Acta Cryst. (2002). E58, m10-m12  [ doi:10.1107/S1600536801020542 ]

-Oxo-bis{chloro[N,N'-dimethyl-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine]iron(III)} diperchlorate 0.751-hydrate

R. K. Egdal, A. Hazell and C. J. McKenzie

Key indicators

• Single-crystal X-ray study
• T = 120 K
• Mean (C-C) = 0.003 Å
• Disorder in solvent or counterion
• R factor = 0.032
• wR factor = 0.034
• Data-to-parameter ratio = 16.2

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



PLAT_420  Alert B D-H Without Acceptor      >O10    -  >HO10A             ?


 Alert Level C:



PLAT_302  Alert C Anion/Solvent Disorder .......................      36.00 Perc.


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 1 Alert Level C = Please check

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