Acta Cryst. (2002). E58, m231-m233  [ doi:10.1107/S1600536802007493 ]

{[-Bis(salicylidene)-1,3-propanediaminato]bis(N,N-dimethylformamide)nickel(II)}diiodozinc(II)

L. Tatar

Online 30 April 2002

Key indicators

• Single-crystal X-ray study
• T = 295 K
• Mean (C-C) = 0.014 Å
• R factor = 0.032
• wR factor = 0.086
• Data-to-parameter ratio = 10.5

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_213  Alert C Atom C19B    has ADP max/min Ratio ...........       3.60 prolate

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.66                 
         From the CIF: _reflns_number_total               3420                  
         Count of symmetry unique reflns         3416                           
         Completeness (_total/calc)            100.12%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured         4                           
         Fraction of Friedel pairs measured     0.001                           
         Are heavy atom types Z>Si present          yes                         
          WARNING: Large fraction of Friedel related reflns may                 
                   be needed to determine absolute structure                    


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check

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