# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 264.95 _exptl_crystal_F_000 1060.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.4715 _cell_length_b 12.7603 _cell_length_c 14.1922 _cell_angle_alpha 76.778 _cell_angle_beta 80.258 _cell_angle_gamma 68.709 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11.21 24.18 11.44 o 3 0 0 1160.81 1150.22 45.71 o 4 0 0 0.55 -4.98 10.20 o 5 0 0 1294.38 1144.50 43.11 o 6 0 0 8074.16 7456.29 304.38 o 7 0 0 2595.61 2272.07 73.20 o 8 0 0 191.37 165.37 28.75 o 9 0 0 786.07 679.55 58.64 o 10 0 0 3268.98 3215.76 199.58 o 11 0 0 499.55 459.98 100.66 o 12 0 0 253.99 208.46 99.21 o 13 0 0 138.70 24.40 90.98 o 14 0 0 486.55 589.49 143.13 o -13 1 0 367.44 430.70 125.94 o -12 1 0 235.88 113.63 91.78 o -11 1 0 59.71 48.58 75.39 o -10 1 0 105.70 125.50 65.85 o -9 1 0 1162.03 1118.65 75.85 o -8 1 0 3872.39 3543.57 130.55 o -7 1 0 714.66 683.72 41.73 o -6 1 0 105.94 73.79 20.76 o -5 1 0 4227.39 3490.84 232.48 o -4 1 0 497.10 442.13 52.08 o -3 1 0 382.39 371.55 43.92 o -2 1 0 230.53 187.08 47.86 o -1 1 0 9979.24 10114.85 348.17 o 0 1 0 2527.76 1461.29 59.87 o 1 1 0 70064.75 69564.06 2317.73 o 2 1 0 13567.45 11541.03 393.11 o 3 1 0 597.27 568.86 37.50 o 4 1 0 163.23 198.29 18.62 o 5 1 0 49.09 65.72 27.27 o 6 1 0 4851.93 4400.38 253.31 o 7 1 0 3966.09 3505.82 97.87 o 8 1 0 2838.33 2736.29 235.30 o 9 1 0 2534.30 2382.72 100.90 o 10 1 0 266.86 281.81 74.22 o 11 1 0 1627.36 1560.79 147.94 o 12 1 0 1067.22 978.23 135.12 o 13 1 0 1199.10 1026.59 147.86 o 14 1 0 0.26 -38.53 93.16 o -13 2 0 498.49 582.86 140.80 o -12 2 0 221.95 61.40 97.68 o -11 2 0 123.47 88.64 81.07 o -10 2 0 26.28 72.69 64.54 o -9 2 0 91.38 98.82 42.39 o -8 2 0 2237.29 2191.06 101.88 o -7 2 0 10653.80 6179.58 260.03 o -5 2 0 2751.01 2375.11 308.76 o -4 2 0 1635.15 1508.62 64.02 o -3 2 0 1349.25 1275.41 54.91 o -2 2 0 841.14 777.48 39.71 o -1 2 0 965.53 947.24 39.47 o 0 2 0 10657.10 11602.73 404.47 o 1 2 0 7905.66 7666.15 274.09 o 2 2 0 3768.81 4017.94 208.06 o 3 2 0 451.61 377.30 127.91 o 4 2 0 4147.62 4175.85 122.02 o 5 2 0 2785.48 2705.04 74.31 o 6 2 0 799.79 802.35 39.97 o 7 2 0 219.91 180.74 24.92 o 8 2 0 884.59 859.07 47.26 o 9 2 0 2708.48 2680.27 89.89 o 10 2 0 5992.04 5859.46 201.20 o 11 2 0 54.19 50.55 63.95 o 12 2 0 452.66 360.92 99.72 o 13 2 0 