Acta Crystallographica Section C

Crystal Structure Communications

Volume 69, Part 7 (July 2013)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The molecular structure of 1,4-bis[2-(4-ferrocenylphenyl)ethynyl]anthraquinone at 90 K from synchrotron X-ray powder diffraction. Displacement ellipsoids are drawn at the 50% probability level. See Sachiko, Nishibori, Aoyagi, Sakata, Takata, Kondo, Murata, Sakamoto & Nishihara [Acta Cryst. (2013), C69, 696-703].

inorganic compounds


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Acta Cryst. (2013). C69, 683-688  [ doi:10.1107/S0108270113014492 ]

Tm2.22Co6Sn20 and TmLi2Co6Sn20 stannides as disordered derivatives of the Cr23C6 structure type

A. Stetskiv, B. Rozdzynska-Kielbik and V. Pavlyuk

Synopsis: The new ternary Tm2.22Co6Sn20 [a = 13.5365 (7) Å] and quaternary TmLi2Co6Sn20 [a = 13.5371 (16) Å] phases crystallize in the same cubic crystal system in the space group Fm3m and are disordered variants of the binary Cr23C6 structure type (cF116).

Formula: Tm2.22Co6Sn20 and TmLi2Co6Sn20

Online 8 June 2013


metal-organic compounds


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Acta Cryst. (2013). C69, 689-695  [ doi:10.1107/S0108270113013711 ]

Two solvatomorphic forms of a copper complex formulated as Cu(L1)(ClO4)2·1.2H2O and Cu(L1)(ClO4)2, where L1 is 3,10-C-meso-3,5,7,7,10,12,14,14-octa­methyl-1,4,8,11-tetra­aza­cyclo­tetra­decane

B. C. Nath, S. Suarez, F. Doctorovich, T. G. Roy and R. Baggio

Formula: [Cu(ClO4)2(C18H40N4)]·1.2H2O and [Cu(ClO4)2(C18H40N4)]

Online 8 June 2013


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Acta Cryst. (2013). C69, 696-703  [ doi:10.1107/S0108270113013978 ]

1,4-Bis[2-(4-ferrocenyl­phenyl)­ethynyl]­anthra­quinone from synchrotron X-ray powder diffraction

M. Sachiko, E. Nishibori, S. Aoyagi, M. Sakata, M. Takata, M. Kondo, M. Murata, R. Sakamoto and H. Nishihara

Formula: [Fe2(C5H5)2(C40H22O2)] at 90, 300 and 500 K

Online 8 June 2013


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Acta Cryst. (2013). C69, 704-708  [ doi:10.1107/S0108270113014078 ]

Bridging behaviour of the 2-thio­barbiturate anion in its complexes with LiI and NaI

N. Golovnev and M. Molokeev

Formula: [Li4(C4H3N2O2S)4(H2O)9]·2H2O and [Na2(C4H3N2O2S)2(H2O)5]

Online 8 June 2013


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Acta Cryst. (2013). C69, 709-711  [ doi:10.1107/S0108270113015047 ]

Bis(4-picoline-[kappa]N)gold(I) di­bromido­aurate(I) and bis­(4-picoline-[kappa]N)gold(I) di­chlorido­aurate(I): space-group ambiguity?

C. Döring and P. G. Jones

Formula: [Au(C6H7N)2][AuBr2] and [Au(C6H7N)2][AuCl2]

Online 8 June 2013


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Acta Cryst. (2013). C69, 712-715  [ doi:10.1107/S0108270113014765 ]

A tubular one-dimensional polymer constructed from alternating clusters of europium(III)-water and copper(I) chloride bridged by 4-(pyridin-4-yl)benzoate

G.-J. Cao, Q.-L. Li, C. Rong and Y.-L. Wang

Formula: [Cu2Er(C12H8NO2)4Cl(H2O)]·2H2O

Online 8 June 2013


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Acta Cryst. (2013). C69, 716-720  [ doi:10.1107/S0108270113012134 ]

ZnII and CuII complexes generated from 5-(pyridin-4-yl)-3-[2-(pyridin-4-yl)ethyl]-1,3,4-oxa­diazole-2(3H)-thione

H.-J. Zhao, J.-P. Ma, Q.-K. Liu and Y.-B. Dong

Formula: [Zn2(NO3)4(C14H12N4OS)2] and [Cu(NO3)(C14H12N4OS)2]NO3·1.5CH3CN·1.5CH2Cl2

Online 13 June 2013


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Acta Cryst. (2013). C69, 721-726  [ doi:10.1107/S0108270113014832 ]

