# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' mm26b in C2/c [NH4(Zn,Ga)2(PO4)2]' _shelx_refln_list_code 4 _shelx_F_calc_maximum 455.08 _exptl_crystal_F_000 1328.00 _reflns_d_resolution_high 0.7100 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 13.3700 _cell_length_b 13.1900 _cell_length_c 8.9980 _cell_angle_alpha 90.000 _cell_angle_beta 100.460 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 33006.91 38884.79 502.11 o 8 0 0 7484.26 7910.35 104.57 o 10 0 0 12193.28 13490.76 247.67 o 12 0 0 1387.28 2541.11 80.79 o 14 0 0 25880.10 26181.37 679.73 o 16 0 0 3105.03 4456.35 240.96 o 18 0 0 17541.78 18697.61 1015.26 o 1 1 0 304.15 314.23 9.55 o 3 1 0 691.75 991.47 16.90 o 5 1 0 4428.97 4540.46 44.02 o 7 1 0 17529.23 17550.67 201.30 o 9 1 0 19439.92 20365.83 218.16 o 11 1 0 9359.32 9173.08 137.93 o 13 1 0 21926.29 21793.15 381.57 o 15 1 0 2558.18 2730.52 116.80 o 17 1 0 4067.35 3988.94 160.82 o 2 2 0 871.13 1098.12 21.31 o 4 2 0 50009.30 52609.89 520.27 o 6 2 0 2413.33 2608.07 41.16 o 8 2 0 27818.38 28564.61 503.25 o 10 2 0 8162.60 7921.51 98.83 o 12 2 0 5746.34 5918.89 88.98 o 14 2 0 5116.25 5000.47 89.91 o 16 2 0 1136.47 1194.00 47.80 o 18 2 0 2000.54 1805.61 81.53 o 1 3 0 6005.12 5579.72 51.11 o 3 3 0 2751.13 2813.85 27.86 o 5 3 0 14807.50 14444.14 131.70 o 7 3 0 1561.59 1907.09 19.03 o 9 3 0 2256.31 2092.11 47.76 o 11 3 0 232.56 268.25 8.78 o 13 3 0 121.84 169.21 17.62 o 15 3 0 1989.13 2008.35 52.39 o 17 3 0 155.42 157.41 25.78 o 2 4 0 43503.68 46518.21 417.19 o 4 4 0 89.00 89.57 10.28 o 6 4 0 82476.12 87700.35 885.90 o 8 4 0 28718.33 28246.45 390.99 o 10 4 0 18.39 1452.15 90.30 o 12 4 0 24627.15 24428.31 499.57 o 14 4 0 8660.73 8405.96 153.66 o 16 4 0 360.27 925.76 109.39 o 18 4 0 6337.85 6112.74 319.76 o 1 5 0 8915.60 8901.56 91.55 o 3 5 0 3.78 678.83 11.33 o 5 5 0 1297.73 1241.31 14.69 o 7 5 0 7982.95 9400.30 144.33 o 9 5 0 3947.52 4528.54 57.13 o 11 5 0 1375.59 1406.03 41.86 o 13 5 0 7471.17 7353.87 196.38 o 15 5 0 20.96 24.08 19.09 o 17 5 0 651.77 561.08 36.65 o 0 6 0 104911.54 110162.05 2773.59 o 2 6 0 7083.34 7268.31 63.01 o 4 6 0 48128.79 53442.54 442.71 o 6 6 0 2437.65 2468.05 30.13 o 8 6 0 20092.72 22377.19 376.92 o 10 6 0 3577.07 3613.19 54.35 o 12 6 0 2078.31 2533.05 63.17 o 14 6 0 500.30 498.12 23.60 o 16 6 0 1320.27 1271.29 50.60 o 1 7 0 9519.56 10048.25 142.31 o 3 7 0 4055.62 4076.67 43.39 o 5 7 0 24237.70 25244.51 246.04 o 7 7 0 33.52 72.30 3.78 o 9 7 0 10157.25 10181.90 155.34 o 11 