Acta Cryst. (2001). E57, m568-m569  [ doi:10.1107/S1600536801018554 ]

Bis(p-chlorothiophenolato)bis(tri-n-butylphosphine)nickel(II)

I. A. Guzei, M. J. Moloto and J. Darkwa

Online 10 November 2001

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean (C-C) = 0.005 Å
• R factor = 0.043
• wR factor = 0.126
• Data-to-parameter ratio = 19.3

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           26.37                 
         From the CIF: _reflns_number_total               3843                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         4171                           
         Completeness (_total/calc)             92.14%                          
          Alert C: < 95% complete                                               


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check

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