Figure 2
Influence of controlled dehydration to different RHf on (a) unit-cell parameters and (b) diffraction data quality of Gpc-1 crystals. All crystals were dehydrated at 0.1% RH per minute and flash-cooled; full data were then collected at 100 K. (a) The changes in [beta] angle (squares), c dimension (circles) and unit-cell volume (diamonds) with RHf are plotted as solid, dotted and dashed lines, respectively. (b) The diffraction data quality as estimated by resolution (squares), anisotropy [Delta]B (circles) and Wilson B factor (diamonds) is plotted as solid, dotted and dashed lines, respectively. The resolution limit is defined as the resolution where the mean I/[sigma](I) is approximately 2.0.  [article HTML]