7 0 49.58 140.64 11.91 o 13 7 0 1486.17 1719.78 61.69 o 15 7 0 2703.30 2849.23 83.70 o 17 7 0 972.96 980.61 58.26 o 0 8 0 2312.03 2799.46 38.14 o 2 8 0 22602.07 23721.39 219.70 o 4 8 0 17573.03 18791.05 247.54 o 6 8 0 60928.43 61096.36 618.65 o 8 8 0 67085.16 68781.77 906.66 o 10 8 0 8416.04 8494.60 124.46 o 12 8 0 35071.85 34418.54 636.73 o 14 8 0 30.38 30.83 24.96 o 16 8 0 1108.76 1009.14 49.93 o 1 9 0 25512.67 25639.35 308.25 o 3 9 0 387.73 433.73 30.10 o 5 9 0 19071.93 18554.18 192.18 o 7 9 0 3276.88 3503.81 42.64 o 9 9 0 2096.51 2127.52 34.79 o 11 9 0 65.40 123.38 27.90 o 13 9 0 65.77 56.95 19.82 o 15 9 0 4232.72 4147.47 112.75 o 0 10 0 38900.66 38269.53 541.68 o 2 10 0 389.82 714.18 30.84 o 4 10 0 31878.38 31187.24 349.05 o 6 10 0 2597.51 2665.96 33.54 o 8 10 0 6846.87 7301.02 115.61 o 10 10 0 1413.06 1541.39 37.35 o 12 10 0 4512.24 4752.99 96.97 o 14 10 0 2379.62 2392.28 69.50 o 1 11 0 658.65 934.93 23.50 o 3 11 0 497.96 520.38 34.51 o 5 11 0 2.37 56.73 13.95 o 7 11 0 2637.76 2677.19 49.15 o 9 11 0 662.92 629.45 22.31 o 11 11 0 4746.23 4718.04 108.58 o 13 11 0 2587.44 2546.74 81.99 o 0 12 0 26919.94 26764.24 561.60 o 2 12 0 6939.21 7391.17 96.97 o 4 12 0 5678.50 6832.91 125.00 o 6 12 0 12170.38 12374.08 215.88 o 8 12 0 2982.52 4130.18 296.07 o 10 12 0 6.75 172.29 18.89 o 12 12 0 3034.23 3015.49 89.11 o 14 12 0 7202.53 6712.88 251.86 o 1 13 0 8982.94 9731.56 137.04 o 3 13 0 359.20 376.07 13.31 o 5 13 0 5166.77 5381.04 90.60 o 7 13 0 7014.59 6907.61 153.06 o 9 13 0 87.64 93.43 16.92 o 11 13 0 1668.71 1741.76 62.08 o 13 13 0 1067.60 1007.37 72.70 o 0 14 0 3228.96 4694.01 217.48 o 2 14 0 727.19 906.51 38.18 o 4 14 0 2109.72 2503.42 48.70 o 6 14 0 0.30 46.10 12.70 o 8 14 0 17.88 17.41 16.89 o 10 14 0 108.28 139.52 26.34 o 12 14 0 32.62 247.71 32.30 o 1 15 0 13.42 88.24 12.95 o 3 15 0 120.12 188.93 14.39 o 5 15 0 4.41 29.14 13.02 o 7 15 0 65.44 148.74 30.83 o 9 15 0 362.22 479.80 53.60 o 0 16 0 31077.06 33018.94 965.08 o 2 16 0 1690.82 1795.44 45.56 o 4 16 0 15049.71 15956.75 328.80 o 6 16 0 2156.72 2123.83 69.81 o 8 16 0 0.77 41.00 21.26 o 1 17 0 2117.89 2166.17 68.46 o 3 17 0 772.08 758.57 42.59 o 5 17 0 281.17 261.61 30.84 o 7 17 0 5171.53 5151.71 193.24 o 0 18 0 1573.52 2347.97 194.61 o 2 18 0 731.38 685.32 34.91 o 4 18 0 2468.24 2834.90 100.77 o -17 1 1 3765.95 3708.40 130.55 o -15 1 1 1401.80 1543.51 49.26 o -13 1 1 111.02 163.34 20.56 o -11 1 1 693.29 795.69 24.23 o -9 1 1 40049.94 41176.41 433.52 o -7 1 1 