# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' kanagawa2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 171.82 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.0948 _cell_length_b 11.2408 _cell_length_c 14.0551 _cell_angle_alpha 85.524 _cell_angle_beta 71.679 _cell_angle_gamma 89.852 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3239.01 2269.64 11.50 o 2 0 0 2190.85 2251.54 23.16 o 3 0 0 3493.45 3519.30 30.01 o 4 0 0 9505.08 9997.67 108.72 o 5 0 0 192.48 193.62 14.35 o 6 0 0 906.08 919.50 24.47 o 7 0 0 1175.12 1212.38 266.86 o 8 0 0 1426.80 1453.15 61.09 o 9 0 0 1039.92 1047.31 24.22 o 10 0 0 573.04 502.90 88.82 o 11 0 0 260.44 345.81 80.17 o 12 0 0 106.06 112.88 92.16 o -12 1 0 359.97 369.30 95.02 o -11 1 0 305.57 271.35 82.29 o -10 1 0 64.10 53.18 60.27 o -9 1 0 1064.54 989.16 127.64 o -8 1 0 3053.62 3073.98 63.94 o -7 1 0 624.39 650.85 25.12 o -6 1 0 458.35 484.87 35.72 o -5 1 0 20.12 21.12 14.52 o -4 1 0 86.42 73.81 14.27 o -3 1 0 10097.79 10357.26 253.81 o -2 1 0 13296.49 13488.17 242.40 o -1 1 0 118.22 132.13 18.92 o 0 1 0 1106.59 8.24 8.07 o 1 1 0 10427.15 10719.88 195.74 o 2 1 0 134.74 138.49 28.06 o 3 1 0 15257.85 15982.60 32.46 o 4 1 0 11724.71 12392.50 69.98 o 5 1 0 54.86 69.98 17.21 o 6 1 0 1306.24 1345.82 134.66 o 7 1 0 2650.95 2825.15 86.70 o 8 1 0 2568.97 2786.00 287.99 o 9 1 0 20.32 15.82 24.88 o 10 1 0 6.18 10.52 20.55 o 11 1 0 318.10 333.66 79.68 o 12 1 0 163.61 166.95 86.86 o -12 2 0 118.21 84.50 95.42 o -11 2 0 110.52 220.13 82.21 o -10 2 0 1656.07 1442.63 210.67 o -9 2 0 544.02 520.19 31.73 o -8 2 0 521.69 531.77 31.16 o -7 2 0 527.33 538.38 20.47 o -6 2 0 392.08 380.72 18.35 o -5 2 0 1359.01 1311.81 21.78 o -4 2 0 3423.15 3435.95 268.09 o -3 2 0 3504.06 3378.12 128.21 o -2 2 0 3924.37 3742.61 25.61 o -1 2 0 4698.23 4982.32 205.20 o 0 2 0 297.81 288.07 32.05 o 1 2 0 1296.64 1465.79 48.28 o 2 2 0 751.12 744.23 28.22 o 3 2 0 2377.72 2454.62 24.63 o 4 2 0 35.77 25.69 21.78 o 5 2 0 4582.42 4842.85 138.08 o 6 2 0 3745.38 3850.11 60.03 o 7 2 0 345.33 355.11 27.89 o 8 2 0 426.41 438.79 46.00 o 9 2 0 3.18 6.52 22.76 o 10 2 0 904.67 839.41 54.89 o 11 2 0 980.56 849.93 78.87 o 12 2 0 242.43 238.81 172.17 o -12 3 0 841.12 980.18 102.77 o -11 3 0 944.03 1005.88 87.27 o -10 3 0 453.32 406.82 86.29 o -9 3 0 505.99 488.30 68.59 