(IUCr) Crystallography Journals Online

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Acta Cryst. (2002). E58, o407-o408 [ doi:10.1107/S1600536802004464 ]

cis-[4a]-cisoid-[4a,4b]-cis-[4b]-4b,8b-Diethyl-1,3,5,7-tetramethylperhydro-1,3,5,7-tetraazabiphenylene-2,4,6,8-tetraone

C. Näther, O. Krüger and U. Wille

Abstract: The title compound, C₁₆H₂₄N₄O₄, was prepared by [2+2]-photocycloaddition of 1,3-dimethyl-6-ethyluracil in acetone. The structure determination was undertaken in order to determine the stereoconfiguration of the product, which could not be extracted from NMR data. However, single-crystal X-ray analysis revealed that the ethyl groups are located on the same side of the cyclobutane ring (cis) and that the monomers are oriented head-to-tail (anti).

Online 15 March 2002