Acta Crystallographica Section C

Crystal Structure Communications

Volume 69, Part 6 (June 2013)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The arrangement of two adjacent strands in the monoclinic unit cell of catena-poly[[(tetra­hydro­furan-[kappa]O)potassium]-[mu]-([eta]5:[eta]5)-2,3,4,5-tetra­methyl-1-n-pentyl­cyclo­penta­dien­yl], viewed along the [010] direction. For the sake of clarity, H atoms and the minor disordered component of the disordered THF ligand are not shown. See Seidel, Ganesamoorthy, Loerke, Winter, Gemel & Fischer [Acta Cryst. (2013), C69, 573-576].

metal-organic compounds


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 565-568  [ doi:10.1107/S0108270113010585 ]

Crystal structure and thermal properties of a square-planar NiII complex of cyanide and a tricyclic bis-amidine ligand formed in situ under solvo­thermal conditions

M. Stolárová, J. Cernák, M. Tomás and L. R. Falvello

Formula: [Ni(CN)2(C10H16N4)]·0.5H2O

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 569-572  [ doi:10.1107/S0108270113009311 ]

An approach to creating novel anions: silylated triel compounds with -CH2- and -O- linkers, [InCl2{O(HO)Si(t-Bu)2}]2 and Li[B(CH2SiMe3)4]

S. Scholz, H. Vitze, M. Bolte and H.-W. Lerner

Formula: [In2(C8H19O2Si)2Cl4] and [Li(C4H8O)4](C16H44BSi4)

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 573-576  [ doi:10.1107/S0108270113011074 ]

catena-Poly[[(tetra­hydro­furan-[kappa]O)potassium]-[mu]-([eta]5:[eta]5)-2,3,4,5-tetra­methyl-1-n-pentyl­cyclo­penta­dien­yl]

R. W. Seidel, C. Ganesamoorthy, S. Loerke, M. V. Winter, C. Gemel and R. A. Fischer

Formula: [K(C14H23)(C4H8O)]

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 577-580  [ doi:10.1107/S0108270113010937 ]

Poly[[tetra­chlorido{[mu]4-tetra­kis[(pyridin-4-yl)oxymeth­yl]methane-[kappa]4N:N':N'':N'''}dizinc(II)] di­methyl­formamide tetrasolvate]

Y.-Q. Wang, F.-Z. Xie and L. Du

Formula: [Zn2Cl4(C25H24N4O4)]·4C3H7NO

Online 10 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 581-583  [ doi:10.1107/S0108270113009049 ]

A novel hexa­iron cluster with one disulfide and two Ph2PCS3- ligands

Y.-C. Shi, H.-R. Cheng and D.-C. Cheng

Formula: [Fe6(C13H10PS)2(S2)(CO)16]

Online 10 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 584-587  [ doi:10.1107/S0108270113009633 ]

Chlorido(dimethyl 2,2'-bi­pyridine-4,4'-di­carboxyl­ate-[kappa]2N,N')([eta]5-penta­methyl­cyclo­penta­dien­yl)rhodium(III) chloride 1-hy­droxy­pyrrolidine-2,5-dione disolvate

D. Sivanesan, H. M. Kim and Y. Sungho

Formula: [Rh(C10H15)Cl(C14H12N2O4)]Cl·2C4H5NO3

Online 10 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 588-593  [ doi:10.1107/S0108270113011554 ]

Two polyoxometallate-based supra­molecular compounds influenced by the ratio between the polyoxometallate anion and organic cation

Q. Zhang, J. Liu, J. Lu and S.-W. Gong

Formula: (C10H16N4)3[PMo12O40]2 and (C10H16N4)(C10H15N4)[PMo12O40]·2H2O

Online 10 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 594-596  [ doi:10.1107/S0108270113011967 ]

catena-Poly[[[2-(2-chlorophenoxy)-N'-(2-oxidobenzylidene-[kappa]O)aceto­hydrazidato-[kappa]2N',O]copper(II)]-[mu]-morpholine-[kappa]2N:O]

M. Wang and Z.-X. Lian

Formula: [Cu(C15H11ClN2O3)]C4H9NO)]

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 597-600  [ doi:10.1107/S0108270113011153 ]

Magnetic investigations of a two-dimensional coordination polymer with a three-dimensional supra­molecular framework: poly[[bis­[[mu]2-1,4-bis­(1,2,4-triazol-1-yl)butane]­bis­(thio­cyanato-[kappa]N)cobalt(II)] dihydrate]