11115.45 11937.69 114.28 o -5 1 1 30480.38 28736.71 263.60 o -3 1 1 55852.57 57321.20 714.43 o -1 1 1 9058.57 9332.13 120.73 o 1 1 1 29601.42 30635.65 322.60 o 3 1 1 33056.02 32706.41 344.48 o 5 1 1 1647.29 2599.62 33.07 o 7 1 1 6017.71 6325.47 85.38 o 9 1 1 34159.04 33105.18 446.49 o 11 1 1 6585.32 6815.89 92.75 o 13 1 1 5738.65 5607.07 101.50 o 15 1 1 13206.11 13358.39 305.87 o 17 1 1 253.27 292.34 27.50 o -18 2 1 1092.66 930.24 58.53 o -16 2 1 9178.37 9119.79 223.30 o -14 2 1 592.20 585.66 27.17 o -12 2 1 6353.45 6402.65 93.05 o -10 2 1 55.45 76.38 5.19 o -8 2 1 4840.76 5087.52 66.94 o -6 2 1 100.82 225.41 4.15 o -4 2 1 2897.72 2862.76 29.64 o -2 2 1 4723.09 4150.12 39.00 o 0 2 1 84.08 138.77 2.08 o 2 2 1 13761.17 13776.55 131.11 o 4 2 1 10147.02 9394.30 134.50 o 6 2 1 7565.44 7833.73 149.58 o 8 2 1 18674.95 17523.48 429.57 o 10 2 1 1128.78 1099.25 18.61 o 12 2 1 13839.01 13382.06 214.66 o 14 2 1 5.73 42.49 13.56 o 16 2 1 192.20 220.84 25.78 o 18 2 1 728.31 798.68 93.98 o -17 3 1 164.46 110.22 30.10 o -15 3 1 514.18 585.20 24.96 o -13 3 1 4305.63 4583.10 144.05 o -11 3 1 84.89 120.81 5.64 o -9 3 1 60620.84 60195.39 1030.22 o -7 3 1 8448.80 8612.77 95.05 o -5 3 1 52618.77 50044.29 478.61 o -3 3 1 90593.41 89813.24 1194.12 o -1 3 1 108377.33 106611.20 2490.11 o 1 3 1 16800.29 15942.06 150.69 o 3 3 1 12046.93 11561.60 105.59 o 5 3 1 5175.81 4544.28 41.92 o 7 3 1 8268.13 8305.15 168.69 o 9 3 1 70737.73 70567.35 1134.79 o 11 3 1 14474.38 14326.50 175.90 o 13 3 1 13969.76 14287.40 245.33 o 15 3 1 19702.96 19550.54 456.79 o 17 3 1 60.07 82.53 23.34 o -18 4 1 2912.29 2760.99 117.53 o -16 4 1 8488.60 8620.52 229.74 o -14 4 1 4374.23 4165.66 94.14 o -12 4 1 8207.73 8277.79 123.35 o -10 4 1 4004.97 4049.50 49.45 o -8 4 1 9543.82 9212.28 96.92 o -6 4 1 10962.05 10975.15 102.11 o -4 4 1 11634.34 12119.06 106.42 o -2 4 1 4327.38 3825.59 67.75 o 0 4 1 6255.32 5830.23 76.71 o 2 4 1 7841.40 7592.84 68.77 o 4 4 1 7829.46 7035.25 93.63 o 6 4 1 12353.24 12469.05 151.30 o 8 4 1 14491.19 13926.37 263.44 o 10 4 1 5656.32 5387.69 215.47 o 12 4 1 6721.11 6616.43 152.24 o 14 4 1 6814.36 6940.57 169.12 o 16 4 1 1644.39 1599.78 96.21 o -17 5 1 13742.47 14091.99 472.48 o -15 5 1 20028.37 20304.41 410.77 o -13 5 1 9185.25 9150.45 290.65 o -11 5 1 44909.44 43559.29 606.14 o -9 5 1 335.10 328.23 7.33 o -7 5 1 7054.67 7044.94 74.64 o -5 5 1 6486.82 6618.96 56.95 o -3 5 1 5434.98 4415.17 59.64 o -1 5 1 28178.21 25412.99 244.96 o 1 5 1 21166.97 