Acta Crystallographica Section E

Structure Reports Online

Volume 57, Part 12 (December 2001)

	Cover illustration: Radical cyclization of a 1,6-diene by a sulfonyl radical yields this highly substituted piperidine. In this enantiopure compound, one phenyl ring is face-to-face with the p-tolyl ring. See Reynoso-Paz, Olmstead, Kurth & Schore [Acta Cryst. E57, o1177-o1178].

• inorganic compounds
• metal-organic compounds
• organic compounds

inorganic compounds

Acta Cryst. (2001). E57, i109-i111  [ doi:10.1107/S1600536801017998 ] Zinc(II) sulfate tetrahydrate A. J. Blake, P. A. Cooke, P. Hubberstey and C. L. Sampson Online 10 November 2001

metal-organic compounds

Acta Cryst. (2001). E57, m553-m555  [ doi:10.1107/S1600536801018566 ] A trigonal-bipyramidal coordinated ytterbium(III) alkyl: tris(trimethylsilylmethyl)bis(tetrahydrofuran-O)ytterbium(III) M. Niemeyer Online 10 November 2001

Acta Cryst. (2001). E57, m556-m557  [ doi:10.1107/S1600536801016403 ] Hexakis(dimethyl sulfoxide)nickel(II) dinitrate dimethyl sulfoxide disolvate A. J. Blake, M. Felloni, P. Hubberstey, M. Schröder and C. Wilson Online 10 October 2001

Acta Cryst. (2001). E57, m558-m560  [ doi:10.1107/S1600536801018360 ] Metal-nucleobase interaction: dibromobis(cytosine)cadmium(II) P. T. Muthiah, J. J. Robert, S. B. Raj, G. Bocelli and R. Ollá Online 10 November 2001

Acta Cryst. (2001). E57, m561-m563  [ doi:10.1107/S1600536801018414 ] Quinolinium trichloro(quinoline)zinc(II) W.-G. Wang, X.-F. Zhang, D.-G. Huang, H.-P. Zhu, C.-N. Chen and Q.-T. Liu Online 10 November 2001

Acta Cryst. (2001). E57, m564-m565  [ doi:10.1107/S1600536801017214 ] Bis(2-naphthoxy)[5,10,15,20-tetra-p-tolylporphyrinato]tin(IV) G. D. Fallon, M.A.-P. Lee and S. J. Langford Online 10 November 2001

Acta Cryst. (2001). E57, m566-m567  [ doi:10.1107/S1600536801018281 ] Bis(dithioacetato-2S)bis(triphenylphosphine-P)copper(I) 1.5-toluene solvate T. C. Deivaraj and J. J. Vittal Online 10 November 2001

Acta Cryst. (2001). E57, m568-m569  [ doi:10.1107/S1600536801018554 ] Bis(p-chlorothiophenolato)bis(tri-n-butylphosphine)nickel(II) I. A. Guzei, M. J. Moloto and J. Darkwa Online 10 November 2001

Acta Cryst. (2001). E57, m570-m572  [ doi:10.1107/S1600536801018876 ] [Indenyllithium·2(N,N,N'-trimethylethylenediamine)]: N-H hydrogen bridges to the indenyl anion G. Boche, B. Ledig, M. Marsch and K. Harms Online 10 November 2001

Acta Cryst. (2001). E57, m573-m575  [ doi:10.1107/S1600536801018852 ] Diethylammonium heptabromidedicadmium(II) R. D. Willett and B. Twamley Online 10 November 2001

Acta Cryst. (2001). E57, m576-m577  [ doi:10.1107/S1600536801018712 ] Double cyclometallation of bis[3-(3-methoxyphenyl)pyrazol-1-yl]methane in a bis[(acetylacetonato)palladium(II)] complex O. Juanes, J.-C. Rodriguez-Ubis and C. J. Pastor Online 10 November 2001

Acta Cryst. (2001). E57, m578-m580  [ doi:10.1107/S1600536801018797 ] A solvated ytterbium diaryl: bis(1,1':3',1''-terphenyl-C2')bis(tetrahydrofuran-O)ytterbium(II) M. Niemeyer Online 10 November 2001

Acta Cryst. (2001). E57, m581-m583  [ doi:10.1107/S1600536801019092 ] Di--chloro-bis{chloro[2-(4-methylphenylamino)-1,2-diphenylethanoximato]copper(II)} H. Puschmann, J. A. K. Howard, B. Soto, R. Bonne and O. Au-Alvarez Online 17 November 2001