The first uranyl complexes with valerate ions

A. V. Savchenkov, A. V. Vologzhanina, L. B. Serezhkina, D. V. Pushkin and V. N. Serezhkin

Formula: [U(C5H9O2)2O2(H2O)2] and K[U(C5H9O2)3O2]

Online 13 June 2013


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Acta Cryst. (2013). C69, 727-729  [ doi:10.1107/S0108270113015060 ]

cis-Di­chlorido(3,6,9-tri­thiabi­cyclo[9.3.1]penta­decane-[kappa]2S3,S6)palladium(II) aceto­nitrile 0.8-solvate

L. N. Dawe, L. Penney, D. A. Black, D. O. Miller and C. R. Lucas

Formula: [PdCl2(C12H22S3)]·0.8C2H3N

Online 14 June 2013


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Acta Cryst. (2013). C69, 730-733  [ doi:10.1107/S0108270113015151 ]

A novel two-dimensional metal-organic supra­molecular framework including [pi]-[pi] stacking and hydrogen-bond inter­actions

X.-L. Wu, X.-M. Zhang, S.-Y. Huang, W.-N. Zhou and Z.-C. Wang

Formula: [Hg2I4(C18H14N4O2)3]

Online 18 June 2013


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Acta Cryst. (2013). C69, 734-737  [ doi:10.1107/S0108270113015709 ]

A new compound in kidney stones? Powder X-ray diffraction study of calcium glycinate trihydrate

A. Le Bail, M. Daudon and D. Bazin

Formula: [Ca(C2H4NO2)2(H2O)2]·H2O

Online 20 June 2013


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Acta Cryst. (2013). C69, 738-741  [ doi:10.1107/S0108270113015436 ]

1,4-Bis{[hy­droxy­(phenyl)­phosphoryl]­methyl}­piperazine-1,4-diium tetra­chlorido­cadmate(II) dihydrate and the cobaltate(II) analogue

C.-J. Du and L.-S. Wang

Formula: (C18H26N2O4P2)[CdCl4]·2H2O and (C18H26N2O4P2)[CoCl4]·2H2O

Online 21 June 2013


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Acta Cryst. (2013). C69, 742-744  [ doi:10.1107/S010827011301559X ]

A three-dimensional supra­molecular framework of silver(I), 2-phenyl­quinoline-4-carboxyl­ate and 4,4'-bi­pyridine

J.-F. Guo, B.-X. Guo, J.-Y. Wu and G.-P. Yan

Formula: [Ag(C16H10NO2)(C10H8N2)(H2O)]·2H2O

Online 21 June 2013


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Acta Cryst. (2013). C69, 745-749  [ doi:10.1107/S0108270113016521 ]

Two isomorphous transition metal complexes displaying a coordinated tetra­thio­nate unit: bis­(4,4'-dimethyl-2,2'-bi­pyridine-[kappa]2N,N')(tetra­thio­nato-[kappa]2S,S')cadmium(II) di­methyl­formamide disolvate and the zinc(II) analogue

M. A. Harvey, S. Suarez, F. Doctorovich and R. Baggio

Formula: [Cd(S4O6)(C12H12N2)2]·2C3H7NO and [Zn(S4O6)(C12H12N2)2]·2C3H7NO

Online 25 June 2013


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Acta Cryst. (2013). C69, 750-753  [ doi:10.1107/S0108270113016168 ]

Two one-dimensional linear zinc(II) polymers: catena-poly[[[2,6-bis­(1H-benzimidazol-2-yl-[kappa]N3)pyridine]zinc(II)]-[mu]-pyridine-2,4-di­carboxyl­ato-[kappa]2O2:O4] and catena-poly[[[2,6-bis­(1H-benzimidazol-2-yl-[kappa]N3)pyri­dine]zinc(II)]-[mu]-pyridine-2,5-di­car­boxyl­ato-[kappa]2O2:O5]

J. Xiang

Formula: [Zn(C7H3NO4)(C19H13N5)] and [Zn(C7H3NO4)(C19H13N5)]

Online 29 June 2013


organic compounds


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Acta Cryst. (2013). C69, 754-760  [ doi:10.1107/S0108270113013590 ]

Four related esters: two 4-(aroyl­hydrazin­yl)-3-nitro­benzoates and two 3-aryl-1,2,4-benzotriazine-6-carboxyl­ates