461.02 576.96 127.69 o 14 2 0 806.13 687.67 145.17 o -12 3 0 34.18 15.37 91.27 o -11 3 0 197.04 168.77 90.03 o -10 3 0 60.34 19.16 78.30 o -9 3 0 350.43 263.68 53.43 o -8 3 0 3755.89 3828.41 222.38 o -7 3 0 583.87 497.81 64.86 o -6 3 0 9398.14 8748.04 253.14 o -5 3 0 8284.00 7849.29 226.29 o -4 3 0 9318.34 9034.85 250.01 o -3 3 0 1557.96 1537.37 65.33 o -2 3 0 1547.69 1405.75 58.73 o -1 3 0 1686.50 1727.37 139.01 o 0 3 0 7105.47 7366.93 276.79 o 1 3 0 17236.26 18852.43 477.28 o 2 3 0 60963.38 64536.35 1823.30 o 3 3 0 3923.88 4101.47 121.69 o 4 3 0 33.85 32.60 12.16 o 5 3 0 4263.45 4444.09 114.27 o 6 3 0 9545.22 9222.04 386.96 o 7 3 0 1697.23 1686.31 75.65 o 8 3 0 136.37 126.50 25.45 o 9 3 0 129.25 129.49 30.15 o 10 3 0 1564.83 1479.83 89.69 o 11 3 0 2400.14 2400.36 121.19 o 12 3 0 191.68 124.99 83.69 o 13 3 0 0.68 -23.24 78.37 o 14 3 0 26.76 -7.65 89.30 o -12 4 0 408.03 668.52 148.52 o -11 4 0 26.16 -29.35 93.67 o -10 4 0 9.54 -9.32 79.25 o -9 4 0 133.76 99.75 89.01 o -8 4 0 1284.70 1151.03 108.35 o -7 4 0 3750.72 3527.35 144.15 o -6 4 0 73.84 71.84 34.41 o -5 4 0 196.20 182.10 34.82 o -4 4 0 7337.54 6902.01 205.09 o -3 4 0 10492.76 10179.33 278.53 o -2 4 0 84.14 81.56 24.02 o -1 4 0 40.70 25.24 17.92 o 0 4 0 8030.74 8153.82 192.14 o 1 4 0 9563.41 6149.93 243.28 o 2 4 0 36629.89 39001.65 969.48 o 3 4 0 31111.02 33463.93 823.39 o 4 4 0 27.42 44.69 19.31 o 5 4 0 487.86 485.71 62.31 o 6 4 0 3420.51 3321.92 121.41 o 7 4 0 2877.14 2722.73 82.53 o 8 4 0 3299.88 3497.83 110.06 o 9 4 0 2044.08 2018.63 95.97 o 10 4 0 298.89 316.04 49.43 o 11 4 0 221.19 208.95 51.99 o 12 4 0 519.40 572.85 95.49 o 13 4 0 28.58 -21.20 81.29 o -11 5 0 876.33 940.86 157.62 o -10 5 0 6.91 -5.75 86.02 o -9 5 0 135.31 71.60 81.22 o -8 5 0 846.79 874.39 82.32 o -7 5 0 1204.71 1125.40 84.83 o -6 5 0 3907.60 3899.81 147.91 o -5 5 0 1589.45 1625.63 115.85 o -4 5 0 327.62 314.79 41.09 o -3 5 0 27.62 19.26 23.41 o -2 5 0 401.96 456.29 42.36 o -1 5 0 3445.01 3279.98 227.26 o 0 5 0 11453.39 11920.75 254.40 o 2 5 0 450.58 403.92 37.00 o 3 5 0 10657.12 11108.62 299.89 o 4 5 0 16949.14 18929.63 487.61 o 5 5 0 659.68 622.51 61.37 o 6 5 0 20.01 4.29 14.40 o 7 5 0 554.91 609.59 38.79 o 8 5 0 9.09 1.57 19.65 o 9 5 0 1425.41 1435.60 64.55 o 10 5 0 3830.73 3736.99 168.08 o 11 5 0 158.59 167.38 79.83 o 12 