(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, o77-o78 [ doi:10.1107/S160053680102027X ]

Tetrahydrothiophene tris(pentafluorophenyl)borane

F. Schaper and H.-H. Brintzinger

Online 22 December 2001

Key indicators

Single-crystal X-ray study
T = 230 K
Mean (C-C) = 0.002 Å
R factor = 0.031
wR factor = 0.083
Data-to-parameter ratio = 11.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.00                 
         From the CIF: _reflns_number_total               4359                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         4609                           
         Completeness (_total/calc)             94.58%                          
          Alert C: < 95% complete                                               


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check