18903.32 159.26 o 3 5 1 83838.75 82974.27 971.89 o 5 5 1 251.97 191.47 4.59 o 7 5 1 58986.93 59479.77 765.77 o 9 5 1 8715.58 8792.42 186.98 o 11 5 1 832.72 866.45 47.73 o 13 5 1 134.33 113.85 15.11 o 15 5 1 1489.94 1472.72 95.47 o 17 5 1 7508.22 7263.74 257.87 o -16 6 1 471.62 417.84 25.74 o -14 6 1 5046.59 4985.93 103.35 o -12 6 1 2742.20 2377.98 48.30 o -10 6 1 14005.29 13634.69 170.65 o -8 6 1 10037.14 9778.73 105.11 o -6 6 1 14272.28 14237.60 267.24 o -4 6 1 41802.97 42059.96 415.88 o -2 6 1 831.34 961.46 29.38 o 0 6 1 22976.36 22948.26 254.11 o 2 6 1 317.94 221.51 3.67 o 4 6 1 1827.06 1738.62 17.30 o 6 6 1 1532.75 1546.16 18.36 o 8 6 1 43.62 72.66 19.09 o 10 6 1 9613.55 9832.87 179.62 o 12 6 1 159.36 149.03 14.68 o 14 6 1 15289.96 15185.54 307.34 o 16 6 1 3919.75 3961.48 118.61 o -17 7 1 5374.16 5288.70 207.98 o -15 7 1 5015.87 4995.16 130.79 o -13 7 1 3905.63 4075.50 84.74 o -11 7 1 3014.94 3018.58 49.75 o -9 7 1 507.85 460.22 10.87 o -7 7 1 3.70 37.57 4.15 o -5 7 1 1009.58 939.33 11.42 o -3 7 1 22613.66 22806.80 429.18 o -1 7 1 8785.59 8134.19 204.91 o 1 7 1 11942.14 12261.12 264.98 o 3 7 1 64341.89 64741.02 599.98 o 5 7 1 4096.65 4305.67 46.76 o 7 7 1 21598.66 21024.96 247.56 o 9 7 1 4594.74 4553.55 71.07 o 11 7 1 1024.78 1002.13 24.67 o 13 7 1 199.67 196.20 16.55 o 15 7 1 2469.95 2374.69 83.74 o -16 8 1 104.06 122.26 21.14 o -14 8 1 548.73 539.47 26.35 o -12 8 1 132.78 83.25 12.33 o -10 8 1 3638.12 3483.71 56.83 o -8 8 1 1634.32 1522.60 21.52 o -6 8 1 1377.31 1343.95 18.61 o -4 8 1 1967.94 1956.80 25.31 o -2 8 1 5984.72 6333.93 61.16 o 0 8 1 4443.58 4390.44 58.10 o 2 8 1 3078.26 3242.37 30.45 o 4 8 1 1265.81 1180.92 23.50 o 6 8 1 1035.89 1066.49 16.62 o 8 8 1 313.01 368.85 11.91 o 10 8 1 4902.68 4680.43 69.56 o 12 8 1 18.39 45.55 33.04 o 14 8 1 1391.33 1288.32 61.69 o 16 8 1 456.54 379.75 32.14 o -15 9 1 3819.89 3399.30 105.89 o -13 9 1 457.18 422.26 22.31 o -11 9 1 12728.28 12127.67 212.43 o -9 9 1 8070.93 8132.26 129.02 o -7 9 1 25.89 59.06 4.59 o -5 9 1 9491.31 9676.40 158.33 o -3 9 1 5441.91 5364.17 57.39 o -1 9 1 2969.88 3105.96 52.18 o 1 9 1 15660.29 16318.49 176.45 o 3 9 1 27861.58 28083.85 281.54 o 5 9 1 2.43 18.53 3.78 o 7 9 1 18220.06 17281.91 228.40 o 9 9 1 5952.48 5534.51 85.22 o 11 9 1 2113.33 2157.43 47.25 o 13 9 1 577.50 489.27 22.56 o 15 9 1 3803.16 3986.49 137.39 o -14 10 1 2558.81 2540.49 73.45 o -12 10 1 23.23 41.72 15.03 o -10 10 1 5631.53 5723.44 133.80 o -8 10 1 1661.17 1789.34 34.23 o -6 