5 0 401.23 304.61 99.72 o 13 5 0 54.13 -26.29 84.71 o -11 6 0 390.29 273.95 123.75 o -10 6 0 374.98 525.75 130.89 o -9 6 0 483.71 562.97 122.73 o -8 6 0 3.53 13.66 46.28 o -7 6 0 209.44 184.44 54.29 o -6 6 0 192.02 195.48 49.94 o -5 6 0 5037.82 5051.66 177.10 o -4 6 0 3578.94 3543.79 333.97 o -3 6 0 153.54 133.54 35.09 o -2 6 0 235.08 246.07 36.79 o -1 6 0 1050.47 1105.95 60.77 o 0 6 0 6347.96 6594.51 154.76 o 1 6 0 34346.30 36139.70 729.67 o 2 6 0 9592.55 9794.89 273.02 o 3 6 0 837.06 1026.46 61.01 o 4 6 0 3080.03 3512.74 125.86 o 5 6 0 315.40 334.55 41.52 o 6 6 0 1930.05 1824.38 97.17 o 7 6 0 414.91 465.22 75.75 o 8 6 0 1199.20 1338.04 107.66 o 9 6 0 38.04 63.76 35.81 o 10 6 0 1039.17 1218.08 129.29 o 11 6 0 1057.78 1018.72 141.31 o 12 6 0 2.19 -12.09 76.04 o 13 6 0 527.53 591.01 131.77 o 14 6 0 6.51 -135.04 106.13 o -10 7 0 192.88 72.91 109.91 o -9 7 0 91.68 167.82 102.56 o -8 7 0 1070.47 1074.71 99.17 o -7 7 0 340.84 389.97 85.48 o -6 7 0 269.74 172.42 54.80 o -5 7 0 11.44 2.54 37.96 o -4 7 0 3166.23 3201.20 136.72 o -3 7 0 1070.85 1055.75 72.20 o -2 7 0 395.71 447.93 48.38 o -1 7 0 57.48 63.05 27.45 o 0 7 0 456.16 484.73 42.48 o 1 7 0 3904.66 4284.94 111.66 o 2 7 0 23449.92 24399.28 626.25 o 3 7 0 6050.09 6219.62 195.01 o 4 7 0 660.87 769.47 82.13 o 5 7 0 2444.23 2490.00 106.29 o 6 7 0 1029.95 1113.96 71.31 o 7 7 0 1163.94 1103.20 72.44 o 8 7 0 2732.40 2896.22 187.12 o 9 7 0 2151.73 2180.70 108.60 o 10 7 0 318.98 289.32 91.63 o 11 7 0 384.66 314.52 99.57 o 12 7 0 332.02 262.66 110.28 o 13 7 0 3.65 -79.39 93.74 o 14 7 0 6.19 34.09 108.24 o 15 7 0 28.98 82.24 135.19 o -9 8 0 29.79 -74.66 89.81 o -8 8 0 57.71 14.01 62.82 o -7 8 0 444.13 430.52 76.04 o -6 8 0 3424.54 3521.34 157.80 o -5 8 0 2829.61 2759.45 292.59 o -4 8 0 2.66 40.49 39.90 o -3 8 0 27.79 49.11 36.48 o -2 8 0 164.75 177.67 80.85 o -1 8 0 497.73 538.11 94.62 o 0 8 0 241.61 232.26 30.23 o 1 8 0 3304.22 3471.93 130.72 o 2 8 0 146.48 156.84 86.17 o 3 8 0 6537.57 6718.64 227.66 o 4 8 0 1925.67 2285.86 104.82 o 5 8 0 96.59 167.05 62.86 o 6 8 0 183.75 218.85 41.33 o 7 8 0 98.11 99.94 36.50 o 8 8 0 404.24 429.20 113.19 o 9 8 0 2372.60 2655.42 191.71 o 10 8 0 518.45 496.25 108.89 o 11 8 0 1185.63 1187.57 159.74 o 12 8 0 0.51 34.74 91.27 o 13 8 0 188.30 133.44 118.73 o 14 8 0 279.97 144.80 135.84 