o -8 3 0 79.10 74.63 25.12 o -7 3 0 3089.24 3213.45 33.93 o -6 3 0 2002.50 1831.59 27.65 o -5 3 0 215.45 246.07 22.84 o -4 3 0 60.58 34.50 29.04 o -3 3 0 2976.23 3207.42 168.99 o -2 3 0 98.31 73.57 21.94 o -1 3 0 15797.24 17859.86 1143.55 o 0 3 0 13297.82 14002.08 592.37 o 1 3 0 585.44 628.09 23.49 o 2 3 0 7529.25 7583.50 155.94 o 3 3 0 643.29 658.51 23.90 o 4 3 0 4480.89 4523.87 44.29 o 5 3 0 57.85 77.40 25.77 o 6 3 0 798.77 779.87 30.83 o 7 3 0 1139.02 985.97 125.11 o 8 3 0 333.78 333.99 27.73 o 9 3 0 119.42 123.89 27.08 o 10 3 0 1594.65 1541.80 36.46 o 11 3 0 97.12 126.83 73.57 o 12 3 0 1.66 4.16 84.41 o -12 4 0 406.13 359.43 99.99 o -11 4 0 61.24 175.52 85.56 o -10 4 0 28.19 35.23 64.60 o -9 4 0 597.13 583.23 33.19 o -8 4 0 1171.15 1183.43 172.50 o -7 4 0 1853.89 1840.39 234.89 o -6 4 0 417.39 416.44 28.46 o -5 4 0 1178.96 1155.37 30.34 o -4 4 0 2219.39 2142.08 33.11 o -3 4 0 4179.04 3881.26 36.62 o -2 4 0 146.01 229.75 36.29 o -1 4 0 107.77 113.86 27.08 o 0 4 0 852.04 943.32 29.36 o 1 4 0 8578.18 8503.82 91.67 o 2 4 0 2500.44 2541.07 31.89 o 3 4 0 16.32 39.96 26.75 o 4 4 0 207.65 246.64 27.73 o 5 4 0 1815.66 1786.97 51.06 o 6 4 0 629.06 545.55 37.76 o 7 4 0 504.73 472.31 54.48 o 8 4 0 5187.77 5304.40 177.23 o 9 4 0 20.68 30.34 31.32 o 10 4 0 74.46 77.89 36.78 o 11 4 0 275.22 279.67 75.61 o -11 5 0 140.19 74.38 87.68 o -10 5 0 369.37 352.01 37.44 o -9 5 0 616.73 565.94 62.80 o -8 5 0 124.63 164.26 58.56 o -7 5 0 265.70 272.33 34.50 o -6 5 0 2231.14 2321.11 119.08 o -5 5 0 38.58 36.05 32.05 o -4 5 0 929.10 888.92 35.89 o -3 5 0 1058.61 1093.72 80.42 o -2 5 0 2196.39 2407.15 142.65 o -1 5 0 3538.34 3398.10 83.44 o 0 5 0 14594.51 15313.32 147.62 o 1 5 0 1304.97 1321.19 36.29 o 2 5 0 82.42 71.85 30.34 o 3 5 0 1341.92 1358.21 34.26 o 4 5 0 966.38 948.62 40.54 o 5 5 0 2081.47 2195.10 52.85 o 6 5 0 1401.79 1451.35 76.42 o 7 5 0 25.30 38.99 69.90 o 8 5 0 650.94 644.73 41.19 o 9 5 0 257.96 260.09 41.60 o 10 5 0 370.01 333.91 43.39 o 11 5 0 425.72 399.07 78.22 o -11 6 0 6.66 -25.45 95.91 o -10 6 0 4.60 14.27 38.50 o -9 6 0 343.55 286.76 52.77 o -8 6 0 137.18 157.65 55.05 o -7 6 0 229.39 214.91 40.86 o -6 6 0 948.05 974.23 41.92 o -5 6 0 4.00 -1.06 38.33 o -4 6 0 25.64 23.08 37.03 o -3 6 0 2230.96 2183.84 189.22 o -2 6 0 8842.52 9768.97 529.73 o -1 6 0 654.00 