10 1 2930.22 2915.10 38.71 o -4 10 1 7911.64 7834.25 99.36 o -2 10 1 1608.74 1596.95 20.47 o 0 10 1 2650.95 2452.43 27.52 o 2 10 1 6106.71 6500.44 70.37 o 4 10 1 555.33 494.20 9.50 o 6 10 1 416.52 497.25 11.91 o 8 10 1 1091.66 1127.53 27.51 o 10 10 1 2618.91 2771.93 63.31 o 12 10 1 32.71 34.14 17.92 o 14 10 1 5989.47 6209.78 175.91 o -15 11 1 6676.29 6310.08 227.14 o -13 11 1 2692.45 2702.44 111.65 o -11 11 1 9439.51 9446.07 170.39 o -9 11 1 530.14 516.37 22.77 o -7 11 1 4070.52 3954.90 70.58 o -5 11 1 1814.53 1815.57 33.79 o -3 11 1 3225.51 3183.83 60.99 o -1 11 1 6634.96 6777.68 82.17 o 1 11 1 4077.83 4041.55 53.54 o 3 11 1 22739.73 22639.69 287.46 o 5 11 1 842.84 779.37 27.90 o 7 11 1 9563.03 9781.17 150.33 o 9 11 1 817.72 892.22 27.52 o 11 11 1 1179.43 1084.23 37.64 o 13 11 1 8.01 9.53 22.30 o -14 12 1 2308.27 2287.19 79.46 o -12 12 1 933.83 869.76 34.08 o -10 12 1 5474.17 5364.47 111.73 o -8 12 1 3376.29 3254.74 68.49 o -6 12 1 1019.70 1062.79 28.54 o -4 12 1 3517.36 3416.43 55.40 o -2 12 1 629.15 612.39 14.54 o 0 12 1 3802.29 3859.01 54.02 o 2 12 1 27.64 27.90 7.27 o 4 12 1 1569.73 1609.94 28.04 o 6 12 1 135.82 171.34 21.29 o 8 12 1 214.62 239.44 48.46 o 10 12 1 5084.61 5156.36 138.01 o 12 12 1 2267.51 2225.69 75.89 o -13 13 1 1792.39 1792.04 81.52 o -11 13 1 3421.35 3067.81 96.85 o -9 13 1 21207.97 22126.25 471.85 o -7 13 1 778.28 766.35 64.62 o -5 13 1 37239.54 38045.80 666.94 o -3 13 1 6199.64 6479.90 95.38 o -1 13 1 9642.43 9780.73 138.43 o 1 13 1 4620.93 4844.94 69.65 o 3 13 1 632.35 594.79 19.09 o 5 13 1 6659.42 6268.35 111.61 o 7 13 1 78.23 82.00 16.07 o 9 13 1 16605.98 16147.24 372.49 o 11 13 1 8769.87 8697.08 296.35 o -12 14 1 3151.70 2936.20 97.78 o -10 14 1 72.20 43.46 17.97 o -8 14 1 43.14 31.42 14.66 o -6 14 1 738.17 694.45 23.21 o -4 14 1 381.90 367.02 18.15 o -2 14 1 8305.34 8251.58 148.51 o 0 14 1 230.03 225.82 17.62 o 2 14 1 14212.69 14295.42 224.86 o 4 14 1 6675.10 6561.66 144.84 o 6 14 1 5906.29 6060.54 120.82 o 8 14 1 9355.57 9304.06 213.83 o 10 14 1 422.63 392.03 32.60 o -11 15 1 26.74 -2.45 27.52 o -9 15 1 5768.93 6039.01 173.09 o -7 15 1 46.50 55.06 24.23 o -5 15 1 10759.81 10978.26 219.69 o -3 15 1 2053.05 2151.99 50.61 o -1 15 1 3810.94 3776.75 70.64 o 1 15 1 953.35 1030.03 27.43 o 3 15 1 91.73 99.42 13.95 o 5 15 1 217.84 157.84 49.19 o 7 15 1 177.21 141.00 23.49 o 9 15 1 2058.28 1892.65 74.26 o -8 16 1 98.15 121.78 23.60 o -6 16 1 555.43 515.98 42.58 o -4 16 1 106.56 77.05 14.42 o -2 