o -8 9 0 0.25 -81.96 68.97 o -7 9 0 720.59 628.97 195.57 o -6 9 0 17.12 -80.35 53.57 o -5 9 0 2978.10 2936.21 241.93 o -4 9 0 4077.88 4176.89 168.37 o -3 9 0 1862.84 1798.63 102.78 o -2 9 0 1059.92 1048.03 79.74 o -1 9 0 127.25 177.44 74.44 o 0 9 0 39.86 37.51 58.05 o 1 9 0 627.07 719.55 63.91 o 2 9 0 5840.54 6424.75 307.82 o 3 9 0 4716.77 5022.04 179.86 o 4 9 0 2000.87 2077.42 144.08 o 5 9 0 1020.70 1151.24 89.48 o 6 9 0 15.41 29.09 45.20 o 7 9 0 3057.61 2940.13 132.92 o 8 9 0 1265.25 1145.54 186.69 o 9 9 0 89.67 156.74 51.32 o 10 9 0 803.78 634.28 118.58 o 11 9 0 499.13 635.37 129.43 o 12 9 0 2013.43 2119.54 204.68 o 13 9 0 1.61 -16.75 96.88 o 14 9 0 162.17 1.02 112.54 o -7 10 0 82.91 148.54 74.62 o -6 10 0 1799.72 1968.59 132.98 o -5 10 0 81.31 167.87 63.33 o -4 10 0 1148.82 1078.23 137.37 o -3 10 0 701.24 591.45 112.75 o -2 10 0 1952.17 2094.19 175.47 o -1 10 0 615.01 772.38 115.81 o 0 10 0 328.52 239.06 85.22 o 1 10 0 820.12 816.96 123.39 o 2 10 0 837.80 987.67 101.17 o 3 10 0 3980.63 4142.03 164.05 o 4 10 0 12097.93 12548.56 502.48 o 5 10 0 307.44 327.54 57.76 o 6 10 0 253.61 369.35 61.35 o 7 10 0 1324.08 1408.45 98.04 o 8 10 0 3314.22 3486.14 227.99 o 9 10 0 1462.91 1461.50 103.77 o 10 10 0 61.97 29.86 72.62 o 11 10 0 190.03 85.59 98.48 o 12 10 0 149.16 123.02 111.15 o 13 10 0 619.97 547.89 158.93 o 14 10 0 65.12 209.92 134.02 o -6 11 0 406.93 495.60 141.53 o -5 11 0 1877.31 1874.07 191.57 o -4 11 0 104.91 56.67 99.50 o -3 11 0 144.48 128.85 103.14 o -2 11 0 42.90 301.63 98.41 o -1 11 0 147.14 167.09 96.66 o 0 11 0 814.45 950.47 133.81 o 1 11 0 1125.41 973.78 144.37 o 2 11 0 710.15 712.58 126.45 o 3 11 0 134.72 149.91 51.75 o 4 11 0 3646.10 3933.65 168.20 o 5 11 0 7782.82 7968.60 269.74 o 6 11 0 3.10 -49.47 44.83 o 7 11 0 251.37 380.89 67.59 o 8 11 0 1628.55 1576.21 112.05 o 9 11 0 616.49 701.33 82.32 o 10 11 0 623.38 679.88 134.75 o 11 11 0 108.82 183.77 116.69 o 12 11 0 101.59 167.31 121.42 o 13 11 0 12.35 89.15 119.24 o -4 12 0 1583.39 1721.33 199.14 o -3 12 0 643.86 767.36 145.68 o -2 12 0 30.15 40.57 99.93 o -1 12 0 163.22 179.62 108.53 o 0 12 0 179.10 193.75 100.74 o 1 12 0 955.88 853.96 151.50 o 2 12 0 2462.22 2463.85 210.21 o 3 12 0 2516.51 2764.38 219.39 o 4 12 0 2620.69 2840.93 147.16 o 5 12 0 1243.53 1165.42 103.69 o 6 12 0 2391.69 