Acta Cryst. (2001). E57, m584-m586  [ doi:10.1107/S1600536801019171 ] {[-N,N'-Bis(salicylidene)-2,2'-dimethyl-1,3-propanediamine](piperidine)copper(II)}dibromozinc(II) I. Svoboda, C. Arici, H. Nazir, Z. Durmus, O. Atakol and H. Fuess Online 17 November 2001

Acta Cryst. (2001). E57, m587-m588  [ doi:10.1107/S1600536801019420 ] Monoclinic form of dichlorobis(quinoline-N)cobalt(II) W. Wang, D. Huang, H. Zhu, C. Chen and Q. Liu Online 24 November 2001

Acta Cryst. (2001). E57, m589-m590  [ doi:10.1107/S1600536801019663 ] Diazido{N,N'-bis[2-(2-pyridyl)ethylene]-1,3-diaminopropane}nickel(II) monohydrate D.-Z. Niu, B.-W. Sun, Z.-S. Lu, Z.-M. Wang and C.-H. Yan Online 24 November 2001

Acta Cryst. (2001). E57, m591-m594  [ doi:10.1107/S1600536801017792 ] Tetraaqua(8-hydroxyquinoline-5-sulfonato-N,O)nickel(II) monohydrate S. B. Raj, P. T. Muthiah, G. Bocelli and L. Righi Online 24 November 2001

Acta Cryst. (2001). E57, m595-m596  [ doi:10.1107/S1600536801019419 ] Double cyclometallation of bis[3-(3-bromophenyl)pyrazol-1-yl]methane in the bis[acetylacetonatopalladium(II)] complex O. Juanes, J.-C. Rodriguez-Ubis and C. J. Pastor Online 24 November 2001

Acta Cryst. (2001). E57, m597-m599  [ doi:10.1107/S160053680101995X ] Bis(acetato-O)diaqua(2,2'-bipyridyl-N,N')cobalt(II) (OC-13): a two-dimensional material R. Carballo, B. Covelo, E. García-Martínez and E. M. Vázquez-López Online 30 November 2001

Acta Cryst. (2001). E57, m600-m602  [ doi:10.1107/S1600536801019857 ] Bis(triethanolamine-N,O,O')zinc(II) disaccharinate Y. Topcu, V. T. Yilmaz and C. Thöne Online 30 November 2001

Acta Cryst. (2001). E57, m603-m604  [ doi:10.1107/S1600536801019833 ] (N,N-Diethyldithiocarbamato)(tricyclohexylphosphine)gold(I) S. Y. Ho and E. R. T. Tiekink Online 30 November 2001

Acta Cryst. (2001). E57, m605-m606  [ doi:10.1107/S1600536801019808 ] Aqua-di-2-chloro-bis(diethylenetriamine)dicopper(II) dichloride R. D. Willett Online 30 November 2001

organic compounds

Acta Cryst. (2001). E57, o1139-o1140  [ doi:10.1107/S1600536801018311 ] 1,3,1',3'-Tetrahydro-[2,2']biindenylidene J. Jovanovic, M. Schürmann, H. Preut and M. Spiteller Online 10 November 2001

Acta Cryst. (2001). E57, o1141-o1142  [ doi:10.1107/S1600536801018396 ] 2,4,6-Collidine A. D. Bond and J. E. Davies Online 10 November 2001

Acta Cryst. (2001). E57, o1143-o1144  [ doi:10.1107/S1600536801018529 ] 4,5,4',5'-Tetrakis(2-methyl-thiophen-3-yl)-[2,2']bi[[1,3]dithiolylidene] T. Gelbrich, S. J. Roberts-Bleming, M. Kalaji, P. J. Murphy and M. B. Hursthouse Online 10 November 2001

Acta Cryst. (2001). E57, o1145-o1146  [ doi:10.1107/S1600536801018384 ] (±)-(1RS,2SR)-1,2-Bis(2'-methyl-3'-oxocyclohex-1'-enyl)-1,2-diphenylethane H. Ibrahim, T. Bach and K. Harms Online 10 November 2001

Acta Cryst. (2001). E57, o1147-o1148  [ doi:10.1107/S1600536801018190 ] 1,5-Di-tert-butyl-3-hydroxy-7-methylene-1-azonia-5-azacyclooctane iodide J. L. Flippen-Anderson, T. Axenrod, L. Qi and R. D. Gilardi Online 10 November 2001

Acta Cryst. (2001). E57, o1149-o1151  [ doi:10.1107/S160053680101858X ] D-Phenylglycinium perchlorate S. Ramaswamy, B. Sridhar, V. Ramakrishnan and R. K. Rajaram Online 10 November 2001