J.-Q. Tao, D. Mao and J. Wang

Formula: [Co(NCS)2(C8H12N6)2]·2H2O

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 601-605  [ doi:10.1107/S0108270113010913 ]

The coordination chemistry of two symmetric double-armed oxa­diazole-bridged organic ligands with copper salts

X.-W. Wu, M.-M. Xin, J.-P. Ma, Z.-H. Wu and Y.-B. Dong

Formula: [Cu(ClO4)2(C28H20N4O5)2] and [Cu4I4(C2H3N)2(C28H20N4O5)2]

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 606-609  [ doi:10.1107/S0108270113011943 ]

Chlorido[N,N'-dibenz­yl-N''-(tri­chloro­acet­yl)phosphor­amidato-[kappa]2O,O'](1,10-phenanthroline-[kappa]2N,N')copper(II)

K. Gubina, V. Ovchynnikov, V. Amirkhanov and S. Shishkina

Formula: [Cu(C16H16Cl3N3O2P)Cl(C12H8N2)]

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 610-612  [ doi:10.1107/S0108270113011992 ]

A novel two-dimensional CuSCN network templated by 2,2'-dimethyl-1,1'-(butane-1,4-di­yl)bis­(1H-imidazol-3-ium) cations

S.-S. Liu, S. Yuan, H.-F. Lu, M.-Z. Xu and D. Sun

Formula: (C12H20N4)[Cu2(NCS)4]

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 613-615  [ doi:10.1107/S0108270113012547 ]

Di-[mu]2-chlorido-dichlorido­bis(di­methyl­formamide)­tetra­kis­[[mu]3-1-(2-oxido­benzoyl)-2-(2-oxo-2-phenyl­ethane­thioyl)hydrazine-1,2-diido]octa­copper(II) di­methyl­formamide disolvate

J.-J. Liu, J.-Z. Liao, Z.-Y. Li, Y. Wang and C.-C. Huang

Formula: [Cu8(C15H10N3O3S)4Cl4(C3H7NO)2]·2C3H7NO

Online 17 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 616-619  [ doi:10.1107/S0108270113012638 ]

Reversible high-temperature phase transition of a manganese(II) formate framework with imidazolium cations

B.-Q. Wang, H.-B. Yan, Z.-Q. Huang and Z. Zhang

Formula: (C3H5N2)[Mn(CHO2)3] at 293 and 453 K

Online 17 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 620-623  [ doi:10.1107/S0108270113013000 ]

A novel two-dimensional coordination polymer: poly[di­aqua­tetra-[mu]2-chlorido-[[mu]2-2,2'-(piperazine-1,4-di­ium-1,4-di­yl)di­acetate]­di­cadmium(II)]

X.-J. Xu, J.-Y. Miao and J. Wang

Formula: [Cd2Cl4(C8H14N2O4)(H2O)2]

Online 18 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 624-626  [ doi:10.1107/S0108270113013437 ]

Bromidobis[2-(pyridin-2-yl)methanol-[kappa]2N,O]copper(II) bromide mono­hydrate

N. Lah and K. Lapanje

Formula: [CuBr(C6H7NO)2]Br·H2O

Online 24 May 2013


organic compounds


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 627-629  [ doi:10.1107/S0108270113010597 ]

Bromine-bromine inter­actions in the packing of cis,trans,cis-1,2,3,4-tetra­kis­(bromo­methyl)cyclo­butane

A. Kelch, I. Dix, H. Hopf and P. G. Jones

Formula: C8H12Br4

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 630-633  [ doi:10.1107/S0108270113011025 ]

An ortho­rhom­bic polymorph of a cyclization product of perindopril

J. Bojarska, W. Maniukiewicz, L. Sieron and M. Remko

Formula: Two polymorphs of C19H30N2O4

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 634-637  [ doi:10.1107/S0108270113010895 ]

Synthesis and photophysical properties of 2,5,8,11-tetra­kis­(5-hexyl­thio­phen-2-yl)tetra­thieno[2,3-a:3',2'-c:2'',3''-f:3''',2'''-h]naphthalene

L. Gao

Formula: C58H64S8

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 638-641  [ doi:10.1107/S0108270113010706 ]