16 1 1698.71 1784.69 79.32 o 0 16 1 311.39 350.78 25.70 o 2 16 1 3284.56 3272.37 74.80 o 4 16 1 1698.58 1661.23 51.43 o 6 16 1 1613.12 1468.90 62.29 o 8 16 1 2525.90 2280.94 94.87 o -7 17 1 274.90 285.39 40.38 o -5 17 1 3690.69 3878.06 126.79 o -3 17 1 3747.61 3840.14 121.45 o -1 17 1 831.86 751.40 31.72 o 1 17 1 3702.59 3766.49 106.41 o 3 17 1 6079.29 6232.39 173.43 o 5 17 1 874.99 699.00 38.04 o 7 17 1 3697.52 3675.41 191.82 o -4 18 1 2616.78 2382.80 92.01 o -2 18 1 77.81 39.06 25.71 o 0 18 1 772.04 662.68 32.86 o 2 18 1 774.19 699.87 80.03 o 4 18 1 783.90 777.05 59.47 o -18 0 2 4363.72 4332.37 273.35 o -16 0 2 305.41 259.90 30.84 o -14 0 2 43564.95 44997.25 955.87 o -12 0 2 17674.56 17783.65 345.31 o -10 0 2 76429.45 75354.80 1261.71 o -8 0 2 65436.13 67089.22 976.70 o -6 0 2 2386.44 3194.56 45.57 o -4 0 2 9674.13 10097.46 137.49 o -2 0 2 1356.33 1229.12 17.64 o 2 0 2 120607.42 118635.51 3376.48 o 4 0 2 57713.77 53140.58 777.44 o 8 0 2 16065.19 16110.16 211.20 o 10 0 2 44302.59 44219.08 735.15 o 12 0 2 1224.63 1261.66 38.19 o 14 0 2 1087.84 1061.83 44.06 o 16 0 2 59.60 76.35 33.77 o -17 1 2 2892.85 2854.70 108.98 o -15 1 2 205.43 206.39 21.29 o -13 1 2 881.02 769.94 19.00 o -11 1 2 4549.50 4494.32 86.01 o -9 1 2 952.01 1093.41 14.43 o -7 1 2 27942.45 27849.93 251.28 o -5 1 2 761.39 557.61 9.55 o -3 1 2 19579.39 18246.61 167.93 o 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11.91 o -9 3 2 3381.20 3138.12 36.89 o -7 3 2 652.70 702.78 9.35 o -5 3 2 935.72 949.38 10.87 o -3 3 2 1395.76 1342.52 25.72 o -1 3 2 28.37 90.35 2.20 o 1 3 2 96.42 114.37 8.08 o 3 3 2 348.13 345.93 5.19 o 5 3 2 12937.19 13018.13 112.70 o 7 3 2 6136.77 6307.38 62.94 o 9 3 2 5737.81 5761.13 91.94 o 11 3 2 6803.18 6582.50 122.83 o 13 3 2 838.60 852.46 25.27 o 15 3 2 1752.79 1742.14 52.48 o 17 3 2 537.70 590.23 35.98 o -18 4 2 443.68 508.54 48.27 o -16 4 2 7830.87 8034.54 183.01 o -14 4 2 9685.41 9451.57 177.92 o -12 4 2 5372.09 5301.20 97.05 o -10 4 2 8383.85 8044.54 139.12 o -8 4 2 61617.96 62037.39 702.65 o -6 4 2 49034.26 49390.21 631.50 o -4 4 2 21897.68 22802.27 374.35 o -2 4 2 68829.25 67521.88 1038.52 o 0 4 2 72873.53 72319.75 916.53 o 2 4 2 612.22 512.95 12.48 o 4 4 2 8733.48 7379.33 68.79 o 6 4 2 29568.47 29351.77 286.79 o 8 4 2 2497.28 2562.73 31.07 o 10 4 2 7314.89 7667.74 116.98 o 12 4 2 23842.00 23100.30 371.36 o 14 4 2 73.59 82.84 14.68 o 16 4 2 5419.21 5506.00 147.05 o -17 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