(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, m234-m236 [ doi:10.1107/S1600536802007444 ]

catena-Poly[[[diaqualanthanum(III)]-tri--glycinato] trichloride monohydrate]

S.-L. Gao, Y.-Z. Li, F. Ren, Q.-Z. Shi and L.-F. Wang

Online 30 April 2002

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.006 Å
R factor = 0.032
wR factor = 0.086
Data-to-parameter ratio = 16.2

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           25.00                 
         From the CIF: _reflns_number_total               3168                  
         Count of symmetry unique reflns         1895                           
         Completeness (_total/calc)            167.18%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured      1273                           
         Fraction of Friedel pairs measured     0.672                           
         Are heavy atom types Z>Si present          yes                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.