C68, o335-o337 [ doi:10.1107/S0108270112029022 ]

Rietveld refinement of the cocrystal 2,4-dihydroxybenzoic acid-N'-(propan-2-ylidene)nicotinohydrazide (1/1)

S. H. Lapidus, A. Lemmerer, J. Bernstein and P. W. Stephens

Formula: C₉H₁₁N₃O·C₇H₆O₄

Online 1 August 2012

Acta Cryst. (2012). C68, o338-o340 [ doi:10.1107/S0108270112032076 ]

3,4,6-Tri-O-acetyl-1,2-O-[1-(exo-ethoxy)ethylidene]--D-mannopyranose 0.11-hydrate

Y.-L. Liu, P. Zou, H. Wu, M.-H. Xie and S.-N. Luo

Formula: C₁₆H₂₄O₁₀·0.11H₂O

Online 1 August 2012

Acta Cryst. (2012). C68, o341-o343 [ doi:10.1107/S0108270112032349 ]

Novel pseudopolymorph of the active metabolite of perindopril

J. Bojarska, W. Maniukiewicz, L. Sieron, A. Fruzinski, P. Kopczacki, K. Walczynski and M. Remko

Formula: C₁₇H₂₈N₂O₅·0.5C₂H₆OS

Online 1 August 2012

Acta Cryst. (2012). C68, o344-o350 [ doi:10.1107/S0108270112031691 ]

Pseudopolymorphs of chelidamic acid and its dimethyl ester

M. Tutughamiarso, T. Pisternick and E. Egert

Formula: C₇H₅NO₅·CH₄O, C₂H₈N⁺·C₇H₄NO₅^-, C₇H₅NO₅·C₂H₆OS and C₉H₉NO₅·H₂O

Online 1 August 2012

Acta Cryst. (2012). C68, o351-o354 [ doi:10.1107/S0108270112033781 ]

The supramolecular architecture of tris(naphthalene-1,5-diaminium) bis(5-aminonaphthalen-1-aminium) octakis[hydrogen (5-carboxypyridin-3-yl)phosphonate]

M. Wilk, J. Janczak and V. Videnova-Adrabinska

Formula: 3C₁₀H₁₂N₂²⁺·2C₁₀H₁₁N₂⁺·8C₆H₅NO₅P^-

Online 4 August 2012

Acta Cryst. (2012). C68, o355-o358 [ doi:10.1107/S0108270112033392 ]

Melaminium (2-carboxyethyl)(phenyl)phosphinate monohydrate

J. Xue, C.-C. Zhao and Z.-Y. Du

Formula: C₃H₇N₆⁺·C₉H₁₀O₄P^-·H₂O

Online 4 August 2012

Acta Cryst. (2012). C68, o359-o361 [ doi:10.1107/S0108270112034208 ]

A three-component cocrystal: benzoyl(hydroxyimino)acetonitrile-18-crown-6-water (2/1/4)

V. V. Ponomarova and K. V. Domasevitch

Formula: 2C₉H₆N₂O₂·C₁₂H₂₄O₆·4H₂O

Online 8 August 2012

Acta Cryst. (2012). C68, o362-o364 [ doi:10.1107/S0108270112034749 ]

1,3-Ninhydrin dihydrazone featuring an R₄⁴(12) motif with $\bf \overline{4}$ symmetry and comprising only N and H atoms

A. J. Blake, Y. Chebude, H. Tadesse and B. Wondimu

Formula: C₉H₈N₄O

Online 10 August 2012

Acta Cryst. (2012). C68, o365-o368 [ doi:10.1107/S0108270112035901 ]

2-Ethyl-6-methylpyridin-3-ol and its salt bis(2-ethyl-3-hydroxy-6-methylpyridinium) succinate

A. S. Lyakhov, L. S. Ivashkevich, V. L. Survilo, A. M. Kipnis and T. V. Trukhachova

Formula: C₈H₁₁NO and 2C₈H₁₂NO⁺·C₄H₄O₄^2-

Online 21 August 2012

Acta Cryst. (2012). C68, o369-o372 [ doi:10.1107/S0108270112035536 ]

Reinterpretation of the monohydrate of clarithromycin from X-ray powder diffraction data as a trihydrate

J. van de Streek

Formula: C₃₈H₆₉NO₁₃·3H₂O

Online 21 August 2012

Acta Crystallographica Section C

Crystal Structure Communications

Volume 68, Part 9 (September 2012)

metal-organic compounds

A two-dimensional coordination polymer containing a two-dimensional zinc-carboxylate layer constructed from helical chains: poly[(4-benzene-1,2-dicarboxylato)zinc(II)]

W.-L. Xiong, Q.-Y. Liu, N. Zhang and L. Wang

rac-1-[(2-Methoxyethyl)sulfanyl]-2-[(2-methoxyethyl)sulfinyl]benzene and its PdCl2 complex

J. Traeger, A. Kelling, U. Schilde and H.-J. Holdt

Binary salt of a palladium(II) complex with (phosphonomethyl)phosphonic (medronic) acid comprising `handbell-like' [Pd{-CH2(PO3)2}]3 units

A. A. Babaryk, A. N. Kozachkova, N. V. Tsaryk, A. V. Dudko and V. I. Pekhnyo

1,1'-Methylenedipyridinium tetrachloridocuprate(II) and bis[tetrachloridoaurate(III)] hybrid salts by X-ray powder diffraction

