Acta Crystallographica Section C

Crystal Structure Communications

Volume 68, Part 11 (November 2012)

metal-organic compounds

bg3152 scheme

Acta Cryst. (2012). C68, m312-m316    [ doi:10.1107/S0108270112040589 ]

Poly[di-[mu]-aqua-[[mu]6-N-(4-bromo­phenyl­sulfon­yl)dithio­carbimato]dipotassium] and poly[di-[mu]-aqua-[[mu]4-N-(4-iodo­phenyl­sulfon­yl)dithio­carbimato]­dipotassium]

J. Janczak, M. M. M. Rubinger, L. C. Alves and M. R. L. Oliveira

Abstract: The rigid organic linkers N-(4-bromo­phenyl­sulfon­yl)dithio­carbimate(2-) and N-(4-iodo­phenyl­sulfon­yl)dithio­car­bim­ate(2-) crystallize with two potassium cations and two water mol­ecules in their asymmetric units, forming the title coordination polymers, [K2(C7H4BrNO2S3)(H2O)2]n and [K2(C7H4INO2S3)(H2O)2]n. The anions and the water mol­ecules link the potassium cations into broad two-dimensional networks, which are further linked by K...halide inter­actions.

Formula: [K2(C7H4BrNO2S3)(H2O)2] and [K2(C7H4INO2S3)(H2O)2]

hkldisplay filedownload file

Structure factor file (CIF format)
[ doi:10.1107/S0108270112040589/bg3152Isup2.hkl ]
Contains datablock I

hkldisplay filedownload file

Structure factor file (CIF format)
[ doi:10.1107/S0108270112040589/bg3152IIsup3.hkl ]
Contains datablock {vcif ERROR: unable to open file /journals/webproduction/sites/cjo-test/c/issues/2012/11/00/bg3152/bg3152IIsup3.hkl - exiting}


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