Acta Cryst. (2002). E58, i29-i31 [ doi:10.1107/S1600536802003574 ]
No syntax errors found ADDSYM reports no extra symmetry
Alert Level B:
ABSTM_02 Alert B The ratio of expected to reported Tmax/Tmin(RR') is < 0.75 Tmin and Tmax reported: 0.406 0.710 Tmin' and Tmax expected: 0.653 0.771 RR' = 0.675 Please check that your absorption correction is appropriate.
Alert Level C:
PLAT_420 Alert C D-H Without Acceptor P - H(1) ? General Notes
ABSTM_02 When printed, the submitted absorption T values will be replaced by the scaled T values. Since the ratio of scaled T's is identical to the ratio of reported T values, the scaling does not imply a change to the absorption corrections used in the study. Ratio of Tmax expected/reported 1.085 Tmax scaled 0.771 Tmin scaled 0.441 REFLT_03 From the CIF: _diffrn_reflns_theta_max 33.98 From the CIF: _reflns_number_total 1798 Count of symmetry unique reflns 1063 Completeness (_total/calc) 169.14% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 735 Fraction of Friedel pairs measured 0.691 Are heavy atom types Z>Si present yes Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF.
0 Alert Level A = Potentially serious problem
1 Alert Level B = Potential problem
1 Alert Level C = Please check
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