M. Al-Ktaifani and M. Rukiah

The weakly coordinating perchlorate group in bis(N,N'-dimethylethylenediamine-2N,N')bis(perchlorato-O)copper(II) studied at 100, 250 and 400 K

S. Schnitzler, M.-D. Serb and U. Englert

-4,4'-Bipyridine-2N:N'-bis[tetraaqua(4,4'-bipyridine-N)dimanganese(II)] bis(4-aminobenzoate) bis(perchlorate)-4,4'-bipyridine-water (1/2/4): a supramolecular system constructed by - and hydrogen-bond interactions

J. Wang, J. Gao and W. Zhao

Tris(1,10-phenanthroline-2N,N')iron(II) bis(2,4,5-tricarboxybenzoate) monohydrate and tris(2,2'-bipyridine-2N,N')iron(II) 2,5-dicarboxybenzene-1,4-dicarboxylate-benzene-1,2,4,5-tetracarboxylic acid-water (1/1/2)

K.-L. Zhong

A novel one-dimensional CoII coordination polymer: catena-poly[[hexaaquacobalt(II)] [[diaquabis(sulfato-O)cobalt(II)]--4,4'-bipyridine-2N:N'] [[triaqua(sulfato-O)cobalt(II)]--4,4'-bipyridine-2N:N']]

K.-L. Zhong and M.-Y. Qian

organic compounds

Hydrogen bonding in cyclic imides and amide carboxylic acid derivatives from the facile reaction of cis-cyclohexane-1,2-carboxylic anhydride with o- and p-anisidine and m- and p-aminobenzoic acids

G. Smith and U. D. Wermuth

An optically resolved crystal of thiomalate: (S)-1-phenylethanaminium (R)-thiomalate

K. Igawa, N. Yoshinari and T. Konno

Rietveld refinement of the cocrystal 2,4-dihydroxybenzoic acid-N'-(propan-2-ylidene)nicotinohydrazide (1/1)

S. H. Lapidus, A. Lemmerer, J. Bernstein and P. W. Stephens

3,4,6-Tri-O-acetyl-1,2-O-[1-(exo-ethoxy)ethylidene]--D-mannopyranose 0.11-hydrate

Y.-L. Liu, P. Zou, H. Wu, M.-H. Xie and S.-N. Luo

Novel pseudopolymorph of the active metabolite of perindopril

J. Bojarska, W. Maniukiewicz, L. Sieron, A. Fruzinski, P. Kopczacki, K. Walczynski and M. Remko

Pseudopolymorphs of chelidamic acid and its dimethyl ester

M. Tutughamiarso, T. Pisternick and E. Egert

The supramolecular architecture of tris(naphthalene-1,5-diaminium) bis(5-aminonaphthalen-1-aminium) octakis[hydrogen (5-carboxypyridin-3-yl)phosphonate]

M. Wilk, J. Janczak and V. Videnova-Adrabinska

Melaminium (2-carboxyethyl)(phenyl)phosphinate monohydrate

J. Xue, C.-C. Zhao and Z.-Y. Du

A three-component cocrystal: benzoyl(hydroxyimino)acetonitrile-18-crown-6-water (2/1/4)

V. V. Ponomarova and K. V. Domasevitch

1,3-Ninhydrin dihydrazone featuring an R44(12) motif with symmetry and comprising only N and H atoms

A. J. Blake, Y. Chebude, H. Tadesse and B. Wondimu

2-Ethyl-6-methylpyridin-3-ol and its salt bis(2-ethyl-3-hydroxy-6-methylpyridinium) succinate

A. S. Lyakhov, L. S. Ivashkevich, V. L. Survilo, A. M. Kipnis and T. V. Trukhachova

Reinterpretation of the monohydrate of clarithromycin from X-ray powder diffraction data as a trihydrate

J. van de Streek

A two-dimensional coordination polymer containing a two-dimensional zinc-carboxylate layer constructed from helical chains: poly[(₄-benzene-1,2-dicarboxylato)zinc(II)]

rac-1-[(2-Methoxyethyl)sulfanyl]-2-[(2-methoxyethyl)sulfinyl]benzene and its PdCl₂ complex

Binary salt of a palladium(II) complex with (phosphonomethyl)phosphonic (medronic) acid comprising `handbell-like' [Pd{-CH₂(PO₃)₂}]₃ units

The weakly coordinating perchlorate group in bis(N,N'-dimethylethylenediamine-²N,N')bis(perchlorato-O)copper(II) studied at 100, 250 and 400 K

-4,4'-Bipyridine-²N:N'-bis[tetraaqua(4,4'-bipyridine-N)dimanganese(II)] bis(4-aminobenzoate) bis(perchlorate)-4,4'-bipyridine-water (1/2/4): a supramolecular system constructed by - and hydrogen-bond interactions

Tris(1,10-phenanthroline-²N,N')iron(II) bis(2,4,5-tricarboxybenzoate) monohydrate and tris(2,2'-bipyridine-²N,N')iron(II) 2,5-dicarboxybenzene-1,4-dicarboxylate-benzene-1,2,4,5-tetracarboxylic acid-water (1/1/2)

A novel one-dimensional Co^II coordination polymer: catena-poly[[hexaaquacobalt(II)] [[diaquabis(sulfato-O)cobalt(II)]--4,4'-bipyridine-²N:N'] [[triaqua(sulfato-O)cobalt(II)]--4,4'-bipyridine-²N:N']]

1,3-Ninhydrin dihydrazone featuring an R₄⁴(12) motif with $\bf \overline{4}$ symmetry and comprising only N and H atoms