A comparison of 3,4,6a,7,10,10a-hexa­hydro-7,10-ep­oxy­pyrimido[2,1-a]isoindol-6(2H)-one and 2-(2-amino­eth­yl)-3a,4,7,7a-tetra­hydro-1H-4,7-ep­oxy­iso­indole-1,3(2H)-dione: structural and reactivity differences of two homologous tricyclic imides

L. A. Mitchell, J. M. Stanley, L. Espinosa De Hoyos and B. J. Holliday

Formula: C11H12N2O2 and C10H12N2O3

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 642-646  [ doi:10.1107/S0108270113010676 ]

N-H...O and N-H...N inter­actions in three pyran derivatives

R. Vishnupriya, J. Suresh, S. Sivakumar and R. R. Kumar

Formula: C19H15N3O3, C19H14FN3O3 and C19H14ClN3O3

Online 2 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 647-650  [ doi:10.1107/S0108270113011852 ]

(2S,3S)-2,6-Di­methyl­heptane-1,3-diol, the oxygenated side chain of 22(S)-hy­droxy­cholestrol, and its synthetic precursor (R)-4-benzyl-3-[(2R,3S)-3-hy­droxy-2,6-di­methyl­hepta­noyl]-1,3-oxazolidin-2-one

O. A. Høgmoen Åstrand, Z. Iqbal, M. Sandberg, E. T. Kase, C. H. Görbitz and P. Rongved

Formula: C9H20O2 and C19H27NO4

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 651-653  [ doi:10.1107/S0108270113011232 ]

meso-Tetra­kis[4-(hept­yloxy)phen­yl]porphyrin

H.-B. Zhao, L. Chen, B.-Y. Wang, J.-X. Liao and Y.-J. Xu

Formula: C72H86N4O4

Online 15 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 654-657  [ doi:10.1107/S0108270113011980 ]

Alkyl levulinates as `green chemistry' precursors: butane-1,4-diyl bis­(4-oxo­pentan­oate) and hexane-1,6-diyl bis­(4-oxo­pentan­oate)

G. J. Gainsford and S. Hinkley

Formula: C14H22O6 and C16H26O6

Online 17 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 658-664  [ doi:10.1107/S0108270113012377 ]

Three salts from the reactions of cyste­amine and cystamine with L-(+)-tartaric acid

A. Benylles, D. Cairns, P. J. Cox and G. Kay

Formula: C2H8NS+·C4H5O6-·H2O, C4H14N2S22+·2C4H5O6-·2H2O and C4H14N2S22+·C4H4O62-

Online 17 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 665-670  [ doi:10.1107/S0108270113011979 ]

Supra­molecular study, Hirshfeld analysis and theoretical study of 6-meth­oxy­quinoline N-oxide dihydrate

R. Moreno-Fuquen, G. Hernandez, A. R. Kennedy and C. A. Morrison

Formula: C10H9NO2·2H2O

Online 17 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 671-673  [ doi:10.1107/S0108270113013267 ]

(E)-2-(1,3-Benzo­thia­zol-2-yl)-3-(4-fluoro­phen­yl)acrylo­nitrile: a chain of [pi]-stacked hydrogen-bonded rings

J. Trilleras, K. Velásquez, J. Cobo and C. Glidewell

Formula: C16H9FN2S

Online 17 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Supplementary Material][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 674-678  [ doi:10.1107/S0108270113012560 ]

Alogliptin and its benzoate salt

T. Gelbrich, V. Kahlenberg and U. J. Griesser

Formula: C18H21N5O2 and C18H22N5O2+·C7H5O2-

Online 18 May 2013


thumbnail of article figure

[HTML version][PDF version][CIF][3d view][Structure Factors][Scheme]  [Buy article online]

Acta Cryst. (2013). C69, 679-682  [ doi:10.1107/S010827011301367X ]

Translationally related nearly identical mol­ecules: 4-meth­oxy­phenyl 4-O-[6-O-acetyl-2-azido-3-O-benzyl-2-de­oxy-4-O-(fluoren-9-yl­meth­oxycarbon­yl)-[alpha]-D-gluco­pyranos­yl]-2-O-benzoyl-3-O-benzyl-6-O-chloro­acetyl-[beta]-D-gluco­pyran­oside

G. J. Gainsford, R. Schwörer and P. C. Tyler

Formula: C59H56ClN3O16

Online 29 May 2013


Copyright © International Union of Crystallography
IUCr Webmaster