2293.18 134.99 o 7 12 0 0.82 -3.07 50.55 o 8 12 0 0.50 -18.59 50.61 o 9 12 0 103.51 33.16 54.58 o 10 12 0 1.68 7.28 87.84 o 11 12 0 513.53 522.91 143.42 o 12 12 0 384.43 249.47 133.88 o -3 13 0 1166.57 962.35 160.61 o -2 13 0 1298.74 1623.14 199.80 o -1 13 0 303.84 346.28 119.09 o 0 13 0 4.40 181.08 111.22 o 1 13 0 122.11 17.19 114.87 o 2 13 0 237.87 89.52 118.14 o 3 13 0 830.08 1192.01 171.90 o 4 13 0 1991.31 1993.45 201.55 o 5 13 0 1613.20 1612.83 123.00 o 6 13 0 117.53 26.59 77.25 o 7 13 0 761.37 771.50 95.98 o 8 13 0 39.15 1.56 142.69 o 9 13 0 566.27 575.65 137.45 o 10 13 0 1296.34 996.36 167.60 o 11 13 0 84.65 -76.92 108.09 o -1 14 0 227.02 352.18 129.73 o 0 14 0 37.54 50.70 102.34 o 1 14 0 77.09 -44.36 128.05 o 2 14 0 24.54 65.48 123.68 o 3 14 0 38.87 143.27 125.87 o 4 14 0 1262.72 1119.75 182.39 o 5 14 0 844.06 523.86 153.76 o 6 14 0 607.15 554.84 94.53 o 7 14 0 70.06 77.64 101.10 o 8 14 0 115.78 135.51 72.98 o 9 14 0 17.39 -93.59 62.61 o 10 14 0 1088.38 942.83 168.69 o 3 15 0 774.61 879.68 154.05 o 4 15 0 115.25 70.14 113.41 o 5 15 0 391.16 176.85 122.01 o 6 15 0 13.48 -154.27 112.75 o 7 15 0 68.34 -0.81 85.55 o -6 -15 1 2.87 286.62 110.50 o -5 -15 1 9.35 -148.92 99.28 o -4 -15 1 43.91 -133.59 96.73 o -9 -14 1 1380.78 1253.76 410.01 o -8 -14 1 23.41 -15.24 65.46 o -7 -14 1 554.85 454.71 91.37 o -6 -14 1 122.90 198.64 77.81 o -5 -14 1 44.46 -143.13 108.89 o -4 -14 1 394.71 190.84 139.27 o -3 -14 1 194.26 44.43 130.31 o -2 -14 1 221.20 236.14 145.24 o -1 -14 1 220.62 195.14 127.47 o 0 -14 1 245.27 277.88 124.48 o -11 -13 1 62.00 -117.27 95.71 o -10 -13 1 380.34 264.84 127.47 o -9 -13 1 1120.33 860.88 101.55 o -8 -13 1 1916.75 1816.14 132.02 o -7 -13 1 311.20 295.57 76.71 o -6 -13 1 475.44 425.68 133.70 o -5 -13 1 14.20 -21.13 61.24 o -4 -13 1 553.52 426.11 138.25 o -3 -13 1 1416.33 1284.95 180.86 o -2 -13 1 656.17 578.92 149.61 o -1 -13 1 493.80 487.58 138.03 o 0 -13 1 0.51 51.21 116.62 o 1 -13 1 524.42 439.29 140.58 o 2 -13 1 43.17 123.24 113.26 o -12 -12 1 25.05 -74.88 105.98 o -11 -12 1 951.23 790.37 160.03 o -10 -12 1 313.61 203.23 73.82 o -9 -12 1 219.71 56.76 67.59 o -8 -12 1 6.65 -79.32 52.88 o -7 -12 1 1132.52 1246.04 107.82 o -6 -12 1 137.73 169.43 62.57 o -5 -12 1 985.04 1111.62 105.04 o -4 -12 1 18.20 -49.98 53.16 o -3 -12 1 584.74 