600.85 38.90 o 0 6 0 3411.64 3509.19 60.76 o 1 6 0 1061.50 1104.07 38.58 o 2 6 0 2811.01 2845.86 75.85 o 3 6 0 1828.87 1866.41 154.39 o 4 6 0 3185.09 3367.76 176.09 o 5 6 0 723.40 753.37 43.72 o 6 6 0 2410.77 2467.91 57.66 o 7 6 0 3326.38 3482.76 178.13 o 8 6 0 1309.08 1392.71 48.77 o 9 6 0 72.52 45.92 67.86 o 10 6 0 21.58 40.21 84.41 o 11 6 0 192.37 155.29 78.54 o -10 7 0 1138.04 931.74 50.24 o -9 7 0 1339.17 1228.21 64.60 o -8 7 0 48.43 74.38 79.36 o -7 7 0 62.74 30.42 45.43 o -6 7 0 1057.04 1043.15 48.77 o -5 7 0 2022.08 2167.45 58.72 o -4 7 0 1193.14 865.51 542.62 o -3 7 0 917.29 878.48 76.58 o -2 7 0 858.12 874.73 207.81 o -1 7 0 5587.65 5799.46 57.66 o 0 7 0 375.85 383.25 41.11 o 1 7 0 1773.87 1734.69 119.00 o 2 7 0 1435.49 1534.63 147.22 o 3 7 0 836.32 828.56 78.13 o 4 7 0 19.78 25.28 42.33 o 5 7 0 2304.89 2314.26 120.38 o 6 7 0 983.09 1081.56 67.86 o 7 7 0 16.07 -18.02 65.00 o 8 7 0 238.77 223.72 51.87 o 9 7 0 436.25 415.38 52.44 o 10 7 0 1366.83 1300.55 64.27 o -10 8 0 75.18 89.55 52.04 o -9 8 0 24.76 -6.85 55.71 o -8 8 0 224.89 194.19 51.95 o -7 8 0 3338.10 3398.59 90.53 o -6 8 0 3082.35 3250.80 133.02 o -5 8 0 14.59 71.20 51.30 o -4 8 0 660.70 695.46 103.01 o -3 8 0 498.26 485.61 47.47 o -2 8 0 1362.94 1430.47 55.05 o -1 8 0 129.31 149.17 50.16 o 0 8 0 80.52 106.52 47.14 o 1 8 0 94.82 57.66 46.82 o 2 8 0 3299.39 3327.47 155.04 o 3 8 0 1735.00 1881.58 176.74 o 4 8 0 772.80 907.92 50.49 o 5 8 0 59.39 84.17 49.10 o 6 8 0 52.54 14.44 57.42 o 7 8 0 64.75 71.69 51.38 o 8 8 0 462.95 448.99 54.73 o 9 8 0 481.29 464.32 50.81 o 10 8 0 241.67 210.42 96.57 o -9 9 0 816.79 723.27 62.23 o -8 9 0 23.46 42.57 57.17 o -7 9 0 321.49 380.23 108.23 o -6 9 0 35.44 12.72 115.98 o -5 9 0 475.26 587.23 58.15 o -4 9 0 1658.86 1579.24 60.60 o -3 9 0 821.51 831.17 74.22 o -2 9 0 196.16 230.16 55.05 o -1 9 0 1638.83 1684.70 63.13 o 0 9 0 931.71 851.16 61.17 o 1 9 0 2400.27 2335.38 295.08 o 2 9 0 1105.27 1114.51 221.19 o 3 9 0 669.28 676.13 65.33 o 4 9 0 712.85 765.52 61.09 o 5 9 0 71.45 93.14 53.42 o 6 9 0 455.62 493.03 56.19 o 7 9 0 503.78 547.51 58.23 o 8 9 0 245.58 255.93 56.44 o 9 9 0 45.19 -21.78 55.13 o -9 10 0 200.61 170.70 119.81 o -8 10 0 129.85 136.45 66.55 o -7 10 0 29.71 65.08 99.42 o -6 10 0 349.86 310.25 76.18 o -5 10 0 167.05 91.59 63.37 o -4 10 0 147.43 16.07 