Acta Cryst. (2001). E57, m106-m108 [ doi:10.1107/S1600536801002586 ]
No syntax errors found ADDSYM reports no extra symmetry General Notes
REFLT_03 From the CIF: _diffrn_reflns_theta_max 27.49 From the CIF: _reflns_number_total 5607 Count of symmetry unique reflns 3181 Completeness (_total/calc) 176.27% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 2426 Fraction of Friedel pairs measured 0.763 Are heavy atom types Z>Si present yes Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF.
Copyright © International Union of Crystallography