Acta Cryst. (2002). E58, o336-o337  [ doi:10.1107/S1600536802003215 ]

A vinylic -carbamoyloxyborane with a carbenoid-type bonding arrangement

P. Kocienski, M. Marsch, K. Harms and G. Boche

Online 28 February 2002

Key indicators

• Single-crystal X-ray study
• T = 193 K
• Mean (C-C) = 0.007 Å
• R factor = 0.059
• wR factor = 0.169
• Data-to-parameter ratio = 10.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level A:



THETM_01  Alert A The value of sine(theta_max)/wavelength is less than 0.550    
          Calculated sin(theta_max)/wavelength =    0.5327                      

General Notes



ABSTM_02  When printed, the submitted absorption T values will be replaced      
          by the scaled T values. Since the ratio of scaled T's is              
          identical to the ratio of reported T values, the scaling does         
          not imply a change to the absorption corrections used in the          
          study.                                                                
          Ratio of Tmax expected/reported      1.372                            
          Tmax scaled      0.919 Tmin scaled      0.686                         


 1 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 0 Alert Level C = Please check

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