93.71 o -3 10 0 0.69 -15.17 77.97 o -2 10 0 125.21 41.02 83.44 o -1 10 0 4008.29 4023.09 573.20 o 0 10 0 27.04 91.75 63.62 o 1 10 0 70.29 12.40 80.74 o 2 10 0 278.99 247.04 54.89 o 3 10 0 206.13 282.60 85.56 o 4 10 0 523.56 540.58 69.00 o 5 10 0 777.39 858.90 61.74 o 6 10 0 700.97 708.26 72.59 o 7 10 0 68.83 120.30 73.16 o 8 10 0 136.85 124.46 61.17 o -8 11 0 23.89 6.28 72.18 o -7 11 0 174.71 154.47 73.73 o -6 11 0 141.17 120.38 70.22 o -5 11 0 74.09 62.23 70.14 o -4 11 0 561.84 660.39 71.28 o -3 11 0 448.85 397.11 114.27 o -2 11 0 724.09 648.24 69.57 o -1 11 0 193.28 232.12 66.80 o 0 11 0 62.33 79.36 71.12 o 1 11 0 10.13 80.99 73.73 o 2 11 0 672.49 664.63 247.78 o 3 11 0 605.20 651.34 67.94 o 4 11 0 150.47 163.61 66.14 o 5 11 0 46.87 72.51 65.41 o 6 11 0 410.24 401.60 67.69 o 7 11 0 517.27 545.31 67.86 o -7 12 0 10.16 16.80 101.95 o -6 12 0 247.46 263.68 121.69 o -5 12 0 393.45 423.13 80.50 o -4 12 0 98.66 53.18 87.84 o -3 12 0 19.29 33.44 94.77 o -2 12 0 94.71 43.47 74.71 o -1 12 0 627.28 598.97 74.71 o 0 12 0 70.60 157.65 79.60 o 1 12 0 1356.55 1275.27 182.37 o 2 12 0 660.04 621.00 68.84 o 3 12 0 101.08 62.31 68.51 o 4 12 0 483.44 497.92 74.55 o 5 12 0 58.87 34.26 70.47 o 6 12 0 227.94 244.60 80.83 o -5 13 0 13.52 -41.51 89.31 o -4 13 0 264.78 189.38 87.02 o -3 13 0 492.96 469.38 91.67 o -2 13 0 217.94 212.63 97.55 o -1 13 0 882.87 763.24 253.41 o 0 13 0 234.39 214.50 83.44 o 1 13 0 56.93 79.52 124.13 o 2 13 0 178.52 185.14 88.17 o 3 13 0 89.79 134.98 112.23 o 4 13 0 213.02 208.30 114.10 o 5 13 0 14.51 9.22 77.89 o -3 14 0 86.02 118.91 96.57 o -2 14 0 24.49 20.39 96.81 o -1 14 0 8.71 9.79 96.81 o 0 14 0 826.44 910.21 107.58 o 1 14 0 718.77 649.70 103.25 o 2 14 0 25.99 26.91 76.58 o 3 14 0 1.60 17.78 84.82 o -2 -14 1 341.31 337.17 100.97 o -1 -14 1 144.36 134.90 138.16 o 0 -14 1 88.28 236.60 119.57 o 1 -14 1 1297.64 1139.71 101.62 o 2 -14 1 331.33 317.43 97.63 o 3 -14 1 134.25 129.11 194.36 o -4 -13 1 47.83 79.36 150.97 o -3 -13 1 85.34 48.45 78.54 o -2 -13 1 87.37 103.99 71.04 o -1 -13 1 732.05 586.09 74.71 o 0 -13 1 327.73 395.08 108.15 o 1 -13 1 1226.51 1065.82 123.32 o 2 -13 1 11.35 31.40 135.23 o 3 -13 1 307.88 380.48 88.82 o 4 -13 1 229.57 231.87 86.29 o 5 -13 1 215.71 272.00 92.00 o -6 -12 1 6.83 47.88 76.42 o -5 -12 1 0.22 92.49 74.22 o -4 -12 1 5.10 -31.81 88.74 o -3 -12 1 543.22 599.22 75.85 o -2 -12 1 457.34 434.39 69.73 o -1 -12 1 13.29 17.86 75.61 o 0 -12 1 103.02 72.67 74.46 o 1 -12 1 21.31 -25.45 94.53 o 2 -12 1 68.39 88.25 75.03 o 3 -12 1 374.60 406.33 78.54 o 4 -12 1 894.18 825.55 118.67 o 5 -12 1 127.10 203.82 105.95 o 6 -12 1 345.43 288.31 105.62 o 7 -12 1 194.98 203.33 107.09 o -7 -11 1 85.15 80.74 69.57 o -6 -11 1 735.34 720.66 87.68 o -5 -11 1 315.28 332.60 69.16 o -4 -11 1 538.43 616.35 136.12 o -3 -11 1 236.82 271.10 69.00 o -2 -11 1 20.85 -31.97 62.88 o -1 -11 1 141.68 133.27 101.62 o 0 -11 1 25.52 33.93 119.32 o 1 -11 1 911.77 858.82 89.14 o 2 -11 1 78.63 106.60 69.16 o 3 -11 1 142.83 187.02 71.12 o 4 -11 1 140.01 194.28 72.83 o 5 -11 1 238.47 259.60 172.50 o 6 -11 1 223.32 226.49 73.00 o 7 -11 1 416.51 440.42 76.18 o 8 -11 1 3.05 8.73 77.73 o -8 -10 1 382.23 386.43 67.45 o -7 -10 1 121.87 179.43 62.88 o -6 -10 1 947.33 977.08 67.61 o -5 -10 1 30.57 80.58 69.98 o -4 -10 1 261.29 253.49 68.27 o -3 -10 1 1141.85 1085.56 165.48 o -2 -10 1 17.54 16.39 68.84 o -1 -10 1 201.65 276.65 155.94 o 0 -10 1 530.74 507.22 136.94 o 1 -10 1 571.18 544.98 97.14 o 2 -10 1 30.42 67.53 81.89 o 3 -10 1 1091.81 954.90 86.45 o 4 -10 1 228.89 343.37 67.86 o 5 -10 1 144.80 95.02 83.44 o 6 -10 1 75.18 15.90 148.44 o 7 -10 1 85.60 88.08 65.90 o 8 -10 1 228.52 297.77 149.34 o 9 -10 1 330.49 351.60 100.48 o -9 -9 1 101.66 80.91 56.44 o -8 -9 1 334.02 375.17 69.73 o -7 -9 1 1095.28 1187.02 61.90 o -6 -9 1 49.35 34.66 56.85 o -5 -9 1 933.83 961.59 64.19 o -4 -9 1 18.59 17.62 63.62 o -3 -9 1 526.48 555.42 56.85 o -2 -9 1 329.25 342.39 51.87 o -1 -9 1 654.24 738.85 77.56 o 0 -9 1 1671.54 1716.99 215.73 o 1 -9 1 765.63 727.10 169.32 o 2 -9 1 574.26 626.79 137.51 o 3 -9 1 24.63 -43.23 56.44 o 4 -9 1 103.23 106.11 58.89 o 5 -9 1 21.03 116.47 59.13 o 6 -9 1 701.55 749.04 62.56 o 7 -9 1 1229.32 1249.74 64.27 o 8 -9 1 24.54 59.78 69.08 o 9 -9 1 72.24 19.41 183.35 o 10 -9 1 69.19 60.68 60.03 o -9 -8 1 181.30 156.76 47.71 o -8 -8 1 248.95 274.04 50.49 o -7 -8 1 376.14 415.95 54.32 o -6 -8 1 309.75 321.51 50.81 o -5 -8 1 61.62 57.42 49.10 o -4 -8 1 227.16 268.09 59.62 o -3 -8 1 1467.62 1506.00 136.69 o -2 -8 1 664.63 661.94 109.37 o -1 -8 1 2544.81 2634.70 184.73 o 0 -8 1 1409.67 1409.43 54.32 o 1 -8 1 3373.00 3566.20 442.38 