Acta Cryst. (2001). E57, o1152-o1153  [ doi:10.1107/S1600536801018268 ] 1-[(2-Nitrophenyl)hydrazono]-1H-naphthalen-2-one (Pigment Orange 2) from powder data A. V. Yatsenko, K. A. Paseshnichenko, V. V. Chernyshev and H. Schenk Online 10 November 2001

Acta Cryst. (2001). E57, o1154-o1155  [ doi:10.1107/S1600536801018426 ] 4-Chloro-2-(phenyldiazenyl)phenol from powder data: a form stable at room temperature A. V. Yatsenko, K. A. Paseshnichenko and H. Schenk Online 10 November 2001

Acta Cryst. (2001). E57, o1156-o1157  [ doi:10.1107/S1600536801018438 ] 4-Chloro-2-(phenyldiazenyl)phenol from powder data: a form metastable at room temperature A. V. Yatsenko, K. A. Paseshnichenko and H. Schenk Online 10 November 2001

Acta Cryst. (2001). E57, o1158-o1160  [ doi:10.1107/S1600536801018773 ] A taxane diterpenoid from the needles of Taxus wallichiana S. K. Chattopadhyay, A. Sharon, U. Yadav, S. Srivastava, V. K. Mehta and P. R. Maulik Online 10 November 2001

Acta Cryst. (2001). E57, o1161-o1162  [ doi:10.1107/S1600536801018694 ] N,N'-Bis(2-methoxyphenyl)pyridine-2,6-dicarboxamide Q. Y. Yang, Z. Y. Zhou and J. Y. Qi Online 10 November 2001

Acta Cryst. (2001). E57, o1163-o1165  [ doi:10.1107/S1600536801018670 ] 1,3-Bis(8-chlorotheophyllin-7-yl)propane: a molecule with no intramolecular stacking P. R. Maulik, K. Avasthi, S. Sarkhel, A. Sharon, D. S. Rawat and C. Bal Online 10 November 2001

Acta Cryst. (2001). E57, o1166-o1167  [ doi:10.1107/S1600536801018700 ] 2-{5,5-Dimethyl-3-[2-(2-methoxyphenyl)vinyl]cyclohex-2-enylidene}malononitrile T. Kolev, Z. Glavcheva, M. Schürmann, D.-C. Kleb, H. Preut and P. Bleckmann Online 10 November 2001

Acta Cryst. (2001). E57, o1168-o1170  [ doi:10.1107/S160053680101902X ] Tetraphenylphosphonium 7-phenylethynyl-8-phenyl-7,8-nido-dicarbadecahydroundecaborate(1-) G. M. Rosair, F. H. Schmidt and A. J. Welch Online 17 November 2001

Acta Cryst. (2001). E57, o1171-o1172  [ doi:10.1107/S1600536801018888 ] Tetra-n-butylammonium 7-phenylethynyl-8-phenyl-7,8-nido-dicarbadecahydroundecaborate(1-) G. M. Rosair, F. H. Schmidt and A. J. Welch Online 17 November 2001

Acta Cryst. (2001). E57, o1173-o1174  [ doi:10.1107/S1600536801018864 ] Chloral adduct of N-hydroxypiperidine W. Kliegel, U. Riebe, B. O. Patrick, S. J. Rettig and J. Trotter Online 17 November 2001

Acta Cryst. (2001). E57, o1175-o1176  [ doi:10.1107/S1600536801019067 ] 2H-Chromene-2-thione P. Munshi and T. N. G. Row Online 17 November 2001

Acta Cryst. (2001). E57, o1177-o1178  [ doi:10.1107/S1600536801019055 ] An enantiopure bicyclic pentasubstituted piperidine M. Reynoso-Paz, M. M. Olmstead, M. J. Kurth and N. E. Schore Online 17 November 2001

Acta Cryst. (2001). E57, o1179-o1182  [ doi:10.1107/S1600536801018657 ] Hydrogen bonding patterns in trimethoprim sulfate trihydrate [trimethoprim = 2,4-diamino-5-(3,4,5-methoxybenzyl)pyrimidine] P. T. Muthiah, B. Umadevi, N. Stanley, X. Shui and D. S. Eggleston Online 17 November 2001

Acta Cryst. (2001). E57, o1183-o1184  [ doi:10.1107/S1600536801019006 ] 5,5-Dihydroxy-1,3-dipropionyl-1,3-diazacyclohexane R. D. Gilardi, T. Axenrod, J. Sun and J. L. Flippen-Anderson Online 17 November 2001

Acta Cryst. (2001). E57, o1185-o1186  [ doi:10.1107/S1600536801019018 ] 1,5-Diacetyl-7,7-dinitro-1,5-diazacyclooctan-3-one ethylene acetal R. D. Gilardi, T. Axenrod, X.-P. Guan and J. L. Flippen-Anderson Online 17 November 2001