585.77 132.06 o -2 -12 1 1881.42 2111.45 205.48 o -1 -12 1 2281.93 2243.15 201.84 o 0 -12 1 3444.35 3681.28 256.03 o 1 -12 1 773.61 831.60 145.75 o 2 -12 1 2.11 130.82 103.94 o 3 -12 1 3.32 109.70 106.34 o 4 -12 1 600.99 708.29 153.03 o -13 -11 1 112.20 76.55 130.38 o -12 -11 1 128.66 181.37 117.20 o -11 -11 1 33.79 119.82 108.68 o -10 -11 1 3427.75 3210.04 192.77 o -9 -11 1 1323.10 1200.91 104.42 o -8 -11 1 422.61 474.36 118.40 o -7 -11 1 40.48 33.28 51.02 o -6 -11 1 667.56 747.78 83.09 o -5 -11 1 48.19 11.32 48.82 o -4 -11 1 1071.32 968.92 124.45 o -3 -11 1 1652.37 1651.93 107.44 o -2 -11 1 543.06 437.11 115.60 o -1 -11 1 552.91 619.71 121.71 o 0 -11 1 6964.71 7220.96 365.51 o 1 -11 1 2452.26 2803.64 209.41 o 2 -11 1 103.69 116.11 95.64 o 3 -11 1 18.53 42.25 97.02 o 4 -11 1 2.61 6.77 91.34 o 5 -11 1 250.79 312.19 126.16 o 6 -11 1 1425.20 1309.28 189.53 o -13 -10 1 144.49 298.71 130.16 o -12 -10 1 4.63 266.66 127.47 o -11 -10 1 576.74 528.74 136.65 o -10 -10 1 33.47 60.93 60.86 o -9 -10 1 716.57 676.56 140.87 o -8 -10 1 1955.22 1673.84 146.92 o -7 -10 1 4460.09 4368.77 178.49 o -6 -10 1 112.43 137.16 51.97 o -5 -10 1 40.08 25.13 41.69 o -4 -10 1 3.96 -33.60 66.14 o -3 -10 1 964.79 1159.57 124.37 o -2 -10 1 2401.14 2256.04 183.04 o -1 -10 1 4027.90 4239.30 251.88 o 0 -10 1 47.42 128.78 78.30 o 1 -10 1 3857.79 3920.26 242.12 o 2 -10 1 38.82 1.82 75.10 o 3 -10 1 556.51 657.66 116.54 o 4 -10 1 492.12 509.58 115.30 o 5 -10 1 138.98 207.88 108.89 o 6 -10 1 164.01 160.97 108.02 o 7 -10 1 989.64 995.08 219.06 o -14 -9 1 265.17 407.68 146.92 o -13 -9 1 90.07 249.62 126.67 o -12 -9 1 17.11 78.67 109.77 o -11 -9 1 57.37 33.21 85.59 o -10 -9 1 433.63 415.12 71.44 o -9 -9 1 663.31 897.31 85.04 o -8 -9 1 134.36 179.36 52.48 o -7 -9 1 2645.10 2746.24 131.47 o -6 -9 1 480.92 557.18 64.07 o -5 -9 1 892.26 963.95 80.79 o -4 -9 1 190.24 135.79 43.45 o -3 -9 1 216.40 214.73 93.34 o -2 -9 1 521.74 441.52 56.70 o -1 -9 1 2798.33 3111.09 199.65 o 0 -9 1 4104.46 4463.71 245.54 o 1 -9 1 198.14 183.77 76.77 o 2 -9 1 49.94 130.45 76.48 o 3 -9 1 2160.75 2289.87 254.64 o 4 -9 1 1188.27 1222.25 94.66 o 5 -9 1 1588.36 1592.95 112.64 o 6 -9 1 1336.40 1423.28 111.35 o 7 -9 1 14.53 77.20 68.00 o 8 -9 1 167.56 125.65 114.87 o -14 -8 1 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