E. Cortés, R. Abonía, J. Cobo and C. Glidewell

Formula: C15H12ClN3O5, C15H12FN3O5, C15H11N3O2 and C16H13N3O2

Online 8 June 2013


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Acta Cryst. (2013). C69, 761-764  [ doi:10.1107/S0108270113013929 ]

(E)-4-[(2-Carbamoylhydrazinyl­idene)meth­yl]-3-hy­droxy-5-hy­droxy­methyl-2-methyl­pyridin-1-ium nitrate

S. B. Novakovic, G. A. Bogdanovic, V. M. Leovac, M. V. Rodic, L. S. Vojinovic-Jesic and S. Ivkovic

Formula: C9H13N4O3+·NO3-

Online 8 June 2013


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Acta Cryst. (2013). C69, 765-769  [ doi:10.1107/S0108270113013991 ]

(E)-Ethyl 3-(3,4-di­hydroxy­phen­yl)prop-2-enoate: a natural polymorph extracted from Aristotelia chilensis (Maqui)

C. Paz, Y. Moreno, J. Becerra, M. Silva, V. Burgos, E. Freire and R. Baggio

Formula: C11H12O4

Online 8 June 2013


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Acta Cryst. (2013). C69, 770-773  [ doi:10.1107/S0108270113014777 ]

Hydrogen-bonded dimers in 3-amino-4-anilino-1H-isochromen-1-one and a hydrogen-bonded sheet in 3-amino-4-[meth­yl(phen­yl)amino]-1H-isochromen-1-one

D. E. Vicentes, R. Rodríguez, J. Cobo and C. Glidewell

Formula: C15H12N2O2 and C16H14N2O2

Online 8 June 2013


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Acta Cryst. (2013). C69, 774-777  [ doi:10.1107/S0108270113014601 ]

Tri­phenyl­silanol-4,4'-bipyridyl (4/1): the Z' = 4 polymorph revisited

G. L. Cascarano, G. Ferguson, C. Giacovazzo, C. Glidewell and A. L. Spek

Formula: 4C18H16OSi·C10H8N2

Online 8 June 2013


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Acta Cryst. (2013). C69, 778-780  [ doi:10.1107/S0108270113015011 ]

A solid-state oxidation of 1,1,3,3-tetra­methyl­guanidinium 4-methyl­benzene­sulfinate to 1,1,3,3-tetra­methyl­guanidinium 4-methyl­benzenesulfonate

Å. Kaupang, C. H. Görbitz and T. Bonge-Hansen

Formula: C5H14N3+·C7H7O2S- and C5H14N3+·C7H7O2.82S-

Online 8 June 2013


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Acta Cryst. (2013). C69, 781-786  [ doi:10.1107/S010827011301411X ]

Three new olanzapine structures: the acetic acid monosolvate, and the propan-2-ol and propan-2-one hemisolvate monohydrates

J. Bojarska, W. Maniukiewicz and L. Sieron

Formula: C17H20N4S·C2H4O2, C17H20N4S·0.5C3H8O·H2O and C17H20N4S·0.5C3H6O·H2O

Online 8 June 2013


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Acta Cryst. (2013). C69, 787-789  [ doi:10.1107/S0108270113015084 ]

Hydrogen-bonding network of N,N'-bis­[2-(tert-butyl­dimethyl­siloxy)­ethyl]­ethyl­ene­di­ammonium dichloride

M.-F. Wen, B.-T. Lin, C.-S. He and J.-Z. Wu

Formula: C18H46N2O2Si22+·2Cl-

Online 13 June 2013


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Acta Cryst. (2013). C69, 790-793  [ doi:10.1107/S0108270113015229 ]

Br...O contacts and [pi]-[pi] stacking dominate the packing in methyl 4-bromo-3,5-di­meth­oxy­benzoate

A. Saeed, M. Qasim and J. Simpson

Formula: C10H11BrO4

Online 14 June 2013


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Acta Cryst. (2013). C69, 794-797  [ doi:10.1107/S0108270113015783 ]

Two hydrate pseudopolymorphs of thi­amine pyrophosphate: a dihydrate and a trihydrate

S.-Q. Li and N.-H. Hu

Formula: C12H18N4O7P2S·2H2O and C12H18N4O7P2S·3H2O

Online 20 June 2013


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Acta Cryst. (2013). C69, 798-802  [ doi:10.1107/S010827011301651X ]

Di­benzyl­ammonium hydrogen maleate and a redetermination at 120 K of bis­(di­benzyl­amino)­methane

J. C. Castillo, R. Abonía, J. Cobo and C. Glidewell

Formula: C14H16N+·C4H3O4- and C29H30N2

Online 25 June 2013


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