Acta Cryst. (2001). E57, o1187-o1188  [ doi:10.1107/S1600536801019122 ] 3-Acétoxy nor-31-lanostène-7,11-dione M. Daoubi, A. Benharref and M. Pierrot Online 17 novembre 2001

Acta Cryst. (2001). E57, o1189-o1190  [ doi:10.1107/S1600536801019237 ] Styrene at 83  K N. Yasuda, H. Uekusa and Y. Ohashi Online 17 November 2001

Acta Cryst. (2001). E57, o1191-o1193  [ doi:10.1107/S1600536801019195 ] Styrene at 120  K A. D. Bond and J. E. Davies Online 17 November 2001

Acta Cryst. (2001). E57, o1194-o1195  [ doi:10.1107/S1600536801017007 ] (2S*)-2-Hydroxy-2-[(2S*,5R*)-5-(1-hydroxy-1-methylethyl)tetrahydrofuran-2-yl]-1-phenylethanone M. E. Light and M. B. Hursthouse Online 17 November 2001

Acta Cryst. (2001). E57, o1196-o1197  [ doi:10.1107/S1600536801017019 ] (2S)-1-(4-Fluorophenyl)-2-hydroxy-2-[(2S,5R)-5-(1-hydroxy-1-methylethyl)-tetrahydrofuran-2-yl]ethanone M. E. Light and M. B. Hursthouse Online 17 November 2001

Acta Cryst. (2001). E57, o1198-o1199  [ doi:10.1107/S1600536801018669 ] Orthorhombic form of 6-phenylhex-5-ene-2,4-dione A. F. Arrieta and A. Mostad Online 17 November 2001

Acta Cryst. (2001). E57, o1200-o1202  [ doi:10.1107/S1600536801019183 ] 2,9,18-Trioxo-3,5,8,19-tetraaza-[55,13][11]metaphane monohydrate T. H. Kim, S. Y. Yang, S. S. Lee, J. S. Kim and J. Kim Online 17 November 2001

Acta Cryst. (2001). E57, o1203-o1205  [ doi:10.1107/S1600536801019511 ] 2,5-Dichloroaniline, a monoclinic structure with a pseudo-tetragonal unit cell P. J. Cox Online 24 November 2001

Acta Cryst. (2001). E57, o1206-o1208  [ doi:10.1107/S1600536801018001 ] N-HO and O-HO hydrogen bonds in crystal engineering: trimethoprim hydrogen glutarate J. J. Robert, S. B. Raj and P. T. Muthiah Online 24 November 2001

Acta Cryst. (2001). E57, o1209-o1210  [ doi:10.1107/S1600536801019274 ] 2-Chlorobenzoxazolo[3,2-b]isoquinolin-6-one T. Ravishankar, K. Chinnakali, A. Senthilvelan, H.-K. Fun, V. T. Ramakrishnan, S. Chantrapromma, I. A. Razak and A. Usman Online 24 November 2001

Acta Cryst. (2001). E57, o1211-o1212  [ doi:10.1107/S1600536801019432 ] trans-2-(2-Bromo-4-methylphenyloxy)cyclohexanol T. Ravishankar, K. Chinnakali, K. Sriraghavan, V. T. Ramakrishnan, H.-K. Fun, S. Chantrapromma, I. A. Razak and A. Usman Online 24 November 2001

Acta Cryst. (2001). E57, o1213-o1215  [ doi:10.1107/S1600536801019730 ] O,O-Diphenyl 2-methyl-1-(3-phenylthioureido)propanephosphonate L. Checinska, M. Malecka, T. A. Olszak and Z. H. Kudzin Online 24 November 2001

Acta Cryst. (2001). E57, o1216-o1218  [ doi:10.1107/S1600536801019729 ] O,O-Diphenyl 1-(3-phenylthioureido)ethanephosphonate L. Checinska, M. Malecka, T. A. Olszak and Z. H. Kudzin Online 24 November 2001

Acta Cryst. (2001). E57, o1219-o1221  [ doi:10.1107/S1600536801019390 ] erythro-2-(2,6-Dimethoxyphenoxy)-1-(3,4,5-trimethoxyphenyl)-1,3-propanediol V. Langer and K. Lundquist Online 24 November 2001

Acta Cryst. (2001). E57, o1222-o1223  [ doi:10.1107/S160053680101978X ] Tri(2-thienyl)arsine oxide H. Mahalakshmi, V. K. Jain and E. R. T. Tiekink Online 24 November 2001

