Acta Cryst. (2001). E57, m188-m189  [ doi:10.1107/S1600536801005086 ]

Aqua(n-pentyl)[3,3'-(propane-1,3-diyldinitrilo)bis(butan-2-one) dioximato-⁴N]cobalt(III) perchlorate

X.-J. Shen, H.-L. Chen, C.-Y. Duan and Y.-J. Liu

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.009 Å
• Disorder in solvent or counterion
• R factor = 0.066
• wR factor = 0.189
• Data-to-parameter ratio = 12.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_302  Alert C Anion/Solvent Disorder .......................      44.00 Perc.

PLAT_601  Alert C Structure Contains Solvent Accessible VOIDS of      49.00 A   3

PLAT_731  Alert C Bond    Calc     0.85(3), Rep   0.849(10) ....       3.00 s.u-Ratio
                     O1W  -H1WB    1.555   1.555

PLAT_732  Alert C Angle   Calc      110(4), Rep   109.8(18) ....       2.22 s.u-Ratio
                     H1WA -O1W  -H1WB    1.555   1.555   1.555

PLAT_735  Alert C D-H     Calc     0.88(8), Rep    0.87(17) ....       2.12 s.u-Ratio
                     O2   -H2      1.555   1.555

PLAT_735  Alert C D-H     Calc     0.85(3), Rep   0.849(10) ....       3.00 s.u-Ratio
                     O1W  -H1WB    1.555   1.555

PLAT_737  Alert C D...A   Calc    2.439(5), Rep   2.441(12) ....       2.40 s.u-Ratio
                     O2   -O1      1.555   1.555


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 7 Alert Level C = Please check

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