Acta Cryst. (2001). E57, m556-m557  [ doi:10.1107/S1600536801016403 ]

Hexakis(dimethyl sulfoxide)nickel(II) dinitrate dimethyl sulfoxide disolvate

A. J. Blake, M. Felloni, P. Hubberstey, M. Schröder and C. Wilson

Online 10 October 2001

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (O-N) = 0.002 Å
• R factor = 0.021
• wR factor = 0.057
• Data-to-parameter ratio = 21.8

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           28.65                 
         From the CIF: _reflns_number_total               4251                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         4850                           
         Completeness (_total/calc)             87.65%                          
          Alert B: < 90% complete (theta max?)                                  

 Alert Level C:



ABSTM_02  Alert C The ratio of expected to reported Tmax/Tmin(RR) is > 1.10     
          Tmin and Tmax reported:      0.703     0.769                          
          Tmin and Tmax expected:      0.638     0.769                          
          RR =      1.102                                                       
          Please check that your absorption correction is appropriate.          


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 1 Alert Level C = Please check

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