(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2001). E57, m106-m108 [ doi:10.1107/S1600536801002586 ]

Dichloro[2-(2-Diphenylphosphino)-N-(1-phenylethyl)benzylamine-C,P]platinum

D. D. Ellis and A. L. Spek

Key indicators

Single-crystal X-ray study
T = 150 K
Mean (C-C) = 0.010 Å
R factor = 0.031
wR factor = 0.065
Data-to-parameter ratio = 18.9

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.49                 
         From the CIF: _reflns_number_total               5607                  
         Count of symmetry unique reflns         3181                           
         Completeness (_total/calc)            176.27%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured      2426                           
         Fraction of Friedel pairs measured     0.763                           
         Are heavy atom types Z>Si present          yes                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.