o 2 -8 1 44.01 40.05 47.71 o 3 -8 1 208.01 142.16 62.23 o 4 -8 1 625.16 613.33 53.67 o 5 -8 1 849.47 889.00 57.42 o 6 -8 1 566.51 547.02 55.38 o 7 -8 1 46.34 84.09 53.58 o 8 -8 1 288.20 328.11 61.01 o 9 -8 1 344.62 333.25 69.57 o 10 -8 1 270.26 260.75 91.92 o -10 -7 1 9.92 100.97 76.58 o -9 -7 1 346.78 402.33 51.87 o -8 -7 1 1053.45 1041.35 96.00 o -7 -7 1 14.06 36.38 63.05 o -6 -7 1 1754.37 1736.24 49.67 o -5 -7 1 186.12 234.65 43.39 o -4 -7 1 661.01 651.09 62.23 o -3 -7 1 2710.82 2920.81 194.93 o -2 -7 1 3122.15 3044.70 174.70 o -1 -7 1 236.86 239.46 48.85 o 0 -7 1 1259.21 1310.58 45.10 o 1 -7 1 417.06 450.86 44.29 o 2 -7 1 519.53 460.16 44.61 o 3 -7 1 1722.61 1701.91 48.04 o 4 -7 1 3322.46 3405.28 68.59 o 5 -7 1 83.52 75.61 47.96 o 6 -7 1 9.43 51.95 46.82 o 7 -7 1 2408.79 2460.00 57.01 o 8 -7 1 422.84 454.86 165.81 o 9 -7 1 125.24 122.99 63.13 o 10 -7 1 65.83 44.94 49.18 o 11 -7 1 366.85 331.46 101.62 o -10 -6 1 530.44 601.99 154.80 o -9 -6 1 471.64 536.42 45.59 o -8 -6 1 169.04 219.40 47.96 o -7 -6 1 51.19 48.04 72.59 o -6 -6 1 1652.51 1787.05 60.44 o -5 -6 1 4140.19 4307.17 235.54 o -4 -6 1 934.84 1054.65 41.43 o -3 -6 1 265.70 226.00 63.70 o -2 -6 1 2.53 7.26 34.91 o -1 -6 1 115.80 101.62 46.49 o 0 -6 1 1986.70 2093.23 43.31 o 1 -6 1 654.24 707.86 41.35 o 2 -6 1 255.32 234.57 37.03 o 3 -6 1 123.16 165.00 89.63 o 4 -6 1 443.57 471.82 46.16 o 5 -6 1 1083.04 1107.74 104.97 o 6 -6 1 126.93 108.72 41.92 o 7 -6 1 1355.68 1406.17 154.23 o 8 -6 1 75.05 78.13 43.31 o 9 -6 1 20.96 62.56 55.38 o 10 -6 1 584.30 502.24 121.61 o 11 -6 1 1087.72 1005.63 54.81 o -11 -5 1 52.50 59.38 164.91 o -10 -5 1 83.26 62.23 74.71 o -9 -5 1 1.56 8.07 36.86 o -8 -5 1 856.40 903.35 34.74 o -7 -5 1 1066.21 1095.43 87.35 o -6 -5 1 3248.49 3300.31 111.25 o -5 -5 1 369.92 333.74 35.48 o -4 -5 1 207.18 162.22 35.97 o -3 -5 1 804.56 859.23 97.55 o -2 -5 1 38.46 17.13 37.03 o -1 -5 1 2088.17 2089.80 57.01 o 0 -5 1 443.93 475.66 35.72 o 1 -5 1 252.43 400.70 47.88 o 2 -5 1 5520.56 5815.29 399.07 o 3 -5 1 4531.47 4687.23 204.88 o 4 -5 1 252.75 226.98 34.58 o 5 -5 1 9.44 -10.36 35.97 o 6 -5 1 21.18 35.80 42.49 o 7 -5 1 31.65 59.78 70.30 o 8 -5 1 801.56 806.14 54.56 o 9 -5 1 269.07 226.33 51.95 o 10 -5 1 22.26 22.92 38.58 o 11 -5 1 6.72 -6.52 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