Acta Cryst. (2001). E57, o1224-o1226  [ doi:10.1107/S1600536801018682 ] 2,3-Dihydroxybenzoic acid N. Okabe and H. Kyoyama Online 24 November 2001

Acta Cryst. (2001). E57, o1227-o1229  [ doi:10.1107/S1600536801019754 ] Intermolecular hydrogen bonding in (2S)-2-(1-oxo-1H-2,3-dihydroisoindol-2-yl)propanoic acid J. F. Gallagher and C. Murphy Online 24 November 2001

Acta Cryst. (2001). E57, o1230-o1232  [ doi:10.1107/S1600536801019961 ] Spiro[2-carbomethoxy-5-(4-methoxyphenyl)-3-phenylpyrrolidine-4,3'-chroman-4'-one] M. N. Nissa, V. Rajakannan, M.-J. Kim and D. Velmurugan Online 30 November 2001

Acta Cryst. (2001). E57, o1233-o1234  [ doi:10.1107/S1600536801019973 ] 1,4-Benzenedimethanol N. Shan and W. Jones Online 30 November 2001

Acta Cryst. (2001). E57, o1235-o1236  [ doi:10.1107/S1600536801020220 ] 8a-Ethyl 2-methyl (4aR,8aS)-3-oxoperhydro-2,8a-naphthalenedicarboxylate H. Surya Prakash Rao, S. Rajamathe, S. Shanmuga Sundara Raj and H.-K. Fun Online 30 November 2001

Acta Cryst. (2001). E57, o1237-o1239  [ doi:10.1107/S1600536801020049 ] 3,6-Di-2-pyridyl-4-{[(2-pyridyl)carbonyldiazenyl](2-pyridyl)methyl}-1H-1,2,4,5-tetrazine: the proton-assisted hydrolysis product of 3,6-di-2-pyridyl-1,2,4,5-tetrazine (dptz) L.-Y. Wang, C.-X. Du and Y.-Q. Fu Online 30 November 2001

Acta Cryst. (2001). E57, o1240-o1241  [ doi:10.1107/S1600536801020268 ] 5-(4-Chlorophenyl)-3-oxa-4-azatricyclo[5.2.1.02,6]dec-4-ene A. Thiruvalluvar, V. Parthasarathi, V. Kabaleeswaran, S. S. Rajan, A. Nagarajan and M. K. Pillay Online 30 November 2001

Acta Cryst. (2001). E57, o1242-o1244  [ doi:10.1107/S1600536801019869 ] 2,6-Lutidine A. D. Bond, J. E. Davies and A. J. Kirby Online 30 November 2001

Acta Cryst. (2001). E57, o1245-o1246  [ doi:10.1107/S1600536801019225 ] Methyl 5-methyl-3,4-diphenyl-1H-pyrrole-2-carboxylate M. E. Light, S. Camiolo, P. A. Gale and M. B. Hursthouse Online 30 November 2001

Acta Cryst. (2001). E57, o1247-o1249  [ doi:10.1107/S1600536801020104 ] 1-(2,6-Dimethylphenylamino)propane-1,2-dione dioxime T. Hökelek, A. Zülfikaroglu and H. Bati Online 30 November 2001

Acta Cryst. (2001). E57, o1250-o1251  [ doi:10.1107/S1600536801020128 ] Redetermination of N,N-dimethyl-N-{4-[(E)-(4-methyl-3-nitrophenyl)diazenyl]phenyl}amine at 193 K: another example of dynamic disorder of substituted azobenzene compounds O. Ya. Borbulevych and M. Yu. Antipin Online 30 November 2001

Acta Cryst. (2001). E57, o1252-o1254  [ doi:10.1107/S1600536801020153 ] Photochemical formation of 2-acetyl-7-methylbenz[e]indole A. Visnjevac, N. Basaric, B. Kojic-Prodic and M. Sindler-Kulyk Online 30 November 2001

Acta Cryst. (2001). E57, o1255-o1257  [ doi:10.1107/S1600536801019559 ] (4R,5R)-2-(N-Methyl-benzylamino)-3-nitro-4-(1',2',3',4',5'-penta-O-acetyl-D-manno-pentitol-1-yl)-5-phenyl-5-phenylcarbamoyl-4,5-dihydrothiophene at 150  K M. J. Diánez, M. D. Estrada, A. López-Castro and S. Pérez-Garrido Online 30 November 2001

Acta Cryst. (2001). E57, o1258-o1260  [ doi:10.1107/S1600536801020074 ] 2-Dihydroxymethyl-3H-benzoimidazol-1-ium chloride monohydrate A. J. Blake, S. J. Hill and P. Hubberstey Online 30 November 2001

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